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    Process for preparing isomers of alpha-bis-oximes
    92.
    发明专利
    Process for preparing isomers of alpha-bis-oximes 未知

    公开(公告)号：CZ288053B6

    公开(公告)日：2001-04-11

    申请号：CZ315597

    申请日：1996-03-25

    Applicant: BASF AG

    Inventor： MUELLER RUTH DR ,  BENOIT REMY DR ,  BAYER HERBERT DR ,  GOETZ NORBERT DR ,  SAUTER HUBERT DR

    IPC: C07D231/12 ,  C07B61/00 ,  C07C249/04 ,  C07C249/12 ,  C07C249/14 ,  C07C251/38 ,  C07C251/48 ,  C07C255/62 ,  C07D261/08

    Abstract: In the present invention there is disclosed a process for preparing of alpha-bis-oxime isomers of the general formula Ia: Re1O-N=CRe2-CRe3=N-ORe4 (Ia), wherein the groups Re1O- and Re2 on the N=C bond are in mutual position cis and wherein Re1 represents alkyl containing 1 to 6 carbon atoms, alkenyl containing 3 to 6 carbon atoms and alkynyl having 3 to 6 carbon atoms, Re2 represents an optionally substituted phenyl or an optionally substituted hetaryl, Re3 represents a hydrogen atom, a cyano group, a halogen atom, alkyl containing 1 to 4 carbon atoms, haloalkyl containing 1 to 4 carbon atoms and cycloalkyl having 3 to 6 carbon atoms and Re4 represents hydrogen. The proposed preparation process is characterized in that {alpha}-bis-oxime isomer of the general formula Ib: Re1O-N=CRe2-CRe3=N-ORe4 (Ib), wherein the groups Re1O- and Re2 on the N=C bond are in mutual position trans and wherein Re1, Re2, Re3 and Re4 are as specified above, optionally in a mixture with the {alpha}-bis-oxime isomer of the general formula Ia: Re1O-N=CRe2-CRe3=N-ORe4 (Ia) is treated in an aromatic hydrocarbon with a Lewis acid.

    93.
    发明专利
    未知

    公开(公告)号：DE19710760A1

    公开(公告)日：1998-09-17

    申请号：DE19710760

    申请日：1997-03-14

    Applicant: BASF AG

    Inventor： WAGNER OLIVER DR ,  BAYER HERBERT DR ,  MISLITZ ULF DR ,  SCHIRMER ULRICH DR ,  AMMERMANN EBERHARD DR ,  LORENZ GISELA DR ,  STRATHMANN SIEGFRIED DR

    IPC: A01N37/50 ,  A01N43/54 ,  A01N47/24 ,  A01N47/34 ,  A01N37/10 ,  A01N43/50 ,  A01N43/76 ,  A01N43/78 ,  A01N43/82

    Abstract: The invention relates to a fungicide mixture with synergistic effect, containing a) a fungicide active compound of formula IA or IB wherein - - - represents a single or double bond and the index and substituents have the following meanings: R' -C[CO2CH3] =CHOCH3, -C[CO2CH3] =NOCH3, -C[CONHCH3] =NOCH3, -C[CO2CH3] =CHCH3, -C[CO2CH3] =CHCH2CH3, -C[COCH3] =NOCH3, -C[COCH2CH3] =NOCH3, -N(OCH3) -CO2CH3, -N(CH3) -CO2CH3, -N(CH2CH3) -CO2CH3; R'' a C-organic radical which is bonded directly or via an oxy-, mercapto-, amino- or alkylamino group; together with a group X and the ring Q or T to which they are bonded, an optionally substituted bicyclic, partially or completely unsaturated system; R -OC[CO2CH3] =CHOCH3, -OC[CO2CH3] =CHCH3, -OC[CO2CH3] =CHCH2CH3, -SC[CO2CH3] =CHOCH3, -SC[CO2CH3] =CHCH3, -SC[CO2CH3] =CHCH2CH3, -N(CH3)C[CO2CH3] =CHOCH3, -N(CH3)C[CO2CH3] =NOCH3, -CH2C[CO2CH3] =CHOCH3, -CH2C[CO2CH3] =NOCH3, -CH2C[CONHCH3] =NOCH3; R oxygen, sulfur, =CH- or =N-; n 0, 1, 2 or 3; X cyano, nitro, halogen, alkyl, halogenalkyl, alkoxy, halogenalkoxy, alkylthio; if n>1, an optionally substituted alkylene, alkenylene, oxyalkylene, oxyalkylenoxy, oxyalkenylene, oxyalkenylenoxy or butadiendiyl group bonded to two adjoining C-atoms of the phenyl ring; Y C- or -N-; Q cyclopentenyl, cyclohexenyl, phenyl, pyrrolyl, thienyl, furyl, pyrazolyl, imidazolyl, oxazolyl, isoxazolyl, thiazolyl, thiadiazolyl, triazolyl, pyridinyl, 2-pyridonyl, pyrimidinyl and triazinyl; T phenyl, oxazolyl, thiazolyl, thiadiazolyl, oxadiazolyl, pyridinyl, pyrimidinyl and triazinyl, and b) the herbicide active agent II and/or b2) the herbicide active agent III. The invention also relates to methods for producing mixtures of that type and the use of such mixtures for combatting harmful fungi in the area of plant and material protection.

