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    124.
    发明专利
    未知

    公开(公告)号：ES2137510T3

    公开(公告)日：1999-12-16

    申请号：ES95917966

    申请日：1995-04-26

    Applicant: BASF AG

    Inventor： RANG HARALD ,  GOTZ NORBERT ,  HARREUS ALBRECHT ,  BORCHERS DIRK ,  HARTMANN HORST ,  MAYWALD VOLKER

    IPC: B01J23/02 ,  B01J31/02 ,  C07B61/00 ,  C07C239/20 ,  C07C249/12 ,  C07C251/54 ,  C07C309/66

    Abstract: PCT No. PCT/EP95/01581 Sec. 371 Date Nov. 4, 1996 Sec. 102(e) Date Nov. 4, 1996 PCT Filed Apr. 26, 1995 PCT Pub. No. WO95/30648 PCT Pub. Date Nov. 16, 1995Preparation of mixtures of O-phenoxyalkylhydroxylamines Ia and Ib (Ia): H2NOCH2CH(R1)OAr (Ib): H2NOCH(R1)CH2OAr and the corresponding salt mixtures by a) converting mixtures of isomers of O-(2-hydroxyethyl)oximes IIa and IIb (IIa): (III): into a mixture of sulfonates IVa and IVb (IVa): (IVb): b) reacting this mixture of IVa and IVb with a phenol HO-Ar (V) to give a mixture of O-phenoxyalkoximes VIa and VIb (VIa): (VIb): c) hydrolyzing this mixture in the presence of an acid and, if desired d) liberating the O-phenoxyalkylhydroxylamines Ia and Ib from the resulting salts using a mineral acid. Compounds Ia/Ib and VIa/VIb are important intermediates for crop protection agents.

    125.
    发明专利
    未知

    公开(公告)号：DE59507102D1

    公开(公告)日：1999-11-25

    申请号：DE59507102

    申请日：1995-04-26

    Applicant: BASF AG

    Inventor： RANG HARALD ,  GOETZ NORBERT ,  HARREUS ALBRECHT ,  BORCHERS DIRK ,  HARTMANN HORST ,  MAYWALD VOLKER ,  HEIMANN FRANK ,  BUSCHULTE THOMAS

    IPC: B01J23/02 ,  B01J31/02 ,  C07B61/00 ,  C07C239/20 ,  C07C249/12 ,  C07C251/54 ,  C07C309/66

    Abstract: PCT No. PCT/EP95/01581 Sec. 371 Date Nov. 4, 1996 Sec. 102(e) Date Nov. 4, 1996 PCT Filed Apr. 26, 1995 PCT Pub. No. WO95/30648 PCT Pub. Date Nov. 16, 1995Preparation of mixtures of O-phenoxyalkylhydroxylamines Ia and Ib (Ia): H2NOCH2CH(R1)OAr (Ib): H2NOCH(R1)CH2OAr and the corresponding salt mixtures by a) converting mixtures of isomers of O-(2-hydroxyethyl)oximes IIa and IIb (IIa): (III): into a mixture of sulfonates IVa and IVb (IVa): (IVb): b) reacting this mixture of IVa and IVb with a phenol HO-Ar (V) to give a mixture of O-phenoxyalkoximes VIa and VIb (VIa): (VIb): c) hydrolyzing this mixture in the presence of an acid and, if desired d) liberating the O-phenoxyalkylhydroxylamines Ia and Ib from the resulting salts using a mineral acid. Compounds Ia/Ib and VIa/VIb are important intermediates for crop protection agents.

    126.
    发明专利
    未知

    公开(公告)号：AT178322T

    公开(公告)日：1999-04-15

    申请号：AT93911471

    申请日：1993-04-16

    Applicant: BASF AG

    Inventor： MAYWALD VOLKER ,  KUEKENHOEHNER THOMAS ,  MUENSTER PETER ,  VON DEYN WOLFGANG ,  WALTER HELMUT ,  GERBER MATTHIAS ,  WESTPHALEN KARL-OTTO ,  KARDORFF UWE

    IPC: A01N43/80 ,  C07D261/18 ,  C07D413/12

    Abstract: PCT No. PCT/EP93/00918 Sec. 371 Date Sep. 29, 1994 Sec. 102(e) Date Sep. 29, 1994 PCT Filed Apr. 16, 1994 PCT Pub. No. WO93/22295 PCT Pub. Date Nov. 11, 1993The invention pertains to isoxazolecarboxamides of the formula I I where R1 is alkyl, cycloalkyl, alkoxyalkyl, alkenyl, alkynyl, phenyl or unsubstituted or substituted benzyl, R2 is hydrogen or alkyl and R3 is alkyl, cycloalkyl, alkenyl, alkynyl, phenyl or unsubstituted or substituted benzyl, and the plant-tolerated salts of those compounds in which R2 is hydrogen, their preparation and their use.

