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公开(公告)号：WO02062729A3
公开(公告)日：2003-01-30
申请号：PCT/EP0200766
申请日：2002-01-25
Applicant: BASF AG , ZEHNER PETER , BEY OLIVER , GEORGI GUNTER , MUELLER JOERN
Inventor： ZEHNER PETER , BEY OLIVER , GEORGI GUNTER , MUELLER JOERN
IPC: C07B43/04 , C07B61/00 , C07C209/36 , C07C211/45 , C07C211/46 , C07C211/47 , C07C211/50 , C07B31/00 , C07C209/32
CPC classification number: C07C209/36 , C07B43/04 , C07C211/50
Abstract: The invention relates to a method for hydrogenating liquid organic compounds, in particular for hydrogenating nitro compounds to obtain amines. Said method is characterised in that the hydrogen that is present in the reactor contains constituent parts of at least one gas that is inert during the hydrogenation reaction.
Abstract translation: 本发明涉及一种用于液体的有机化合物，特别是Nitroverbidungen氢化成胺的方法，其特征在于，存在于所述反应器包括氢化气体中的至少一个氢惰性的比例。
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公开(公告)号：DE59905881D1
公开(公告)日：2003-07-10
申请号：DE59905881
申请日：1999-12-09
Applicant: BASF AG
Inventor： SANDER MICHAEL , PENZEL ULRICH , SCHWARZ VOLKMAR , STROEFER ECKHARD , STUETZER DIETER , MUELLER JOERN , MAURER MARKUS , ZEHNER PETER , SCHWAB EKKEHARD , BOEHLING RALF , VANOPPEN DOMINIC
IPC: B01J10/00 , B01J19/00 , B01J19/24 , B01J19/26 , C07B61/00 , C07C209/32 , C07C209/34 , C07C209/36 , C07C211/46 , C07C211/50 , C07C211/51
Abstract: The invention relates to a process for the preparation of amines by hydrogenation of nitro compounds, which comprises carrying out the hydrogenation in a vertical reactor whose length is greater than its diameter, having a downward-facing jet nozzle arranged in the upper region of the reactor through which the starting materials and the reaction mixture are fed in, and having an outlet at any desired point of the reactor, through which the reaction mixture is fed back to the jet nozzle in an external circuit by means of a conveying means, and having flow reversal in the lower region of the reactor.
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公开(公告)号：DE59902306D1
公开(公告)日：2002-09-12
申请号：DE59902306
申请日：1999-11-23
Applicant: BASF AG
Inventor： BERG STEFAN , ZEHNER PETER , BENFER REGINA , MUELLER JOERN , NILLES MICHAEL , SCHULZ RALF , STUETZER DIETER
IPC: B01J8/22 , B01J10/00 , B01J19/00 , B01J19/24 , B01J19/26 , C07B61/00 , C07C45/72 , C07C51/235 , C07C53/122
Abstract: A reactor (1) of high cylindrical construction for continuously carrying out gas-liquid, liquid-liquid or gas-liquid-solid reactions, provided with a downward-directed jet nozzle (2) via which the starting materials and the reaction mixture are fed in and which is located in the upper region of the reactor, and provided with an offtake (3), preferably in the lower region of the reactor, via which the reaction mixture is conveyed via an external circuit back to the jet nozzle (2) by means of a pump (P), wherein a guide tube (4) which extends essentially over the total length of the reactor (1) with the exception of the reactor ends and has a cross-sectional area in the range from one tenth to one half of the cross-sectional area of the reactor (1) is located concentrically in the reactor (1), and the jet nozzle (2) is located above the upper end of the guide tube (4), preferably at a distance of from one eighth of the guide tube diameter to one guide tube diameter, or projects into the guide tube (4) to a depth up to a plurality of guide tube diameters is proposed. A heat exchanger, in particular a heat exchanger having heat exchange tubes (6), preferably running parallel to the guide tube, welded in between plates (5), is integrated into the annular space.
