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    폴리아미드섬유 염색용 반응성 염료 및 이의 제조방법
    11.
    发明授权
    폴리아미드섬유 염색용 반응성 염료 및 이의 제조방법 有权
    聚酰胺纤维的反应性及其制备方法

    公开(公告)号：KR100830421B1

    公开(公告)日：2008-05-22

    申请号：KR1020070023459

    申请日：2007-03-09

    Applicant: 주식회사 오영 ,  한국화학연구원

    Inventor： 김진수 ,  김태경 ,  박희문 ,  오세화 ,  허선희

    IPC: C09B62/002 ,  C09B62/006

    CPC classification number: C09B62/0025 ,  C09B62/004 ,  C09B62/006 ,  D06P3/248

    Abstract: A novel reactive dye for dyeing polyamide fiber, and a method for preparing the reactive dye are provided to improve the purity of a dye by lowering water solubility and to enhance fixation, dyeing uniformity and washing fastness. A reactive dye is represented by the formula I, wherein A1 and A2 are independently H, a methyl A reactive dye, a methoxy group, Br, Cl, a cyano group, a nitro group, a hydroxysulfonyl group, a C1-C2 alkyl sulfonyl group or a vinyl sulfonyl group; L is an amino group or an azo group; and D is a dye mother material represented by the formula VIII, IX or X. In the formula VIII, R1 is H, a C1-C2 alkyl group, an acetyl group, a benzyl group or a benzoyl group; and M is H or an alkali metal. In the formula IX, R3 is a methyl group or a hydroxycarbonyl group; X1 and X2 is H or Cl; and M is H or an alkali metal.

    Abstract translation: 提供用于染色聚酰胺纤维的新型活性染料和制备活性染料的方法，以通过降低水溶性并提高固色，染色均匀性和耐洗牢度来提高染料的纯度。 活性染料由式I表示，其中A1和A2独立地为H，甲基A活性染料，甲氧基，Br，Cl，氰基，硝基，羟基磺酰基，C1-C2烷基磺酰基 基团或乙烯基磺酰基; L是氨基或偶氮基; D是由式VIII，IX或X表示的染料母体材料。在式Ⅷ中，R 1是H，C 1 -C 2烷基，乙酰基，苄基或苯甲酰基; M为H或碱金属。 在式IX中，R 3是甲基或羟基羰基; X1和X2是H或Cl; M为H或碱金属。

    벤조티아졸계 분산 반응성 염료 및 이의 제조방법
    12.
    发明授权
    벤조티아졸계 분산 반응성 염료 및 이의 제조방법 失效
    벤조티아졸계분산반응성염료및이의제조방법

    公开(公告)号：KR100385300B1

    公开(公告)日：2003-05-23

    申请号：KR1020010003009

    申请日：2001-01-18

    Applicant: 한국화학연구원

    Inventor： 오세화 ,  신승림 ,  전근 ,  박희문 ,  박수열 ,  윤성령

    IPC: C09B29/045

    Abstract: PURPOSE: Provided is benzothiazole-based dispersion-reactive dye, which reduces pollution, dose not contain hazardous amine and metals, can be used in acidic and neutral condition, and is excellent in washing-fastness and properties. CONSTITUTION: The benzothiazole-based dispersion-reactive dye represented by the formula 1 is produced by a process comprising the steps of: diazotizing 2-amino-5-(beta-acetoxy ethyl sulfone)benzothiazole or 2-amino-5-(beta-hydroxy ethyl sulfone)benzothiazole; preparing a coupling solution by dissolving a coupler in an acid mixture; mixing the diazotized 2-amino-5-(beta-acetoxy ethyl sulfone)benzothiazole and the coupling solution at 5-10deg.C and adding a base and separating the produced dye or mixing the diazotized 2-amino-5-(beta-hydroxy ethyl sulfone)benzothiazole and the coupling solution at 5-10deg.C and stirring at 80-90deg.C by using acetic anhydride. In the formula, R, R1, R2, and R3 are identically or differently hydrogen, alkyl, alkoxy, cyanoalkyl, or amino acetyl.