    PROCESS FOR PREPARING HYDROXYLAMINE-ETHERS AND THEIR SALTS AND THEIR INTERMEDIATES
    127.
    发明专利
    PROCESS FOR PREPARING HYDROXYLAMINE-ETHERS AND THEIR SALTS AND THEIR INTERMEDIATES 未知

    公开(公告)号：HU215116B

    公开(公告)日：1998-09-28

    申请号：HU9501904

    申请日：1993-12-17

    Applicant: BASF AG

    Inventor： GOETZ NORBERT ,  HARREUS ALBRECHT ,  KLEIN ULRICH ,  MAYWALD VOLKER ,  MISSLITZ ULF ,  RANG HARALD

    IPC: C07C239/20 ,  C07C251/54 ,  C07C253/30 ,  C07C255/54 ,  C07C259/06

    Abstract: PCT No. PCT/EP93/03597 Sec. 371 Date Jun. 6, 1995 Sec. 102(e) Date Jun. 6, 1995 PCT Filed Dec. 17, 1993 PCT Pub. No. WO94/14757 PCT Pub. Date Jul. 7, 1994Hydroxylamine ethers I I (where X is NO2, CN, halogen, alkyl or haloalkyl, Y is H, NO2, CN, halogen, alkyl or haloalkyl, n is 0-2 or 1-4 where Y and all radicals X are halogen and Alk is unsubstituted or substituted alkylene) and their salts with mineral acids or strong organic acids are prepared by reacting either a hydroximino compound II II (where R1 is alkyl, R2 is alkyl or alkoxy or R1+R2 form an alkylene chain) in the presence of an alkali metal hydroxide, alkali metal alcoholate, alkali metal bicarbonate or alkali metal carbonate as the base, or the corresponding anion II directly, with an alkylating agent III III (where R3 is unsubstituted or substituted alkyl or unsubstituted or substituted phenyl) to give an oximino derivative IV IV said derivative is cleaved by means of a mineral acid or a strong organic acid to give the salt of I and, if desired, the latter is converted by means of a base into the free compound I. The hydroxylamine ethers I are intermediates for crop protection agents and drugs.

    PROCESS FOR THE PREPARATION OF MIXTURES OF ISOMERS OF O-PHENOXYALKYLHYDROXYLAMINES OR O-PHENOXYALKYLOXIMES
    128.
    发明专利
    PROCESS FOR THE PREPARATION OF MIXTURES OF ISOMERS OF O-PHENOXYALKYLHYDROXYLAMINES OR O-PHENOXYALKYLOXIMES 未知

    公开(公告)号：CA2189584A1

    公开(公告)日：1995-11-16

    申请号：CA2189584

    申请日：1995-04-26

    Applicant: BASF AG

    Inventor： RANG HARALD ,  GOETZ NORBERT ,  HARREUS ALBRECHT ,  BORCHERS DIRK ,  HARTMANN HORST ,  MAYWALD VOLKER ,  HEIMANN FRANK ,  BUSCHULTE THOMAS

    IPC: B01J23/02 ,  B01J31/02 ,  C07B61/00 ,  C07C239/20 ,  C07C249/12 ,  C07C251/54 ,  C07C309/66 ,  C07C253/30 ,  C07C255/54

    Abstract: A process is disclosed for producing isomer mixtures from Ophenoxyalkylhydroxyl amines Ia: H2N-O-CH2-CH(R1)-O-Ar and Ib: H2N-O-CH(R1)-CH2-O-Ar (wherein R1 represents alkyl, Ar where appropriate a substituted phenyl) and the corresponding salt mixtures. This process involves the following steps: (a) an isomer mixture of O-(2-hydroxyethyl)-oximes (IIa) and (IIb) (in which R2 is an alkyl and R3 is an alkyl or alkoxy, or R2 and R3 together with the common C atom form a 5-7 member ring) is converted by reaction with a sulphonyl halogenide of formula (III): Hal-SO2-R4 (wherein R4 represents an organic group and Hal is a halogen) in the presence of a base to form the corresponding sulphonate mixture of (IVa) and (IVb); (b) this sulphonate mixture is reacted in the presence of a base with a phenol of formula (V): HOAr to produce a mixture of O-phenoxyalkyloximes of general formulae (VIa) and (VIb); (c) the mixture is hydrolysed in the presence of an acid and, if required, (d) the O-phenoxyalkylhydroxyl amines (Ia) and (Ib) are released from the resulting salts using a mineral base. The O-phenoxyalkylhydroxyl amines (Ia/Ib) and their precursors (VIa/VIb) are important intermediate products for plant protective agents and drugs.

