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    1.
    发明专利
    未知

    公开(公告)号：ES2135820T3

    公开(公告)日：1999-11-01

    申请号：ES96108372

    申请日：1996-05-25

    Applicant: DEGUSSA

    Inventor： TURK GUNTER DR ,  SCHMIDT GEROLD ,  SIRAY MUSTAFA DR ,  MEIER KARL

    IPC: C01B33/193 ,  H01M2/16

    Abstract: Precipitated silicic acid has a BET surface area of 100-130m /g (DIN 66131); a DBP absorption (water-free (DIN53601) ASTM D244 of plus or minus 275g/100g, a dry loss (2 hrs./105 degrees C) of 3.5-5.5 wt.% (DIN ISO787/11,ASTM D280, JISK5101/21), and a sieve residue with ALPINE air sieve of plus or minus 10;0 wt.% (

    METHOD FOR THE PRODUCTION OF PRECIPITATED SILICAS
    2.
    发明专利
    METHOD FOR THE PRODUCTION OF PRECIPITATED SILICAS 未知

    公开(公告)号：DE3263713D1

    公开(公告)日：1985-06-27

    申请号：DE3263713

    申请日：1982-02-26

    Applicant: DEGUSSA

    Inventor： NAUROTH PETER ,  KUHLMANN ROBERT ,  TURK GUNTER DR ,  BECKER ADAM

    IPC: C01B33/20 ,  A61K8/00 ,  A61K8/25 ,  A61Q11/00 ,  C01B33/187 ,  C01B33/193 ,  C01B37/02 ,  C08K3/00 ,  C08K3/34 ,  C08K3/36 ,  C08K7/18 ,  C08L7/00 ,  C08L21/00 ,  C09C1/30

    Abstract: Precipitated silicas which have the following physicochemical characteristics, depending on the manner in which they are milled: -Pendulum -roller mill Jet mill -BET m2/g 15-110 15-110 -surface -area -Tamped g/l 150-750 90-650 -den- -sity -Cu abrasion in 10% mg 5-30 5-30 -strength glycerol -dispersion -Lightness % 86-96 90-96 -value -A -Particle size dis- as in FIG. 1 as in FIG. 2 -tribution curve -determined by a -Coulter Counter -"ALPINE screen retain- % by 63 mu m weight -Viscosity of a 30% mPa.s 30,000 to 60,000 -strength dispersion in -a 1:1 glycerol/water -mixture (Brookfield -RTV, Sp5) - are prepared by diluting a precipitated silica original suspension obtained according to German Published Application DAS 1,467,019 and simultaneously adding alkali metal silicate solution, sulfuric acid and water while keeping the pH constant between 7 and 9. The precipitated silica is then filtered off, washed, dried and milled using a pendulum roller mill or a jet mill. Because of their abrasiveness, the precipitated silicas can be employed as cleansing and abrasive agents and, in the case of the jet-milled product, also as a polishing agent, abrasive and thickener in toothpastes.

    5.
    发明专利
    未知

    公开(公告)号：ID17208A

    公开(公告)日：1997-12-11

    申请号：ID962111

    申请日：1996-07-25

    Applicant: DEGUSSA

    Inventor： TURK GUNTER DR ,  SCHMIDT GEROLD ,  SIRAY MUSTAFA DR ,  MEIER KARL

    IPC: C01B33/193 ,  H01M2/16 ,  H01M14/00 ,  C01B33/12

    Abstract: Precipitated silicic acid has a BET surface area of 100-130m /g (DIN 66131); a DBP absorption (water-free (DIN53601) ASTM D244 of plus or minus 275g/100g, a dry loss (2 hrs./105 degrees C) of 3.5-5.5 wt.% (DIN ISO787/11,ASTM D280, JISK5101/21), and a sieve residue with ALPINE air sieve of plus or minus 10;0 wt.% (