    Abstract translation: 用途：本发明提供了一种苯并噻唑类分散体 - 活性染料，它可以减少污染，不含有害胺和金属，可在酸性和中性条件下使用，并具有优异的耐洗牢度和性能。 构成：由式1表示的苯并噻唑基分散体 - 活性染料通过包括以下步骤的方法制备：将2-氨基-5-（β-乙酰氧基乙基砜）苯并噻唑或2-氨基-5-（β- 羟基乙基砜）苯并噻唑; 通过将成色剂溶解在酸混合物中制备偶联溶液; 在5-10℃将重氮化的2-氨基-5-（β-乙酰氧基乙基砜）苯并噻唑和偶联溶液混合并加入碱并分离产生的染料或将重氮化的2-氨基-5-（β-羟基 乙基砜）苯并噻唑和偶合溶液在5-10℃，并在80-90℃下用乙酸酐搅拌。 在该式中，R，R1，R2和R3相同或不同地为氢，烷基，烷氧基，氰基烷基或氨基乙酰基。

    염모제 조성물 및 그 제조방법
    14.
    发明公开
    염모제 조성물 및 그 제조방법 有权
    毛发的组成及其制造方法

    公开(公告)号：KR1020080061335A

    公开(公告)日：2008-07-02

    申请号：KR1020080017278

    申请日：2008-02-26

    Applicant: 광주과학기술원 ,  한국화학연구원

    Inventor： 김진수 ,  오세화 ,  허선희 ,  김태경 ,  박희문

    IPC: A61K8/44 ,  A61K8/46 ,  A61Q5/10

    CPC classification number: A61K8/466 ,  A61K8/411 ,  A61K2800/4324 ,  A61Q5/10

    Abstract: A composition comprising hair dye is provided to reduce skin irritation and hair damage after dyeing by using no harmful aromatic amine, improve convenience of use as compared with the conventional permanent hair coloring products, and enhance washability and coloring ability. A hair dyeing composition comprises 1-10 wt.% of thickening agent, 1-20 wt.% of penetrant, 0.01-5 wt.% of reactive dye having a vinylsulfone group, represented by the formula(2) in which M is an alkali metal ion such as H, Li, Na or K, and a remaining amount of water, and further comprises 1-5 wt.% of a pH regulating agent or a reducing agent for reducing a -S-S bond, wherein under acidic condition, the reactive group of dye forms a covalent bond with a reactive group of hair keratin, thereby coloring the hair keratin.

    Abstract translation: 提供一种包含染发剂的组合物，通过使用无有害芳香胺，可以减轻染色后的皮肤刺激和毛发损伤，提高使用方便性，与常规的永久性着色产品相比，提高了洗涤性和着色能力。 染发组合物包含1-10重量％的增稠剂，1-20重量％的渗透剂，0.01-5重量％的具有乙烯基砜基的活性染料，由式（2）表示，其中M是 碱金属离子如H，Li，Na或K和剩余量的水，还包含1-5重量％的pH调节剂或还原-SS键的还原剂，其中在酸性条件下， 染料的反应性基团与毛发角蛋白的反应性基团形成共价键，从而着色头发角蛋白。

    염모제 조성물 및 그 제조방법
    15.
    发明公开
    염모제 조성물 및 그 제조방법 有权
    毛发的组成及其制造方法

    公开(公告)号：KR1020080060480A

    公开(公告)日：2008-07-02

    申请号：KR1020060134625

    申请日：2006-12-27

    Applicant: 광주과학기술원 ,  한국화학연구원

    Inventor： 김진수 ,  오세화 ,  허선희 ,  김태경 ,  박희문

    IPC: A61K8/49 ,  A61Q5/10

    CPC classification number: A61K8/463 ,  A61K8/411 ,  A61K2800/4324 ,  A61Q5/10

    Abstract: A hair dyeing composition is provided to inhibit skin irritation by removing use of harmful components, improve convenience of use, coloring ability and washability, express various colors, and increase maintenance of color. A hair dyeing composition comprises 1-10 wt.% of thickening agent, 1-20 wt.% of penetrant, 0.01-5 wt.% of reactive dye with a vinylsulfone group, represented by the formula(1), (2), (3), (4) or (5) in which M is alkali metal ion such as H, Li, Na or K, and a remaining amount of water, and further comprises 1-5 wt.% of pH regulator and a reducing agent for reducing -S-S bond of hair keratin. A method for manufacturing the hair dyeing composition comprises the steps of: (a) dissolving the thickening agent in water to obtain a mixture; (b) adding the penetrant into the mixture to form a base solution; and (c) adding the reactive dye with a vinylsulfone group into the base solution.

