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    Manufacture of anthraquinonoid disperse dyes containing bromine
    11.
    发明授权
    Manufacture of anthraquinonoid disperse dyes containing bromine 失效
    含溴的蒽醌类分散染料的制造

    公开(公告)号：US3925427A

    公开(公告)日：1975-12-09

    申请号：US48641874

    申请日：1974-07-08

    Applicant: BASF AG

    Inventor： ELSER WOLFGANG ,  EILINGSFELD HEINZ ,  SCHOCH WERNER

    IPC: C09B1/00 ,  C07C225/36 ,  C09B1/50 ,  C09B1/54 ,  C07C97/26

    CPC classification number: C09B1/545 ,  C09B1/50

    Abstract: A process for the manufacture of blue anthraquinonoid disperse dyes based on 1,5(1,8)-diamino-4,8(4,5)-dihydroxyanthraquinone, wherein 1,5(1,8)-dinitro-4,8(4,5)-dimethoxy-anthraquinone or mixtures of these compounds are reduced, in 20 to 45% strength by weight oleum, with sulfur at -10* to +50*C in the presence of boric acid, and the product of the reduction is brominated in sulfuric acid or 0 to 5% strength by weight oleum or in organic solvents until the product thus obtained contains 12 to 30% by weight of bromine. Dyes which give deep and, in particular, light-fast dyeings, above all on fibrous materials consisting of linear polyesters, are obtained.

    Abstract translation: 一种制备基于1,5（1,8） - 二氨基-4,8（4,5） - 二羟基蒽醌的蓝色蒽醌类分散染料的方法，其中1,5（1,8） - 二硝基-4,​​8（ 4,5） - 二甲氧基 - 蒽醌或这些化合物的混合物在20-45％重量的发烟硫酸中与硫在-10℃至+ 50℃下在硼酸存在下还原，并且还原产物 在硫酸中溴化，或0〜5％重量的发烟硫酸或有机溶剂，直到由此获得的产物含有12至30重量％的溴。 得到深色的染料，特别是轻度染色，尤其是由线性聚酯组成的纤维材料上。

    Production of 3,6-dihalodiphenylalkanes
    13.
    发明授权
    Production of 3,6-dihalodiphenylalkanes 失效
    生产3,6-二卤代二苯基烷烃

    公开(公告)号：US3911033A

    公开(公告)日：1975-10-07

    申请号：US41625873

    申请日：1973-11-15

    Applicant: BASF AG

    Inventor： SCHAFFNER ERNST ,  EILINGSFELD HEINZ ,  PATSCH MANFRED

    IPC: A01N29/04 ,  C07C17/00 ,  C07C17/12 ,  C07C25/18 ,  C07C67/00 ,  C09B11/00

    CPC classification number: C07C25/18 ,  C07C17/12

    Abstract: The production of 3,6-dihalodiphenylalkanes by reaction of a diphenylalkane with a halogen and the novel 3,6dihalodiphenylalkanes themselves. The new compounds which can be prepared according to the process of the invention may be used as dispersing agents in dye/styrene mixtures and also as dyeing auxiliaries. They are also valuable starting materials for the production of dyes and pesticides.

    Abstract translation: 通过二苯基烷烃与卤素反应生成3,6-二卤代二苯基烷烃和本身的新型3,6-二卤代二苯基烷烃。 可以根据本发明的方法制备的新化合物可以用作染料/苯乙烯混合物中的分散剂，也可以用作染色助剂。 它们也是生产染料和农药的有价值的起始原料。

    Anthraquinone dyes
    15.
    发明授权
    Anthraquinone dyes 失效
    ANTHRAQUINONE染发剂

    公开(公告)号：US3671536A

    公开(公告)日：1972-06-20

    申请号：US3671536D

    申请日：1970-03-17

    Applicant: BASF AG

    Inventor： PATSCH MANFRED ,  EILINGSFELD HEINZ

    IPC: C09B1/22 ,  C09B1/28 ,  C09B1/32 ,  C09B1/58 ,  C07D85/52

    CPC classification number: C09B1/32 ,  C09B1/16 ,  C09B1/22 ,  C09B1/28 ,  C09B1/58

    Abstract: 1,4-DIAMINOANTHRAQUINONES BEARING IN POSITION 2 A 1,2,4OXADIAZOLE GROUP WHICH IS SUBSTITUTED IN POSITION 3 BY AN AROMATIC OR ALIPHATIC RADICAL. These anthraquinone derivatives are valuable blue disperse dyes for use in dyeing and printing synthetic textile materials.

