13.
    发明专利
    未知

    公开(公告)号:DE50009431D1

    公开(公告)日:2005-03-10

    申请号:DE50009431

    申请日:2000-08-31

    Applicant: BASF AG

    Abstract: Process for the purification of carbonyl chlorides which have been prepared by reacting carboxylic acids with phosgene or thionyl chloride in the presence of a catalyst adduct, in which the carbonyl chlorides are treated with a hydrohalide of carboxamides of the formula (I)in which R is hydrogen or C1- to C3-alkyl; R and R independently of one another are C1- to C4-alkyl, or R and R together are a C4- or C5-alkylene chain, and the carbonyl chloride purified in this way is isolated by separation off from the carboxamide hydrohalide phase.

    METHOD FOR PRODUCING CHLOROCARBOXYLIC ACID CHLORIDES

    公开(公告)号:HU0301077A2

    公开(公告)日:2003-08-28

    申请号:HU0301077

    申请日:2001-02-28

    Applicant: BASF AG

    Abstract: The invention relates to a method for producing chlorocarboxylic acid chlorides of formula (I), wherein R and R , independently from one another, mean a hydrogen atom, an organic radical containing carbon, a halogen, a nitro or cyano group and Y means an alkylene chain having 1 to 10 carbon atoms in the chain which is unsubstituted or is substituted by organic radicals that contain carbon, by halogen, nitro and/or cyano groups, whereby the alkylene chain can be interrupted by an ether-, thioether-, tertiary amino- or keto group, whereby the organic radicals of Y and/or R and/or R can be connected to one another and thereby form a non-aromatic system, whereby said radicals contain carbon, by converting a lactone of formula (II), wherein R , R and Y have the aforementioned meanings, using a hydrogen chloride and phosgene in the presence of a catalyst. Hydrogen chloride is added before and/or while phosgene is added. The hydrogen chloride is only introduced at a temperature of at least 60 DEG C. A pyridine compound is used as the catalyst.

    18.
    发明专利
    未知

    公开(公告)号:AT241580T

    公开(公告)日:2003-06-15

    申请号:AT99911747

    申请日:1999-03-08

    Applicant: BASF AG

    Abstract: The invention relates to a continuous method for producing propargyl chloride by reacting propargyl alcohol with a chlorinating agent in the presence of a catalyst. According to the invention, the chlorinating agent, propargyl alcohol and 0.1 to 10 mol.% of the catalyst with regard to the amount of propargyl alcohol is continuously dosed in a reaction zone and is reacted at a temperature ranging from 40 to 70 DEG C.

    20.
    发明专利
    未知

    公开(公告)号:ES2174527T3

    公开(公告)日:2002-11-01

    申请号:ES98963492

    申请日:1998-11-21

    Applicant: BASF AG

    Abstract: The present invention provides process for the preparation of chlorocarbonyl chlorides of the formula IwhereR1 is for example hydrogen or C1- to C20-alkyl andY is for example a saturated or mono- or polyolefinically unsaturated C2-C8-alkylene chain,by reacting lactones with a chlorinating agent in the presence of a urea compound.

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