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公开(公告)号：DE19533659A1
公开(公告)日：1997-03-13
申请号：DE19533659
申请日：1995-09-12
Applicant: BASF AG
Inventor： HAGEMEYER ALFRED DR , TRUEBENBACH PETER DR , RIEKER CHRISTOPHER WILLIAM DR , WUENSCH MARTIN DR , WATZENBERGER OTTO DR
IPC: B01J23/08 , B01J23/10 , B01J23/18 , B01J23/46 , B01J23/70 , B01J27/224 , B01J27/24 , B01J35/10 , B01J37/08 , C01B7/04 , B01J27/138 , B01J27/128
Abstract: The novel feature in Cl2 prodn. by alternatingly (a) loading a catalyst with HCl at 300-420 (pref. 360-410) degrees C and then (b) regenerating the catalyst with an O2-contg. gas at 370-460 (pref. 380-420) degrees C is that the catalyst is a sintered shape made of (by wt.): (i) 2-30% oxides and/or chlorides of Cu, Fe, Ru, Ce, Bi, Ni, Co, Ga and/or Nd; (ii) 0-30% Li-, Na-, K- and/or Zn-chloride; and (iii) 98-40% ceramic-, silicate- and/or glass-carrier. This catalyst is prepd. using inorganic metal powder and/or an active component, together with a specified polymer (mixt.) and a dispersant.
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公开(公告)号：AT340763T
公开(公告)日：2006-10-15
申请号：AT04026974
申请日：2004-11-12
Applicant: BASF AG
Inventor： UNGER GABRIELE DR , SCHOENFELDER HENDRIK DR , WATZENBERGER OTTO DR , STERZEL HANS-JOSEF DR , KUEHLING KLAUS DR
Abstract: Production of iron pentacarbonyl by reaction of iron with carbon monoxide in a suspension is catalyzed by a polysulfide. Production of iron pentacarbonyl by reaction of iron with carbon monoxide in a suspension is catalyzed by a polysulfide of formula (I) RSxR> (I) R and R> are organic residues; and x = 2-10.
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公开(公告)号：DE19733681A1
公开(公告)日：1999-02-11
申请号：DE19733681
申请日：1997-08-04
Applicant: BASF AG
Inventor： WATZENBERGER OTTO DR , MAUER PETER , STROEFER ECKHARD DR , SCHELLING HEINER , SCHNEIDER HANS-MICHAEL DR
IPC: C01B21/14
Abstract: The invention relates to a method for producing an aqueous solution of free hydroxylamine by treating a hydroxylammonium salt with ammonia in the counter-current in a stripping column. As a result, hydroxylamine is released and at the same time, the solution obtained is separated into an aqueous hydroxylamine solution and a salt fraction by distillation. The inventive method is simple and mild, and can be carried out on a large scale. The risk of decomposition is minimal due to the low thermal burden, the low concentration of hydroxylamine and the short residence time involved in the process.
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公开(公告)号：DE19725851A1
公开(公告)日：1998-12-24
申请号：DE19725851
申请日：1997-06-18
Applicant: BASF AG
Inventor： WATZENBERGER OTTO DR , SCHELLING HEINER , PFAB PETER DR , STROEFER ECKHARD DR
Abstract: The invention relates to a method for the production of highly pure aqueous solution from free hydroxylamine, wherein the diluted aqueous hydroxylamine solution is concentrated in a column, the vapor containing hydroxylamine is removed from the bottom of the column via a side-stream and highly pure hydroxylamine is obtained through condensation of the vapors. The inventive method is simple and mild, can be used in large-scale production and yields "electronic grade" hydroxylamine.
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公开(公告)号：DE502004001585D1
公开(公告)日：2006-11-09
申请号：DE502004001585
申请日：2004-11-12
Applicant: BASF AG
Inventor： UNGER GABRIELE DR , SCHOENFELDER HENDRIK DR , WATZENBERGER OTTO DR , STERZEL DR , KUEHLING KLAUS DR
Abstract: Production of iron penta carbonyl by reaction of iron with carbon monoxide in a suspension is catalyzed by a mixture of an alkali sulfide and sulfur.
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Patent Agency Ranking
公开(公告)号：ES2133869T3
公开(公告)日：1999-09-16
申请号：ES96114467
申请日：1996-09-10
Applicant: BASF AG
Inventor： HAGEMEYER ALFRED DR , TRUBENBACH PETER DR , RIEKER CHRISTOPHER WILLIAM , WUNSCH MARTIN DR , WATZENBERGER OTTO DR
IPC: B01J23/08 , B01J23/10 , B01J23/18 , B01J23/46 , B01J23/70 , B01J27/224 , B01J27/24 , B01J35/10 , B01J37/08 , C01B7/04
Abstract: The novel feature in Cl2 prodn. by alternatingly (a) loading a catalyst with HCl at 300-420 (pref. 360-410) degrees C and then (b) regenerating the catalyst with an O2-contg. gas at 370-460 (pref. 380-420) degrees C is that the catalyst is a sintered shape made of (by wt.): (i) 2-30% oxides and/or chlorides of Cu, Fe, Ru, Ce, Bi, Ni, Co, Ga and/or Nd; (ii) 0-30% Li-, Na-, K- and/or Zn-chloride; and (iii) 98-40% ceramic-, silicate- and/or glass-carrier. This catalyst is prepd. using inorganic metal powder and/or an active component, together with a specified polymer (mixt.) and a dispersant.
