113.
    发明专利
    未知

    公开(公告)号:ID24217A

    公开(公告)日:2000-07-13

    申请号:ID20000978

    申请日:1998-11-24

    Applicant: BASF AG

    Abstract: A process for continuous extraction of polyamide particles in an essentially vertical extraction column using an aqueous extractant comprises using an extraction column that is divided into two zones and performing an extraction with a recirculating 15-40% strength by weight aqueous epsi-caprolactam solution in the first zone and then with countercurrent water at a from 5 to 40° C. lower temperature in the second zone. The process provides for economical extraction of polyamides with a low level of monomers and oligomers.

    114.
    发明专利
    未知

    公开(公告)号:BR9711257A

    公开(公告)日:1999-08-17

    申请号:BR9711257

    申请日:1997-08-26

    Applicant: BASF AG

    Abstract: A process for preparing a polyamide by reacting at least one aminonitrile with water comprises:(1) reacting at least one aminonitrile with water at a temperature from 100 to 360° C. and a pressure from 0.1 to 35x106 Pa to obtain a reaction mixture,(2) further reacting the reaction mixture at a temperature from 150 to 400° C. and a pressure which is lower than the pressure in step 1, the temperature and the pressure being selected so as to obtain a first gas phase and a first liquid or a first solid phase or a mixture of first solid and first liquid phase, and the first gas phase is separated from the first liquid or the first solid phase or from the mixture of first liquid and first solid phase, and(3) admixing the first liquid or the first solid phase or the mixture of first liquid and first solid phase with a gaseous or liquid phase comprising water at a temperature from 150 to 360° C. and a pressure from 0.1 to 30x106 Pa to obtain a product mixture.

    115.
    发明专利
    未知

    公开(公告)号:AT179195T

    公开(公告)日:1999-05-15

    申请号:AT95927741

    申请日:1995-07-28

    Applicant: BASF AG

    Abstract: PCT No. PCT/EP95/03003 Sec. 371 Date Feb. 12, 1997 Sec. 102(e) Date Feb. 12, 1997 PCT Filed Jul. 28, 1995 PCT Pub. No. WO96/05241 PCT Pub. Date Feb. 22, 1996A process for preparing polyaspartic acid by polycondensation of fine-particle aspartic acid at temperatures above 150 DEG C. in the presence of acidic catalysts, wherein first contact between the acidic catalysts and the fine-particle aspartic acid takes place in the reaction zone where the polycondensation takes place.

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