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    Preparation method of 2-alkyne-1-acetal
    1.
    发明专利
    Preparation method of 2-alkyne-1-acetal 有权
    2-烷基-1-乙酸的制备方法

    公开(公告)号：JP2006037233A

    公开(公告)日：2006-02-09

    申请号：JP2005213194

    申请日：2005-07-22

    Applicant: Basf Ag ,  ビーエーエスエフ アクチェンゲゼルシャフト

    Inventor： RICHTER INGO DR ,  GRIESBACH ULRICH ,  BECKER MICHAEL ,  KESSINGER ROLAND

    IPC: C25B3/02

    CPC classification number: C25B3/02

    Abstract: PROBLEM TO BE SOLVED: To economically prepare 2-alkyne-1-acetal with a high selectivity and in a high product yield.
    SOLUTION: In a preparation method of 2-alkyne-1-acetal of formula I (wherein substituents are as indicated in the patent claim), a compound of formula III (wherein R
    1 is as indicated in formula I) is electrochemically oxidized either in the presence of a 1-6C alkyl alcohol (alcohol A) or in the form of a substance.
    COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 待解决的问题：以高选择性和高产率生产经济地制备2-炔炔-1-缩醛。 解决方案：在式I（其中取代基如专利权利要求中所示）的2-炔炔-1-缩醛的制备方法中，式III化合物（其中R 1 = 在式I中表示）在1-6C烷基醇（醇A）或物质形式的存在下进行电化学氧化。 版权所有（C）2006，JPO＆NCIPI

    ELECTROCHEMICAL ALKOXYLATING OXIDATIVE CARBON-CARBON BOND CLEAVAGE IN 1,2-DIPHENYLETHANE AND DERIVATIVES THEREOF ON A DIAMOND ELECTRODE
    3.
    发明申请
    ELECTROCHEMICAL ALKOXYLATING OXIDATIVE CARBON-CARBON BOND CLEAVAGE IN 1,2-DIPHENYLETHANE AND DERIVATIVES THEREOF ON A DIAMOND ELECTRODE 审中-公开
    电化学氧化的烷氧基化炭键裂解AM 1,2-二苯基乙烷及其衍生物AT的金刚石电极

    公开(公告)号：WO2005066390A3

    公开(公告)日：2005-09-22

    申请号：PCT/EP2005000085

    申请日：2005-01-07

    Applicant: BASF AG ,  GRIESBACH ULRICH ,  PUETTER HERMANN ,  ZOLLINGER DANIEL

    Inventor： GRIESBACH ULRICH ,  PUETTER HERMANN ,  ZOLLINGER DANIEL

    IPC: C25B3/02

    CPC classification number: C25B3/02

    Abstract: The invention relates to a method for the electrolytic oxidative alkoxylating cleavage of 1,2-diarylethane derivatives by electrolytically oxidizing the respective 1,2-diarylethane derivative in a solvent containing the alcohol required for alkoxylation, electrolytic oxidation being performed on a diamond electrode. The inventive method makes it possible to especially produce diaryl derivatives when a 1,2-diarylethane derivative in which the two aryl radicals are directly bonded to each other is used as a substrate.

    Abstract translation: 本发明涉及一种用于通过在含有必需的烷氧基化醇，其中所述电解氧化在金刚石电极进行溶剂中的相应的1,2- Diarylethanderivats的电解氧化烷氧基化1,2- Diarylethanderivaten的电解氧化裂解 ， 特别是本发明的方法允许联芳基衍生物的制备中，当1,2- Diarylethanderivat被用作衬底，其中，所述两个芳基直接连接到彼此。

    ANODIC DIMERISATION OF SUBSTITUTED BENZOLS
    4.
    发明申请
    ANODIC DIMERISATION OF SUBSTITUTED BENZOLS 审中-公开
    阳极二聚取代苯

    公开(公告)号：WO2005075709A2

    公开(公告)日：2005-08-18

    申请号：PCT/EP2005001066

    申请日：2005-02-03

    Applicant: BASF AG ,  ROMMEL CHRISTINA E ,  MALKOWSKY ITAMAR ,  WALDVOGEL SIEGFRIED ,  PUETTER HERMANN ,  GRIESBACH ULRICH

    Inventor： ROMMEL CHRISTINA E ,  MALKOWSKY ITAMAR ,  WALDVOGEL SIEGFRIED ,  PUETTER HERMANN ,  GRIESBACH ULRICH

    IPC: C25B3/10

    CPC classification number: C25B3/10

    Abstract: The invention relates to a method for producing biarylalcohols by means of the electrodimerisation of arylalcohols, said method comprising the following steps: a) an aryloxy compound of the alcohol to be coupled is produced with an element from the group B and Al; b) the aryloxy compounds obtained in a) are electrolytically oxidised and coupled to form the corresponding biaryl derivatives; and c) the desired biaryl alcohols are released. The inventive method enables the dimerisation of arylalcohols with a high degree of selectivity in order to obtain an ortho product.