    129.
    发明专利
    未知

    公开(公告)号：BR9307802A

    公开(公告)日：1995-11-14

    申请号：BR9307802

    申请日：1993-12-17

    Applicant: BASF AG

    Inventor： HARREUS ALBRECHT ,  GOETZ NORBERT ,  MAYWALD VOLKER ,  RANG HARALD ,  MISSLITZ ULF ,  KLEIN ULRICH

    IPC: C07C239/20 ,  C07C251/54 ,  C07C253/30 ,  C07C255/54 ,  C07C259/06

    Abstract: PCT No. PCT/EP93/03597 Sec. 371 Date Jun. 6, 1995 Sec. 102(e) Date Jun. 6, 1995 PCT Filed Dec. 17, 1993 PCT Pub. No. WO94/14757 PCT Pub. Date Jul. 7, 1994Hydroxylamine ethers I I (where X is NO2, CN, halogen, alkyl or haloalkyl, Y is H, NO2, CN, halogen, alkyl or haloalkyl, n is 0-2 or 1-4 where Y and all radicals X are halogen and Alk is unsubstituted or substituted alkylene) and their salts with mineral acids or strong organic acids are prepared by reacting either a hydroximino compound II II (where R1 is alkyl, R2 is alkyl or alkoxy or R1+R2 form an alkylene chain) in the presence of an alkali metal hydroxide, alkali metal alcoholate, alkali metal bicarbonate or alkali metal carbonate as the base, or the corresponding anion II directly, with an alkylating agent III III (where R3 is unsubstituted or substituted alkyl or unsubstituted or substituted phenyl) to give an oximino derivative IV IV said derivative is cleaved by means of a mineral acid or a strong organic acid to give the salt of I and, if desired, the latter is converted by means of a base into the free compound I. The hydroxylamine ethers I are intermediates for crop protection agents and drugs.

    PROCESS AND INTERMEDIATE PRODUCTS FOR PREPARING HYDROXYLAMINE-ETHERS AND THEIR SALTS
    130.
    发明专利
    PROCESS AND INTERMEDIATE PRODUCTS FOR PREPARING HYDROXYLAMINE-ETHERS AND THEIR SALTS 未知

    公开(公告)号：HU9501904D0

    公开(公告)日：1995-08-28

    申请号：HU9501904

    申请日：1993-12-17

    Applicant: BASF AG

    Inventor： GOETZ NORBERT ,  HARREUS ALBRECHT ,  MAYWALD VOLKER ,  KLEIN ULRICH ,  MISSLITZ ULF ,  RANG HARALD

    IPC: C07C239/20 ,  C07C251/54 ,  C07C253/30 ,  C07C255/54 ,  C07C259/06

    Abstract: PCT No. PCT/EP93/03597 Sec. 371 Date Jun. 6, 1995 Sec. 102(e) Date Jun. 6, 1995 PCT Filed Dec. 17, 1993 PCT Pub. No. WO94/14757 PCT Pub. Date Jul. 7, 1994Hydroxylamine ethers I I (where X is NO2, CN, halogen, alkyl or haloalkyl, Y is H, NO2, CN, halogen, alkyl or haloalkyl, n is 0-2 or 1-4 where Y and all radicals X are halogen and Alk is unsubstituted or substituted alkylene) and their salts with mineral acids or strong organic acids are prepared by reacting either a hydroximino compound II II (where R1 is alkyl, R2 is alkyl or alkoxy or R1+R2 form an alkylene chain) in the presence of an alkali metal hydroxide, alkali metal alcoholate, alkali metal bicarbonate or alkali metal carbonate as the base, or the corresponding anion II directly, with an alkylating agent III III (where R3 is unsubstituted or substituted alkyl or unsubstituted or substituted phenyl) to give an oximino derivative IV IV said derivative is cleaved by means of a mineral acid or a strong organic acid to give the salt of I and, if desired, the latter is converted by means of a base into the free compound I. The hydroxylamine ethers I are intermediates for crop protection agents and drugs.

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