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公开(公告)号：DE59602232D1
公开(公告)日：1999-07-22
申请号：DE59602232
申请日：1996-09-10
Applicant: BASF AG
Inventor： HAGEMEYER ALFRED DR , TRUEBENBACH PETER DR , RIEKER CHRISTOPHER WILLIAM , WUENSCH MARTIN DR , WATZENBERGER OTTO DR
IPC: B01J23/08 , B01J23/10 , B01J23/18 , B01J23/46 , B01J23/70 , B01J27/224 , B01J27/24 , B01J35/10 , B01J37/08 , C01B7/04
Abstract: The novel feature in Cl2 prodn. by alternatingly (a) loading a catalyst with HCl at 300-420 (pref. 360-410) degrees C and then (b) regenerating the catalyst with an O2-contg. gas at 370-460 (pref. 380-420) degrees C is that the catalyst is a sintered shape made of (by wt.): (i) 2-30% oxides and/or chlorides of Cu, Fe, Ru, Ce, Bi, Ni, Co, Ga and/or Nd; (ii) 0-30% Li-, Na-, K- and/or Zn-chloride; and (iii) 98-40% ceramic-, silicate- and/or glass-carrier. This catalyst is prepd. using inorganic metal powder and/or an active component, together with a specified polymer (mixt.) and a dispersant.
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公开(公告)号：DE19545095A1
公开(公告)日：1997-06-05
申请号：DE19545095
申请日：1995-12-04
Applicant: BASF AG
Inventor： WATZENBERGER OTTO DR , HAGEMEYER ALFRED DR
Abstract: The invention relates to a process for the preparation of styrene by dehydrogenating a mixture of ethyl benzol and at least one xylol isomer in the gas phase in the presence of a regeneratable, oxygen-carrying, metallic-oxide catalyst (redox catalyst), with a reducible active ingredient preferably consisting of at least one metallic oxide from the group of oxides of the elements Bi, Ce, Co, Cr, Cu, Fe, In, Mn, Mo, Nb, Ni, Sb, Sn, Pb and V, the xylol being at least partially oxidised.
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公开(公告)号：DE4437252A1
公开(公告)日：1996-04-25
申请号：DE4437252
申请日：1994-10-18
Applicant: BASF AG
Inventor： HAGEMEYER ALFRED DR , WATZENBERGER OTTO DR , DEIMLING AXEL DR
IPC: B01J23/08 , B01J23/10 , B01J23/14 , B01J23/48 , B01J23/70 , B01J38/12 , C07B35/04 , C07B61/00 , C07C5/42 , C07C11/02 , C07C15/46 , B01J23/18 , B01J23/92 , B01J38/04 , C07C5/333
Abstract: Regenerative process for prodn. of olefinically unsatd. cpds. by an alternating and cyclically repeated oxidn. of selectively oxidisable hydrocarbons at a temp. Treact using an oxygen transfer catalyst (I) in the absence of molecular oxygen, with regeneration of the spent (I) with a gaseous molecular oxidising agent (II), whereby (i) before introducing the (II), the spent (reduced) catalyst (I) is cooled to a temp. Tregen which is also below the reaction temp. Treact whilst still in the presence of the reaction having a reducing action or under an inert gas; (ii) regeneration is carried out at the temp. Tregen by beginning the introduction of the (II) and continuing the addn. such that the highest temp. achieved during the regeneration remains lower than the reaction initiation temp. Treact.0 for the subsequent oxidn./dehydrogenation reaction; and (iii) after removing the oxidising medium, the regenerated catalyst is heated to the reaction initiation temp. Treact and only then is the oxidisable hydrocarbon starting material introduced. The catalyst is pref. at least one reducible metal oxide chosen from oxides of Bi, V, Ce, Fe, In, Ag, Cu, Co, Mn, Pb, Sn, Mo, W, As and/or Sb, opt. mounted on a carrier such as a transition metal oxide, esp. TiO2 or Cr2O3.
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公开(公告)号：AT340764T
公开(公告)日：2006-10-15
申请号：AT04026975
申请日：2004-11-12
Applicant: BASF AG
Inventor： UNGER GABRIELE DR , SCHOENFELDER HENDRIK DR , WATZENBERGER OTTO DR , STERZEL HANS-JOSEF DR , KUEHLING KLAUS DR
Abstract: Production of iron penta carbonyl by reaction of iron with carbon monoxide in a suspension is catalyzed by a mixture of an alkali sulfide and sulfur.
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