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公开(公告)号：DE19854637A1
公开(公告)日：2000-05-31
申请号：DE19854637
申请日：1998-11-26
Applicant: BASF AG
Inventor： BERG STEFAN , ZEHNER PETER , BENFER REGINA , MUELLER JOERN , NILLES MICHAEL , SCHULZ RALF , STUETZER DIETER
IPC: B01J8/22 , B01J10/00 , B01J19/00 , B01J19/24 , B01J19/26 , C07B61/00 , C07C45/72 , C07C51/235 , C07C53/122 , B01J14/00 , B01J8/00
Abstract: The invention relates to a vertical cylinder reactor (1) for carrying out gas-liquid, liquid-liquid or gas-liquid-solid chemical reactions. Said reactor comprises a nozzle (2) which is arranged in the upper portion of the reactor and which is directed downwards and by way of which the educts and the reaction mixture are supplied. The reactor further comprises a discharge (3), preferably in the lower portion of the reactor, through which the reaction mixture can be re-fed to the nozzle (2) via an exterior circuit by way of a pump (P). A concentric guide tube is arranged in the reactor which substantially extends across the entire length of the reactor (1) except the reactor ends. Said guide tube has a cross-sectional area in the range of a tenth to half of the cross-sectional area of the reactor (1). The nozzle is arranged above the upper end of the guide tube (4), preferably in a distance of an eighth to a full cross-sectional area of the guide tube or it dips into the guide tube (4) in a depth of up to several cross-sectional areas of the guide tube. A heat exchanger is integrated into the annulus, especially a heat exchanger with heat exchanger tubes (6) welded between bottoms (6). Said tubes are preferably arranged parallel to the guide tube.
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公开(公告)号：AT266692T
公开(公告)日：2004-05-15
申请号：AT01927689
申请日：2001-02-22
Applicant: BASF AG
Inventor： OSTROWSKI THOMAS , HARRE KATHRIN , ZEHNER PETER , MUELLER JOERN , STUETZER DIETER , GROSCH GEORG HEINRICH , WINKLER JUERGEN , BAUER STEPHAN
Abstract: Production of polyether polyols comprises use of a multi-metal cyanide complex catalyst in a tall cylindrical reactor having a downward facing spray nozzle in the upper reactor portion, through which the educts and reaction mixture are fed and an outlet, preferably in the lower portion of the reactor to recirculate the reaction mixture via an external circuit and equalizing reservoir. A process for the production of polyether polyols (I) by reaction of diols or polyols with ethylene oxide, propylene oxide and/or butylene oxide in the presence of a multi-metal cyanide complex catalyst (II) comprises carrying out the reaction in a tall cylindrical reactor having a downward facing spray nozzle in the upper reactor portion, through which the educts and reaction mixture are fed, and an outlet, preferably in the lower portion of the reactor, through which the reaction mixture is fed by means of a pump through an external circuit via an equalizing reservoir to the spray nozzle. The external circuit comprises a concentric pipe stretching the entire length of the reactor excluding the reactor ends and contains a heat exchanger integrated within the annulus.
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Patent Agency Ranking
公开(公告)号：DE10124600A1
公开(公告)日：2002-11-28
申请号：DE10124600
申请日：2001-05-21
Applicant: BASF AG
Inventor： VANOPPEN DOMINIC , SCHWAB EKKEHARD , MUELLER JOERN , PENZEL ULRICH , GEORGI GUNTER , WEIDNER BERND , TITTELBACH-HELMRICH DIETRICH , DAHLHAUS JUERGEN
IPC: B01J23/76 , B01J21/06 , B01J23/755 , B01J23/78 , B01J23/83 , B01J35/10 , B01J37/03 , B01J37/16 , C07B61/00 , C07C209/36 , C07C211/46 , C07C211/47 , C07C211/50 , C07C211/51 , C07C211/44
Abstract: Production of a supported nickel catalyst involves co-precipitating nickel and at least one other metal (M), selected from silicon, zirconium, hafnium, alkaline earth metals, yttrium, lanthanum and cerium, and optionally a Group 5-11 metal dopant, from a solution containing the corresponding metal salts onto a particulate titania (TiO2) support, and drying, calcining, reducing and optionally passivating the product. An Independent claim is included for a process in which the above catalyst is used.
