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公开(公告)号：JP2004034019A
公开(公告)日：2004-02-05
申请号：JP2002367784
申请日：2002-12-19
Applicant: Basf Ag , ビーエーエスエフ アクチェンゲゼルシャフト
Inventor： KAIBEL GERD DR , MILLER CHRISTIAN , KLAS KATRIN , KINDLER ALOIS , AQUILA WERNER , DOBLER WALTER , BREUER KLAUS , POMMER ACHIM , DIRNSTEINER THOMAS
CPC classification number: B01D3/141 , B01D3/14 , Y10S203/11 , Y10S203/20
Abstract: PROBLEM TO BE SOLVED: To provide a distillation column having high separation efficiency, in which the vapor amount is made constant all over the column including a feed section and a side steam take-off section.
SOLUTION: Partition walls DW are arranged substantially along the longitudinal direction of the distillation column so that the inside of the distillation column is divided into an upper zone 2 and a lower zone 4 of the feed section, an upper zone 3 and a lower zone 5 of the side stream take-off section, an upper common column section 1 and a lower common column section 6. A feeding mixture to be separated between the zones 2 and 4 of the feed section is in a wholly or partially vaporized state and/or the side stream to be taken off from the zones 3 and 5 of the side stream take-off section is in a wholly or partially vaporized state.
COPYRIGHT: (C)2004,JPO-
公开(公告)号：JP2004292461A
公开(公告)日：2004-10-21
申请号：JP2004202237
申请日：2004-07-08
Applicant: Basf Ag , ビーエーエスエフ アクチェンゲゼルシャフト
Inventor： ERNST HANSGEORG , DOBLER WALTER , PAUST JOACHIM , RHEUDE UDO
IPC: C07C41/18 , C07C45/45 , C07C49/303 , C07C403/24 , C07D317/46 , C07D317/50 , C07D317/54 , C07D407/06 , C07D407/12 , C07F9/54 , C09B23/10
CPC classification number: C07C403/24 , C07C403/04 , C07C403/08 , C07C403/10 , C07C2601/16 , C07D317/46 , C07F9/5435 , C07F9/5442 , Y02P20/55
Abstract: PROBLEM TO BE SOLVED: To improve a known method for synthesizing astaxanthin so as to avoid defects of a conventional technology for connecting a 9C unit with a 6C unit. SOLUTION: The 9C unit is connected with the proper 6C unit by using a 3-methylpentenyn-3-ol derivative represented by formula (I) (wherein, R 3 is an ether transformable into hydroxy by hydrolysis, a silyl ether or an acetal protective group) in an organic solvent in the presence of lithium amide instead of butyllithium or a Grignard reagent. The method for synthesizing is more economical than ones using butyllithium or a Grignard reagent. COPYRIGHT: (C)2005,JPO&NCIPI
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公开(公告)号：JP2003026620A
公开(公告)日：2003-01-29
申请号：JP2002130876
申请日：2002-05-02
Applicant: Basf Ag , ビーエーエスエフ アクチェンゲゼルシャフト
Inventor： ANSMANN ANDREAS , HENKELMANN JOCHEM , KINDLER ALOIS , ETZRODT HEINZ , OOST CARSTEN , STUTZ SUSANNE , TRAGUT CHRISTIAN , BOCKSTIEGEL BERNHARD , REIMER KLAUS , STROEZEL MANFRED , DOBLER WALTER
IPC: B01J23/44 , B01J23/50 , B01J35/04 , B01J35/06 , B01J37/02 , C07B61/00 , C07C29/17 , C07C29/32 , C07C29/42 , C07C33/02 , C07C33/048 , C07C45/48 , C07C45/62 , C07C45/67 , C07C49/203
CPC classification number: C07C49/203 , B01J23/44 , B01J23/50 , B01J35/04 , B01J35/06 , B01J37/0225 , C07C29/17 , C07C29/42 , C07C45/62 , C07C45/676 , C07C33/02 , C07C33/048 , C07C49/04
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing a higher α,β-unsaturated alcohol in which engineering is easily performed. SOLUTION: This method for producing the alcohol represented by formula Ia or Ib [R is a 1-4C alkyl group; R is a group of formula II (R is hydrogen or a 1-4C alkyl group; a broken line is an additional double bond; and n is 0 or 1-6), hydrogen, or a saturated alkyl group] comprises (a) mono-ethynylating a ketone or formula: R -CO-CH2 -R in ammonia solution by using a basic catalyst, (b) optionally hydrogenating the alcohol of formula Ib on a Pd catalyst, and (c) subjecting the hydrogenated product to a purification distillation, and if necessary, reacting Ia or Ib produced by the steps (a) to (c) or by the steps (a) and (c) with an alkyl acetoacetate of formula IV [R is a 1-4C alkyl group], or a diketene to provide a methyl ketone, and using the ketone as a starting material in the steps (a) to (c).