    Abstract translation: 在位置2中的1,4-二氨基四氢喹啉2通过芳族或脂肪族自由基取代位置3中的1,2,4-氧代噻唑基。 这些蒽醌衍生物是用于染色和印刷合成纺织材料的有价值的蓝色分散染料。

    PURE 1-NITROANTHRAQUINONE
    17.
    发明专利
    PURE 1-NITROANTHRAQUINONE 未知

    公开(公告)号：AU6174073A

    公开(公告)日：1975-04-24

    申请号：AU6174073

    申请日：1973-10-24

    Applicant: BASF AG

    Inventor： BANTEL KARL-HEINZ ,  EILINGSFELD HEINZ

    IPC: C07C205/47 ,  C07C67/00 ,  C07C201/00 ,  C07C79/14

    Abstract: 1442670 1-Nitroanthraquinone BASF AG 30 Oct 1973 [31 Oct 1972] 50329/73 Heading C2C 1-Nitroanthraquinone is separated from a mixture containing 1-nitro-anthraquinone, optionally in admixture with 2-nitroanthraquinone together with one or more dinitro-substituted anthraquinones, by treating the mixture to effect reaction of the dinitroanthraquinone(s) with a compound containing one or more methylene groups activated by the presence in the compound of one or more carbonyl groups, the reaction being effected in the presence of from 0À1 to 10% by weight based on the total weight of the starting mixture of an initiator for the reaction and in an aprotic polar organic solvent which optionally contains water in an amount of not more than 10% by weight to form a mother liquor containing in dissolved form the material resulting from the reaction together with any 2-nitroanthraquinone present in the starting mixture and containing 1-nitroanthraquinone in undissolved form. The initiator is preferably a compound which yields nitrite, halide, thiocyanate, alcoholate or phenolate ions and the compounds containing activated methylene groups are preferably aliphatic, cycloaliphatic, araliphatic and heterocyclic unsubstituted or substituted ketones, beta-hetocarboxylic esters or amides, betacarbonyl compounds and cyclic carbonamides.

    New anthraquinone oxdiazole dyes
    18.
    发明专利
    New anthraquinone oxdiazole dyes 未知

    公开(公告)号：GB1041529A

    公开(公告)日：1966-09-07

    申请号：GB3073865

    申请日：1965-07-20

    Applicant: BASF AG

    Inventor： WEIDINGER HANS ,  EILINGSFELD HEINZ ,  MOEBIUS LEANDER

    IPC: C07D271/10 ,  C07D271/113 ,  C09B1/06 ,  C09B1/22 ,  C09B1/26 ,  C09B1/58 ,  C09B1/60

    Abstract: The invention comprises dyes of the formula wherein X is amino, or alkylamino; Y is hydrogen, amino, alkylamino, hydroxy, piperidinyl or alkylmercapto; Z is a linear or branched chain alkyl of up to 8 carbon atoms which may bear alkoxy, cyano, unsubstituted or substituted carbamoyl or carbalkoxy groups, or denotes an aralkyl radical or the propinyl group. The compounds are prepared by reacting a carboxylic hydrazide of the formula where Z11 is No2 or as Y, either with CS2 in a alkaline reacting agent, and simultaneously or subsequently reacting with an alkylating agent which yields Z, or with a mercapto formamide chloride of the formula where R1 and R2 are substituted or unsubstitute alkyl or aryl radicals or together with the nitrogen form a piperidinyl or morpholino ring, and subsequently reducing the nitro group to an amino group. The mercapto formamide chloride may be formed in situ by treating a dithiocarbamic ester of the formula with chlorinating agents.