    100.
    发明专利
    未知

    公开(公告)号：DE59502205D1

    公开(公告)日：1998-06-25

    申请号：DE59502205

    申请日：1995-03-17

    Applicant: BASF AG

    Inventor： KIRSTGEN REINHARD DR ,  OBERDORF KLAUS DR ,  SAUTER HUBERT DR ,  BAYER HERBERT DR ,  GRAMMENOS WASSILIOS DR ,  RANG HARALD DR ,  HARRIES VOLKER DR ,  LORENZ GISELA DR ,  AMMERMANN EBERHARD DR

    IPC: A01N37/38 ,  A01N37/50 ,  A01N37/52 ,  C07C251/48 ,  C07C251/50 ,  C07C255/62 ,  C07C255/64 ,  C07C259/02 ,  C07C259/10 ,  C07C259/18 ,  C07C323/47 ,  C07C327/58 ,  C07D317/18 ,  C07D333/28 ,  C07D521/00

    Abstract: Oximino-substd benzyloxybenzene derivs of formula (I) are new. Ra = a gp. of formula (i); X = CHOMe, CH-Me or N-OMe; R1 = 1-6C alkyl (opt substd by halo, 1-4C alkoxy, CN, 1-6C alkoxycarbonyl, aryl, aryloxy or heteroaryl); 2-6C alkenyl; 3-6C alkynyl or haloalkenyl; 3-6C cycloalkyl; 3-6C cycloalkyl(1-4C)alkyl; aryl(3-6C)alkenyl; satd or unsatd 4-6 membered heterocyclyl or heterocyclyl(1-4C)alkyl where the heterocyclic rings includes 1 or 2 ring members selected from one O or S and one or two N and one or two NMe gps.; and carbocyclic or heterocyclic rings are opt substd by 1 or more halo, 1-4C alkyl or alkoxy, 1-2C haloalkyl or haloalkoxy, 3-6C cycloalkyl, aryl or aryloxy; R2 and R3 = H, halo, CN, NO2, 1-4C alkyl or alkoxy, 1-2C haloalkyl or haloalkoxy, or if on adjacent C atoms are together oxy(m)ethylideneoxy (opt substd on each C by 1 or 2 halo and/or Me); R4 = CN, Cl, Br, 1-6C alkoxy or alkylthio, 1-4C haloalkoxy, 1-4C alkoxy(1-4C)alkoxy, 3-6C cycloalkyl(1-2C)alkoxy, mon o or di(1-6C)alkylamino, 3-6C alkenyloxy or alkynyloxy, aryloxy or arylthio (aromatic rings opt substd by 1-3 of 1-4C(halo)alkyl, (halo)alkoxy or alkylthio, and additionally by halo atoms to a total no of 4 or 5 substits); R5 = NO2, CN, halo, 1-4C(halo)alkyl, (halo)alkoxy or alkylthio, phenyl or phenoxy (opt substd as aromatic rings in R4); or 2 R5 on adjacent C form a 1,3-butadiene-1,4-diyl gp. (i.e. a fused benzene ring), opt. substd by 1 or 2 halo, and opt. also by 1 or 2 of NO2, CN, halo, 1-4C haloalkyl, (halo)alkoxy or alkylthio; n = 0-4 (R5 same or different if n = 2 or more); Y = O, NH or NMe; R6 = H or 1-4C alkyl. Also new are intermediates of formulae (XI') and (IVb'). Y' = NH or NMe; R2 and R3 are above except that in (X1') they do not represent alkylenedioxy; in (IVb') Y is limited to Y'.

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