Abstract translation: 要解决的问题：提供一种制造其中易于进行工程的较高α，β-不饱和醇的方法。 解决方案：用于制备由式Ia或Ib表示的醇的方法[R 1]是1-4C烷基; R 2是式II的基团（R 3是氢或1-4C烷基;虚线是另外的双键; n是0或1-6），氢或饱和烷基 基团]包括（a）通过使用碱性催化剂在氨溶液中使酮或式：R 1 -CO-CH 2 -R 2单乙炔基化，（b）任选地在Pd催化剂上氢化式Ib的醇 和（c）使氢化产物进行纯化蒸馏，如果需要，使由步骤（a）至（c）或步骤（a）和（c）制备的Ia或Ib与式 IV [R 5是1-4C烷基]或二烯酮以提供甲基酮，并且在步骤（a） - （c）中使用酮作为原料。
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公开(公告)号：MXPA04004917A
公开(公告)日：2006-03-09
申请号：MXPA04004917
申请日：2002-12-05
Applicant: BASF AG
Inventor： DOBLER WALTER
IPC: B01D3/26 , B01J19/32 , B01D3/00 , B01J8/00 , B01J8/02 , B01J8/04 , B01J8/12 , B01J19/24 , B01J21/04 , B01J23/10 , B01J23/92 , B01J35/02 , B01J38/64 , B01J38/66 , C07B41/06 , C07B61/00 , C07C45/72 , C07C45/74 , C07C49/203
Abstract: Se describe un catalizador soportado que comprende uno o mas oxidos metalicos como componente activo en un soporte catalizador para llevar a cabo una condensacion de aldol. El soporte catalizador es oxido de y-aluminio, el componente activo es uno o mas oxidos de los metales de tierras raras y la concentracion de los componentes activos, en base al peso del soporte catalizador, se ubica en el rango de 5 hasta 12% en peso. La invencion se refiere ademas a un metodo para la produccion de pseudoionona mediante aldolizacion de citral y acetona por medio de destilacion reactiva en una columna en presencia de dicho catalizador y se describe tambien la regeneracion de catalizadores soportados con una solucion alcalina acuosa.
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公开(公告)号：AU2003246692A1
公开(公告)日：2004-02-02
申请号：AU2003246692
申请日：2003-07-14
Applicant: BASF AG
Inventor： KAIBEL GERD , MILLER CHRISTIAN , DOBLER WALTER , DIRNSTEINER THOMAS , HAHN THILO , BREUER KLAUS , AQUILA WERNER , GOBBEL HANS-GEORG
Abstract: A process is described for preparing tetrahydrogeranylacetone in which pseudoionone, geranylacetone and/or dihydrogeranylacetone in a liquid phase, in which particles of a catalyst which is capable of preferentially hydrogenating carbon-carbon double bonds over carbon-oxygen double bonds are suspended, is conducted through a device which inhibits the transport of the catalyst particles in the presence of a hydrogen-containing gas.