    Dye compositions for dyeing and printing linear aromatic polyesters
    19.
    发明专利
    Dye compositions for dyeing and printing linear aromatic polyesters 未知

    公开(公告)号：GB1001497A

    公开(公告)日：1965-08-18

    申请号：GB2005964

    申请日：1964-05-14

    Applicant: BASF AG

    Inventor： WEIDINGER HANS ,  EILINGSFELD HEINZ ,  MOEBIUS LEANDER

    IPC: C09B1/20 ,  C09B1/58 ,  D06P1/20

    Abstract: Anthraquinone dyes of the formula wherein X is -NH2 or -OH, Y is a -NH2, alkylamino, aralkylamino, arylamino, morpholyl, -OH, alkoxy, alkyl- or aryl-mercapto group and R is an alkyl, alkyl ether, alkyl-mercapto, alkoxy, alkylamino, aralkylamino or arylamino group or an aromatic radical possibly substituted by halogen atoms, alkyl or alkoxy groups are employed to dye or print materials of aromatic polyesters. The dyes may be prepared according to the methods described in Specifications 789,759 and 986,045.ALSO:Dyeing or printing aromatic polyester materials is effected by applying a composition containing as dyestuff: wherein X is -NH2 or -OH, Y is a -NH2, alkylamino, aralkylamino, arylamino, morpholyl, -OH, alkoxy, alkyl- or aryl-mercapto group and R is an alkyl, alkyl ether, alkylmercapto, alkoxy, alkylamino, aralkylamino or arylamino group or an aromatic radical possibly substituted by halogen atoms, alkyl or alkoxy groups. The dyes may be applied in finely divided form at 95-140 DEG C. or printed on and later steamed. Carriers may be coemployed. Examples are given.

    Water-soluble azo dyes
    20.
    发明专利
    Water-soluble azo dyes 未知

    公开(公告)号：GB969116A

    公开(公告)日：1964-09-09

    申请号：GB3492662

    申请日：1962-09-13

    Applicant: BASF AG

    Inventor： WEIDINGER HANS ,  EILINGSFELD HEINZ

    IPC: C09B62/08 ,  C09B62/085

    Abstract: Diazotisable aromatic amines for use in the preparation of azo dyes (see Division C4) are obtained by halogenating, preferably chlorinating 2-nitroaryl-4, 6-dihydroxytriazines -(1, 3, 5), exchanging a halogen atom for the radical of an amine and catalytically reducing the nitro group. 2-(3-aminophenyl) -4- morpholino 6-choro-1, 3, 5-triazine is obtained by chlorinating 2-(3-nitrophenyl)-4 6-dihydroxy-1, 3, 5-triazine), reacting the product with morpholine and reducing the product with hydrogen using a Raney nickel catalyst. 2-(3-aminophenyl) -4- phenylamino-6-chloro-1, 3, 5-triazine is prepared by a similar process. Specification 874,519 is referred to.ALSO:The invention comprises water-soluble monoazo, disazo or polyazo dyes containing one or more water-solubilizing groups, preferably one or more sulphonic acid groups and having the general formula in which A denotes an unsubstituted aromatic radical or a substituted aromatic radical, X denotes a halogen atom, preferably a chlorine or bromine atom or the group wherein R1 denotes an aliphatic, cycloaliphatic, araliphatic, aromatic or heterocyclic radical or a hydrogen atom, R2 denotes an aliphatic, cycloaliphatic, araliphatic, aromatic or heterocyclic radical, or the radicals R1 and R2 together with the nitrogen atom may form a heterocyclic ring which may also contain other hetero atoms and E denotes the radical of a coupling component which may in turn contain an azo group and also once again the radical The dyes are produced by reacting a diazotized 2 - aminoaryl - 6 - halo - 4 - amino - 1,3,5 - triazine which is substituted at the amino nitrogen in the 4-position with a compound capable of coupling. Disazo dyes are obtained by converting monoazo dyes containing a diazotizable amino group into diazo compounds and coupling with suitable coupling components or by reacting monoazo dyes capable of coupling with any aromatic diazo compounds. Coupling components specified include various hydroxynaphthalene sulphonic acids, amino hydroxynaphthalene sulphonic acids and N-acyl derivatives thereof and such pyrazolones as 1-(2-methyl - 4 - sulphophenyl) - 3 - methyl -, 1 - (2 - chloro - 5 - sulphophenyl) - 3 - methyl -, 1 - phenyl - 3 - carboxy - pyrazolones (5). The diazo components may be obtained by halogenating 2-nitro-aryl 4,6-dihydroxytriazines (1, 3, 5) exchanging a halogen atom for the radical of an amine and reducing the nitro group (see Division C2) Amines specified from which the radical NR1R2 may be derived include aniline, morpholine, piperidine and thiomorpholine-dioxide. Examples are furnished. The dyes are suitable for dyeing wool, silk, synthetic polyamides, polyurethanes, leather and natural or regenerated cellulose. Specification 874,519 is referred to.

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