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公开(公告)号：DE10105277A1
公开(公告)日：2002-08-14
申请号：DE10105277
申请日：2001-02-02
Applicant: BASF AG
Inventor： ZEHNER PETER , BEY OLIVER , GEORGI GUNTER , MUELLER JOERN
IPC: C07B43/04 , C07B61/00 , C07C209/36 , C07C211/45 , C07C211/46 , C07C211/47 , C07C211/50 , C07B31/00
Abstract: The invention relates to a method for hydrogenating liquid organic compounds. Said method is characterised in that the hydrogen that is present in the reactor contains constituent parts of at least one gas that is inert during the hydrogenation reaction.
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公开(公告)号：HU229646B1
公开(公告)日：2014-03-28
申请号：HU0400780
申请日：2002-05-16
Applicant: BASF AG
Inventor： VANOPPEN DOMINIC , SCHWAB EKKEHARD , MUELLER JOERN , PENZEL ULRICH , GEORGI GUNTER , WEIDNER BERND , TITTELBACH-HELMRICH DIETRICH , DAHLHAUS JUERGEN
IPC: B01J23/755 , B01J23/76 , B01J21/06 , B01J23/78 , B01J23/83 , B01J35/10 , B01J37/03 , B01J37/16 , C07B61/00 , C07C209/36 , C07C211/46 , C07C211/47 , C07C211/50 , C07C211/51
Abstract: A catalyst comprising nickel on a TiO 2 support is obtainable by coprecipitation of nickel and at least one further metal selected from among Si, Zr, Hf, alkaline earth metals, Y, La and Ce, and optionally at least one dopant metal selected from groups 5 to 11 of the Periodic Table of the Elements, from a solution in which the corresponding metal salts are present onto a particulate TiO 2 support, subsequent drying, calcination and reduction and optionally passivation to give the nickel-containing catalyst. It is used, in particular, for the hydrogenation of nitroaromatic compounds.
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公开(公告)号：DE50206151D1
公开(公告)日：2006-05-11
申请号：DE50206151
申请日：2002-05-16
Applicant: BASF AG
Inventor： VANOPPEN DOMINIC , SCHWAB EKKEHARD , MUELLER JOERN , PENZEL ULRICH , GEORGI GUNTER , WEIDNER BERND , TITTELBACH-HELMRICH DIETRICH , DAHLHAUS JUERGEN
IPC: B01J23/755 , B01J23/76 , B01J21/06 , B01J23/78 , B01J23/83 , B01J35/10 , B01J37/03 , B01J37/16 , C07B61/00 , C07C209/36 , C07C211/46 , C07C211/47 , C07C211/50 , C07C211/51
Abstract: A catalyst comprising nickel on a TiO 2 support is obtainable by coprecipitation of nickel and at least one further metal selected from among Si, Zr, Hf, alkaline earth metals, Y, La and Ce, and optionally at least one dopant metal selected from groups 5 to 11 of the Periodic Table of the Elements, from a solution in which the corresponding metal salts are present onto a particulate TiO 2 support, subsequent drying, calcination and reduction and optionally passivation to give the nickel-containing catalyst. It is used, in particular, for the hydrogenation of nitroaromatic compounds.
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公开(公告)号：DE10008630A1
公开(公告)日：2001-09-06
申请号：DE10008630
申请日：2000-02-24
Applicant: BASF AG
Inventor： OSTROWSKI THOMAS , HARRE KATHRIN , ZEHNER PETER , MUELLER JOERN , STUETZER DIETER , GROSCH GEORG HEINRICH , WINKLER JUERGEN , BAUER STEPHAN
Abstract: Production of polyether polyols comprises use of a multi-metal cyanide complex catalyst in a tall cylindrical reactor having a downward facing spray nozzle in the upper reactor portion, through which the educts and reaction mixture are fed and an outlet, preferably in the lower portion of the reactor to recirculate the reaction mixture via an external circuit and equalizing reservoir. A process for the production of polyether polyols (I) by reaction of diols or polyols with ethylene oxide, propylene oxide and/or butylene oxide in the presence of a multi-metal cyanide complex catalyst (II) comprises carrying out the reaction in a tall cylindrical reactor having a downward facing spray nozzle in the upper reactor portion, through which the educts and reaction mixture are fed, and an outlet, preferably in the lower portion of the reactor, through which the reaction mixture is fed by means of a pump through an external circuit via an equalizing reservoir to the spray nozzle. The external circuit comprises a concentric pipe stretching the entire length of the reactor excluding the reactor ends and contains a heat exchanger integrated within the annulus.
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