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    11.
    发明专利
    未知

    公开(公告)号：BR0313247A

    公开(公告)日：2005-07-12

    申请号：BR0313247

    申请日：2003-07-30

    Applicant: BASF AG

    Inventor： ADAMI CHRISTOPH ,  KARL JOERN ,  HAUK ALEXANDER ,  BOEHLING RALF ,  PASTRE JOERG ,  LENZ ROBERT

    IPC: C07C51/09 ,  C07C51/43 ,  C07C51/44 ,  C07C53/02 ,  C07C53/06 ,  A23K3/03 ,  A23L1/304 ,  A61L9/00

    Abstract: A method for the production of formic acid-formates (I) involves (a) partial hydrolysis of methyl formate (MF) with water, (b) distillation to give formic acid and water (stream S1) and (c) combination of (S1) with the corresponding formate (F) to give a mixture of (I) and water. An Independent claim is also included for apparatus for the production of (I), comprising a reactor (A) for the hydrolysis of MF, a distillation column (B) for separating a stream containing MF, formic acid, methanol and water into MF, methanol and a stream (S1) containing formic acid and water, and a column (E) for removing water from S1.

    14.
    发明专利
    未知

    公开(公告)号：DE50308660D1

    公开(公告)日：2008-01-03

    申请号：DE50308660

    申请日：2003-07-30

    Applicant: BASF AG

    Inventor： ADAMI CHRISTOPH ,  KARL JOERN ,  HAUK ALEXANDER ,  BOEHLING RALF ,  PASTRE JOERG ,  LENZ ROBERT

    IPC: A23K1/16 ,  C07C51/09 ,  A01N1/00 ,  A01N3/00 ,  A61K31/19 ,  A61P3/00 ,  B01D9/02 ,  C07C51/41 ,  C07C53/02 ,  C07C53/06

    Abstract: Formic acid-formates are produced by (a) partial hydrolysis of methyl formate (MF) with water, (b) distillation to give (S1) formic acid and water, (c) conversion of the other product from (b) (mainly MF) into a stream (S2) containing formate and water by reaction with aqueous strong base and distillation of methanol, and (d) combination of (S1) with (S2). A method for the production of formic acid-formates (I) involves: (a) partial hydrolysis of methyl formate (MF) with water; (b) distillation to give a stream (S1) containing formic acid and water; (c) conversion of the MF- and possibly methanol-containing stream from (b) into a formate- and water-containing stream (S2) by (i) reaction with a basic compound of an acid with a pKa value of at least 3 in presence of water followed by (ii) removal of methanol by distillation; and (d) combination of streams (S1) and (S2). An Independent claim is also included for apparatus for the production of (I), comprising: (A) a reactor for the hydrolysis of MF; (B) a distillation column for separating a stream containing MF, formic acid, methanol and water; (C) a column for the hydrolysis of MF with a basic compound with removal of methanol by distillation (with an inlet for the base above the inlet for the product from (B)); and (D) a column connected to the bottom of (B) for removing water from the stream containing formic acid and water.

    METHOD AND DEVICE FOR PRODUCING FORMIC ACID FORMATES AND USE OF SAID FORMATES
    19.
    发明专利
    METHOD AND DEVICE FOR PRODUCING FORMIC ACID FORMATES AND USE OF SAID FORMATES 未知

    公开(公告)号：PL375582A1

    公开(公告)日：2005-11-28

    申请号：PL37558203

    申请日：2003-07-30

    Applicant: BASF AG

    Inventor： ADAMI CHRISTOPH ,  KARL JOERN ,  HAUK ALEXANDER ,  BOEHLING RALF ,  PASTRE JOERG ,  LENZ ROBERT

    IPC: A23K1/16 ,  A01N1/00 ,  A01N3/00 ,  A61K31/19 ,  A61P3/00 ,  B01D9/02 ,  C07C51/09 ,  C07C51/41 ,  C07C53/06 ,  C07C53/02

    Abstract: Formic acid-formates are produced by (a) partial hydrolysis of methyl formate (MF) with water, (b) distillation to give (S1) formic acid and water, (c) conversion of the other product from (b) (mainly MF) into a stream (S2) containing formate and water by reaction with aqueous strong base and distillation of methanol, and (d) combination of (S1) with (S2). A method for the production of formic acid-formates (I) involves: (a) partial hydrolysis of methyl formate (MF) with water; (b) distillation to give a stream (S1) containing formic acid and water; (c) conversion of the MF- and possibly methanol-containing stream from (b) into a formate- and water-containing stream (S2) by (i) reaction with a basic compound of an acid with a pKa value of at least 3 in presence of water followed by (ii) removal of methanol by distillation; and (d) combination of streams (S1) and (S2). An Independent claim is also included for apparatus for the production of (I), comprising: (A) a reactor for the hydrolysis of MF; (B) a distillation column for separating a stream containing MF, formic acid, methanol and water; (C) a column for the hydrolysis of MF with a basic compound with removal of methanol by distillation (with an inlet for the base above the inlet for the product from (B)); and (D) a column connected to the bottom of (B) for removing water from the stream containing formic acid and water.

    20.
    发明专利
    未知

    公开(公告)号：BR0315375A

    公开(公告)日：2005-08-23

    申请号：BR0315375

    申请日：2003-10-21

    Applicant: BASF AG

    Inventor： PASTRE JOERG ,  EXNER KAI MICHAEL ,  STUER WOLFRAM ,  GEISSLER ELKE ,  MACHHAMMER OTTO

    IPC: C07C51/09 ,  C07C51/54 ,  C07C51/56 ,  C07C67/10 ,  C07C53/122 ,  C07C53/124 ,  C07C63/313 ,  C07C53/02 ,  C07C69/14 ,  C07C53/12

    Abstract: Disclosed is a method for jointly producing (i) formic acid (III); (ii) a carboxylic acid comprising at least two carbon atoms (II) and/or the derivatives thereof; and (iii) a carboxylic acid anhydride (VII). According to said method, (a) a formic acid ester (I) is transesterfied to formic acid (III) and the corresponding carboxylic acid ester (IV) by means of a carboxylic acid comprising at least two carbon atoms (II); (b) at least one portion of the carboxylic acid ester (IV) formed in step (a) is carbonylated in order to obtain the carboxylic acid anhydride (V); and (c) at least one portion of the carboxylic acid anhydride (V) formed in step (b) is further dehydrated by means of a carboxylic acid (VI) so as to form a carboxylic acid anhydride (VII) and the carboxylic acid (II).

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