    7.
    发明专利
    未知

    公开(公告)号：DE3274796D1

    公开(公告)日：1987-02-05

    申请号：DE3274796

    申请日：1982-02-26

    Applicant: DEGUSSA

    Inventor： MULLER KARL-HANS DR ,  NEUMULLER MATTHIAS ,  TURK GUNTER DR

    IPC: A61K8/00 ,  A61K8/25 ,  A61K8/86 ,  A61Q11/00 ,  A61K7/16

    Abstract: A dental-care composition having improved shelf life in respect of rheology and abrasiveness, which as a novel feature, contains, as a cleansing agent, a bifunctional (thickening and abrasive) precipitated silica characterized by the following physico-chemical properties: -Pendulum - roller - mill Jet mill -BET surface area m2/g 15-110 15-110 -Tamped density g/l 150-750 90-650 -Secondary particle size FIG. 1 FIG. 2 -distribution according to -Coulter Counter -"ALPINE" screen % by 63 mu m weight -Cu abrasion in 10% mg 5-30 5-30 -strength glycerol disper- -sion -Lightness value A % 86-96 90-96 -Viscosity in a 30% 30,000-60,000 30,000-60,000 -strength dispersion in a -1:1 glycerol/water -mixture, Brookfield RTV, -Sp5 - The dental-care composition may additionally contain 0.5-5% by weight of polyethylene glycol or 2-14% by weight of a precipitated silica which in 15% strength dispersion in a glycerol/water mixture has a viscosity of not less than 30,000 mPa.s. Pyrogenic silica can also be employed successfully to regulate the viscosity of the product.

    PRECIPITATED SILICA HAVING A HIGH STRUCTURE AND PROCESS FOR PRODUCING IT
    8.
    发明专利
    PRECIPITATED SILICA HAVING A HIGH STRUCTURE AND PROCESS FOR PRODUCING IT 未知

    公开(公告)号：DE3270779D1

    公开(公告)日：1986-05-28

    申请号：DE3270779

    申请日：1982-09-25

    Applicant: DEGUSSA

    Inventor： NAUROTH PETER ,  ESCH HEINZ ,  TURK GUNTER DR

    IPC: C01B33/18 ,  C01B33/12 ,  C01B33/158 ,  C01B33/187 ,  C01B33/193 ,  C01B33/20 ,  C01B37/02 ,  C04B30/00 ,  C08K3/00 ,  C08K3/34 ,  C08K3/36 ,  C08K5/00 ,  C08K5/36 ,  C08L7/00 ,  C08L23/00 ,  C08L101/00

    Abstract: There are disclosed precipitated silicas which are characterized by the following physical-chemical data: -A B C -BET-surface area m2/g 400-600 400-600 400-600 -according to DIN 66131 -DBP-Number % 340-380 320-360 310-360 -Bulk density according g/l 180-220 75-120 35-70 -to DIN 53194 -"ALPINE-Sieve Wt. % 25-60 63 m mu - Depending on the particle distribution curve, these precipitated silicas can be employed as silica carriers for active materials of all types, as antiblocking agents for polypropylene and polyethylene films, as thickening silica in specific polar systems in which pyrogenic silicas show little thickening capacity, as highly active matting agents for varnishes and as catalyst carriers as well as insulating materials. The precipitated silicas are produced by establishing a silica final concentration of 46 grams/l in a receiver having water present heated to a temperature of 40 DEG -42 DEG C. while holding the pH constant in the range of 6-7 by simultaneously running in a water glass solution and sulfuric acid while maintaining shearing with an Ekato Turbine over the entire precipitation time, interrupting the precipitation for 90 minutes from the 13th to 103rd minute according to a total precipitation of 146 minutes, aging the suspension of precipitated silica for 12-17 hours, separating the precipitated silica from the suspension with the help of a filter press, washing, liquifying the filter cake with water and/or acid to a suspension having 10-16 weight % solids, finally spray drying and either not grinding or grinding with a cross flow mill or jet mill.

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