    Abstract translation: 本发明描述了通过包括以下步骤的芳基醇的electrodimerization为Biarylalkoholen的制备方法：a）制备醇的芳氧基化合物被加上从B组和Al的元素; B）电解氧化，并在获得的Arylloxyverbindungen的耦合），得到相应的二芳基衍生物; c）中释放期望的Biarylalkohole。 本发明的方法使得能够芳基醇的二聚化具有高选择性的邻位产物。

    ELECTROCHEMICAL METHOD FOR PRODUCING DIPHENYLPHOSPHINE OXIDE, DIPHENYLPHOSPHINE OR PHOSPHINE AND THEIR DERIVATIVES
    5.
    发明申请
    ELECTROCHEMICAL METHOD FOR PRODUCING DIPHENYLPHOSPHINE OXIDE, DIPHENYLPHOSPHINE OR PHOSPHINE AND THEIR DERIVATIVES 审中-公开
    电化学过程用于生产二苯基膦，DIPHENYLPHOPHIN磷化氢及其衍生物

    公开(公告)号：WO2005031040A3

    公开(公告)日：2005-11-24

    申请号：PCT/EP2004010420

    申请日：2004-09-17

    Applicant: BASF AG ,  GRIESBACH ULRICH ,  WEISKOPF VERENA ,  MAASE MATTHIAS

    Inventor： GRIESBACH ULRICH ,  WEISKOPF VERENA ,  MAASE MATTHIAS

    IPC: C25B3/04

    CPC classification number: C25B3/04

    Abstract: The invention relates to a method for producing diphenylphosphine oxide (DPPO) or its nucleus-substituted derivatives, diphenylphosphine (DPP) or its nucleus-substituted derivatives or phosphine (PP) or its nucleus-substituted derivatives, starting from triphenylphosphine oxide (TPPO) or the corresponding nucleus-substituted derivatives, or in the case of the production of DPP and PP, starting from triphenylphosphine (TPP) or the corresponding nucleus-substituted derivatives or DPPO. According to said method, the starting products are reduced electrochemically in the presence of ammonia or an amine.

    Abstract translation: 一种用于制备二苯基氧化膦或它的环上取代的衍生物（DPPO），二苯基膦或其环上取代的衍生物（DPP）或膦或其环上取代的衍生物（PP）过程中，从三苯基膦氧化物或相应的环上取代的衍生物（TPPO）或在DPP的制剂的情况下开始 和PP还从三苯基膦或相应的环取代的衍生物（TPP）或DPPO，其被电化学还原，起始产品中氨或胺的存在下开始。

    8.
    发明专利
    未知

    公开(公告)号：DE102005013631A1

    公开(公告)日：2006-09-28

    申请号：DE102005013631

    申请日：2005-03-24

    Applicant: BASF AG

    Inventor： RICHTER INGO ,  PUETTER HERMANN ,  GRIESBACH ULRICH ,  BOTTKE NILS

    IPC: C07D307/32 ,  C07D307/89 ,  C25B3/23

    Abstract: A process for the preparation of 2,5-dihydrofuran derivatives substituted in the 3- or 4-position, which in the 2- or in the 5-position or at both positions each carry a C 1 - to C 6 -alkoxy radical (DHF-alkoxy derivatives 1), or 1,1,4,4-tetraalkoxy-but-2-ene derivatives substituted in the 3- or 4-position, from 2-butene-1 ,4-diol derivatives of the general formula (I) in which the radicals R 1 and R 2 independently of one another are hydrogen, C 1 - to C 6 -alkyl, C 6 - to C 12 -aryl or C 5 - to C 12 -cycloalkylene or R 1 and R 2 , together with the double bond to which they are bonded, form a C 6 - to C 12 -aryl radical or a mono- or polyunsaturated C 5 - to C 12 -cycloalkyl radical, or from their mixture with 2,5-dihydrofuran derivatives substituted in the 3- position or 4-position, which in the 2- or in the 5-position carry a C 1 - to C 6 -alkoxy radical, by electro-chemical oxidation in the presence of a C 1 - to C 6 -monoalkyl alcohol.

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