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公开(公告)号:DE19827086A1
公开(公告)日:1999-12-23
申请号:DE19827086
申请日:1998-06-18
Applicant: BASF AG
Inventor: THERRE JOERG , SCHWARZ HANS VOLKMAR , MAURER MARKUS , SANDER MICHAEL , STROEFER ECKHARD , LEUTHOLD RENE , HANTEL BURGHARD , RICHTER SIEGFRIED
IPC: C07C263/20 , C07C209/62 , C07C211/51 , C07C263/10 , C07C263/18 , C07C265/14 , C08G18/50 , C08G65/26
Abstract: The invention relates to a method for treating distillation residues from the synthesis of toluene diisocyanate by reacting the distillation residues with water. The invention is characterized in that the TDI distillation residues are reacted with water in a continuos or semi-continuos method in a back-mixed reactor in the presence of hydrolyzates.
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公开(公告)号:DE59907555D1
公开(公告)日:2003-12-04
申请号:DE59907555
申请日:1999-06-02
Applicant: BASF AG
Inventor: SCHWARZ VOLKMAR , MAURER MARKUS , SANDER MICHAEL , STROEFER ECKHARD , LEUTHOLD RENE , HANTEL BURGHARD , RICHTER SIEGFRIED , THERRE JOERG
IPC: C07C263/20 , C07C209/62 , C07C211/51 , C07C263/10 , C07C263/18 , C07C265/14 , C08G18/50 , C08G65/26
Abstract: A process for working up distillation residues from the synthesis of tolylene diisocyanate by reaction of the distillation residues with water comprises reacting the TDI distillation residues with water in a continuous or semicontinuous process in a backmixed reactor in the presence of hydrolysate.
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公开(公告)号:DE59905881D1
公开(公告)日:2003-07-10
申请号:DE59905881
申请日:1999-12-09
Applicant: BASF AG
Inventor: SANDER MICHAEL , PENZEL ULRICH , SCHWARZ VOLKMAR , STROEFER ECKHARD , STUETZER DIETER , MUELLER JOERN , MAURER MARKUS , ZEHNER PETER , SCHWAB EKKEHARD , BOEHLING RALF , VANOPPEN DOMINIC
IPC: B01J10/00 , B01J19/00 , B01J19/24 , B01J19/26 , C07B61/00 , C07C209/32 , C07C209/34 , C07C209/36 , C07C211/46 , C07C211/50 , C07C211/51
Abstract: The invention relates to a process for the preparation of amines by hydrogenation of nitro compounds, which comprises carrying out the hydrogenation in a vertical reactor whose length is greater than its diameter, having a downward-facing jet nozzle arranged in the upper region of the reactor through which the starting materials and the reaction mixture are fed in, and having an outlet at any desired point of the reactor, through which the reaction mixture is fed back to the jet nozzle in an external circuit by means of a conveying means, and having flow reversal in the lower region of the reactor.
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公开(公告)号:DE10260082A1
公开(公告)日:2004-07-01
申请号:DE10260082
申请日:2002-12-19
Applicant: BASF AG
Inventor: SOHN MARTIN , STROEFER ECKHARD , NEVEJANS FILIP , PENZEL ULRICH , PALLASCH HANS-JUERGEN , LEUTHOLD RENE , BRODHAGEN ANDREAS , WOELFERT ANDREAS , MACKENROTH WOLFGANG , MAURER MARKUS
IPC: C07C263/10 , C07C265/14
Abstract: The invention relates to a process for preparing polyisocyanates by reacting organic amines with phosgene, wherein the reaction is carried out in at least three stages, with the first stage being carried out in a mixing apparatus, the second stage in at least one residence apparatus and the third stage in at least one separation apparatus and the pressure in each successive stage being lower than that in the previous stage.
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公开(公告)号:DE19857409A1
公开(公告)日:2000-06-15
申请号:DE19857409
申请日:1998-12-12
Applicant: BASF AG
Inventor: SANDER MICHAEL , PENZEL ULRICH , SCHWARZ HANS VOLKMAR , STROEFER ECKHARD , STUETZER DIETER , MUELLER JOERN , MAURER MARKUS
IPC: B01J10/00 , B01J19/00 , B01J19/24 , B01J19/26 , C07C209/36 , C07C211/51 , C07B43/04 , C07C209/32
Abstract: The production of amines (I) by hydrogenation of nitro compounds (II), carried out in a vertical reactor with length greater than its diameter. It has a spray at the top for introducing educts and reaction mixture and an outlet through which the reaction mixture is pumped into an external cycle. The circulation is reversed in the lower zone of the reactor.
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公开(公告)号:CA2335068A1
公开(公告)日:1999-12-23
申请号:CA2335068
申请日:1999-06-02
Applicant: BASF AG
Inventor: LEUTHOLD RENE , SANDER MICHAEL , STROFER ECKHARD , SCHWARZ HANS VOLKMAR , HANTEL BURGHARD , THERRE JORG , MAURER MARKUS , RICHTER SIEGFRIED
IPC: C07C263/20 , C07C209/62 , C07C211/51 , C07C263/10 , C07C263/18 , C07C265/14 , C08G18/50 , C08G65/26
Abstract: The invention relates to a method for treating distillation residues from th e synthesis of toluene diisocyanate by reacting the distillation residues with water. The invention is characterized in that the TDI distillation residues are reacted with water in a continuos or semi-continuos method in a back-mix ed reactor in the presence of hydrolyzates.
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公开(公告)号:CA2335068C
公开(公告)日:2005-05-17
申请号:CA2335068
申请日:1999-06-02
Applicant: BASF AG
Inventor: SANDER MICHAEL , STROFER ECKHARD , THERRE JORG , RICHTER SIEGFRIED , HANTEL BURGHARD , LEUTHOLD RENE , SCHWARZ HANS VOLKMAR , MAURER MARKUS
IPC: C07C263/20 , C07C209/62 , C07C211/51 , C07C263/10 , C07C263/18 , C07C265/14 , C08G18/50 , C08G65/26
Abstract: The invention relates to a method for treating distillation residues from th e synthesis of toluene diisocyanate by reacting the distillation residues with water. The invention is characterized in that the TDI distillation residues are reacted with water in a continuos or semi-continuo s method in a back-mixed reactor in the presence of hydrolyzates.
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公开(公告)号:AU2003293871A1
公开(公告)日:2004-07-14
申请号:AU2003293871
申请日:2003-12-13
Applicant: BASF AG
Inventor: SOHN MARTIN , STROEFER ECKHARD , NEVEJANS FILIP , PENZEL ULRICH , PALLASCH HANS-JURGEN , LEUTHOLD RENE , BRODHAGEN ANDREAS , WOLFERT ANDREAS , MACKENROTH WOLFGANG , MAURER MARKUS
IPC: C07C263/10 , C07C265/14
Abstract: The invention relates to a process for preparing polyisocyanates by reacting organic amines with phosgene, wherein the reaction is carried out in at least three stages, with the first stage being carried out in a mixing apparatus, the second stage in at least one residence apparatus and the third stage in at least one separation apparatus and the pressure in each successive stage being lower than that in the previous stage.
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