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Patent Agency Ranking
公开(公告)号：DE10226120A1
公开(公告)日：2003-12-24
申请号：DE10226120
申请日：2002-06-12
Applicant: BASF AG
Inventor： SIGL MARCUS , MILLER CHRISTIAN , DOBLER WALTER , HAAKE MATHIAS
IPC: B01J8/00 , B01J8/02 , B01J8/12 , B01J19/24 , B01J21/04 , B01J23/10 , B01J23/92 , B01J35/02 , C07C45/72 , C07C45/74 , C07C49/203
Abstract: The supported catalyst has one or more metal oxides as active components on a carrier for aldol condensation. The catalyst carrier is gamma -aluminum oxide. The active components include one or more oxides of rare earth metals. The concentration of the active components is 5-12 wt.% of the catalyst carrier weight. The active component is preferably yttrium oxide or praseodymium oxide. The condensation column packing (1) is composed of packing sheets (2) with straight kinks (5) forming angled kink surfaces (6). Catalyst particles (4) fill the space (3) between neighboring sheets.
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公开(公告)号：DE59408898D1
公开(公告)日：1999-12-16
申请号：DE59408898
申请日：1994-06-27
Applicant: BASF AG
Inventor： ERNST HANSGEORG , DOBLER WALTER , PAUST JOACHIM , RHEUDE UDO
IPC: C07C41/18 , C07C45/45 , C07C49/303 , C07C403/24 , C07D317/46 , C07D317/50 , C07D317/54 , C07D407/06 , C07D407/12 , C07F9/54 , C09B23/10
Abstract: Compounds of the general formula I in which R is H or C1-C4-alkyl, R is C1-C4-alkyl and R is an ether, silyl ether or acetal protective group which can be converted into a hydroxyl group by hydrolysis, in particular one of the radicals and a process for the production of these compounds by reacting an alkenyne of the general formula II in an inert solvent with additional use of lithium amide with a cyclohexenone of the general formula III and the use of the compounds of the formula I for the production of astaxanthin.
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公开(公告)号：AU2926495A
公开(公告)日：1996-02-09
申请号：AU2926495
申请日：1995-07-03
Applicant: BASF AG
Inventor： DOBLER WALTER , ECKHARDT HEINZ , SAMBALE CLEMENS , SCHWEIKERT LONI , KAH-HELBIG ASTRID
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公开(公告)号：NO942523L
公开(公告)日：1995-01-06
申请号：NO942523
申请日：1994-07-04
Applicant: BASF AG
Inventor： ERNST HANSGEORG , DOBLER WALTER , PAUST JOACHIM , RHEUDE UDO
IPC: C07C41/18 , C07C45/45 , C07C49/303 , C07C403/24 , C07D317/46 , C07D317/50 , C07D317/54 , C07D407/06 , C07D407/12 , C07F9/54 , C09B23/10
Abstract: Compounds of the general formula I in which R is H or C1-C4-alkyl, R is C1-C4-alkyl and R is an ether, silyl ether or acetal protective group which can be converted into a hydroxyl group by hydrolysis, in particular one of the radicals and a process for the production of these compounds by reacting an alkenyne of the general formula II in an inert solvent with additional use of lithium amide with a cyclohexenone of the general formula III and the use of the compounds of the formula I for the production of astaxanthin.
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公开(公告)号：NO942523A
公开(公告)日：1995-01-06
申请号：NO942523
申请日：1994-07-04
Applicant: BASF AG
Inventor： ERNST HANSGEORG , DOBLER WALTER , PAUST JOACHIM , RHEUDE UDO
IPC: C07C41/18 , C07C45/45 , C07C49/303 , C07C403/24 , C07D317/46 , C07D317/50 , C07D317/54 , C07D407/06 , C07D407/12 , C07F9/54 , C09B23/10
CPC classification number: C07C403/24 , C07C403/04 , C07C403/08 , C07C403/10 , C07C2601/16 , C07D317/46 , C07F9/5435 , C07F9/5442 , Y02P20/55
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