    Abstract translation: 提供一种染发组合物，通过去除使用有害成分，提高使用方便性，着色能力和洗涤性，表现各种颜色，增加颜色的维持来抑制皮肤刺激。 染发组合物包含1-10重量％的增稠剂，1-20重量％的渗透剂，0.01-5重量％的由乙烯基砜基组成的活性染料，由式（1），（2）， （3），（4）或（5）其中M为碱金属离子如H，Li，Na或K，剩余量为水，还包含1-5重量％的pH调节剂和还原剂 减少头发角蛋白-SS键的药剂。 毛染染色组合物的制造方法包括以下步骤：（a）将增稠剂溶解于水中得到混合物; （b）将渗透剂加入到混合物中以形成碱溶液; 和（c）将具有乙烯砜基团的活性染料加入到碱溶液中。

    벤조티아졸계 분산 반응성 염료 및 이의 제조방법
    16.
    发明公开
    벤조티아졸계 분산 반응성 염료 및 이의 제조방법 失效
    基于苯并噻唑的分散反应性染料及其制备方法

    公开(公告)号：KR1020020061916A

    公开(公告)日：2002-07-25

    申请号：KR1020010003009

    申请日：2001-01-18

    Applicant: 한국화학연구원

    Inventor： 오세화 ,  신승림 ,  전근 ,  박희문 ,  박수열 ,  윤성령

    IPC: C09B29/045

    Abstract: PURPOSE: Provided is benzothiazole-based dispersion-reactive dye, which reduces pollution, dose not contain hazardous amine and metals, can be used in acidic and neutral condition, and is excellent in washing-fastness and properties. CONSTITUTION: The benzothiazole-based dispersion-reactive dye represented by the formula 1 is produced by a process comprising the steps of: diazotizing 2-amino-5-(beta-acetoxy ethyl sulfone)benzothiazole or 2-amino-5-(beta-hydroxy ethyl sulfone)benzothiazole; preparing a coupling solution by dissolving a coupler in an acid mixture; mixing the diazotized 2-amino-5-(beta-acetoxy ethyl sulfone)benzothiazole and the coupling solution at 5-10deg.C and adding a base and separating the produced dye or mixing the diazotized 2-amino-5-(beta-hydroxy ethyl sulfone)benzothiazole and the coupling solution at 5-10deg.C and stirring at 80-90deg.C by using acetic anhydride. In the formula, R, R1, R2, and R3 are identically or differently hydrogen, alkyl, alkoxy, cyanoalkyl, or amino acetyl.

    Abstract translation: 目的：提供苯基噻唑类分散反应性染料，其降低污染，不含有害胺类和金属，可用于酸性和中性条件，耐洗涤性和耐性均优异。 构成：由式1表示的基于苯并噻唑的分散体活性染料通过包括以下步骤的方法制备：将2-氨基-5-（β-乙酰氧基乙基砜）苯并噻唑或2-氨基-5-（β- 羟基乙基砜）苯并噻唑; 通过将成色剂溶解在酸混合物中制备偶联溶液; 将重氮化的2-氨基-5-（β-乙酰氧基乙基砜）苯并噻唑和偶联溶液在5-10℃下混合并加入碱并分离生成的染料或混合重氮化的2-氨基-5-（β-羟基 乙基砜）苯并噻唑和偶联溶液在5-10℃下，通过使用乙酸酐在80-90℃下搅拌。 在该式中，R 1，R 2，R 2和R 3相同或不同，为氢，烷基，烷氧基，氰基烷基或氨基乙酰基。

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