公开(公告)号：IN2341MUN2014A

公开(公告)日：2015-08-14

申请号：IN2341MUN2014

申请日：2014-11-18

Applicant: BASF SE

Inventor： REINHARD ROBERT ,  CHIODO TIZIANA ,  WOLF BERND ,  SCHERER STEFAN ,  BRATZ MATTHIAS ,  WITSCHEL MATTHIAS ,  NEWTON TREVOR WILLIAM ,  SEITZ THOMAS

IPC: C07D413/04 ,  A01N43/90

Abstract: The present invention relates to a novel crystalline form B of 1 5 dimethyl 6 thioxo 3 (2 2 7 trifluoro 3 oxo 4 (prop 2 ynyl) 3 4 dihydro 2H benzo[b][1 4]oxazin 6 yl) 1 3 5 triazinane 2 4 dione The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1 5 dimethyl 6 thioxo 3 (2 2 7 trifluoro 3 oxo 4 (prop 2 ynyl) 3 4 dihydro 2H benzo[b][1 4]oxazin 6 yl) 1 3 5 triazinane 2 4 dione.

公开(公告)号：CO7160073A2

公开(公告)日：2015-01-15

申请号：CO14278794

申请日：2014-12-18

Applicant: BASF SE

Inventor： REINHARD ROBERT ,  CHIODO TZIANA ,  WOLF BERND ,  SCHERER STEFAN ,  BRATZ MATTHIAS ,  WITSCHEL MATTHIAS ,  NEWTON TREVOR WILLIAM ,  SEITZ THOMAS

IPC: A01N43/84 ,  A01P13/00 ,  C07D413/04

Abstract: Una forma cristalina A novedosa de 1,5-dimetil-6-tioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-inil)-3,4-dihidro-2H-benzo[b][1,4]oxazin-6-il)-1,3,5-triazinan-2,4-diona. También un proceso para la producción de esta forma cristalina y formulaciones para la fitoprotección que contienen la forma cristalina novedosa de 1,5-dimetil-6-tioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-inil)-3,4-dihidro-2H-benzo[b][1 ,4]oxazin-6-il)-1 ,3,5-triazinan-2,4-diona.

公开(公告)号：BRPI0718771A2

公开(公告)日：2013-11-26

申请号：BRPI0718771

申请日：2007-11-05

Applicant: BASF SE

Inventor： SAXELL HEIDI EMILIA ,  ERK PETER ,  TARANTA CLAUDE ,  KROEHL THOMAS ,  COX GERHARD ,  DESIRAJU GAUTAM R ,  BANERJEE RAHUL ,  BHATT PRASHANT M ,  SUKOPP MARTIN ,  SCHERER STEFAN ,  OJALA ANTTI

IPC: A01N47/02 ,  A01N25/00 ,  A01P7/00

Abstract: The present invention relates to a novel crystalline modification of fipronil, to a process for the preparation of the same, to pesticidal and parasiticidal mixtures and compositions comprising said crystalline modification and to their use for combating pests and parasites.

公开(公告)号：MX2009004264A

公开(公告)日：2009-05-05

申请号：MX2009004264

申请日：2007-11-05

Applicant: BASF SE

Inventor： ERK PETER ,  KROEHL THOMAS ,  COX GERHARD ,  TARANTA CLAUDE ,  SAXELL HEIDI EMILIA ,  SUKOPP MARTIN ,  DESIRAJU GAUTAM R ,  BANERJEE RAHUL ,  BHATT PRASHANT M ,  SCHERER STEFAN ,  OJALA ANTTI

IPC: A01N47/02 ,  A01N25/00 ,  A01P7/00

Abstract: Una novedosa modificación cristalina de fipronil, a un procedimiento para preparar esa modificación, a mezclas plaguicidas y parasiticidas y composiciones que comprenden esa modificación cristalina, y a su uso para combatir plagas y parásitos.

公开(公告)号：BR122019020541B1

公开(公告)日：2022-04-19

申请号：BR122019020541

申请日：2007-11-05

Applicant: BASF SE

Inventor： OJALA ANTTI ,  TARANTA CLAUDE ,  GAUTAM R DESIRAJU ,  COX GERHARD ,  HEIDI EMILIA SAXELL ,  SUKOPP MARTIN ,  ERK PETER ,  PRASHANT M BHATT ,  BANERJEE RAHUL ,  SCHERER STEFAN ,  KRÖHL THOMAS

IPC: A01N25/00 ,  A01N47/02 ,  A01P7/00

Abstract: a presente invenção diz respeito a uma modificação cristalina inédita de fipronil, a um processo para a preparação do mesmo, a misturas e composições pesticidas e parasiticidas compreendendo a dita modificação cristalina e a seu uso para combater pragas e parasitas.

公开(公告)号：CA2871345C

公开(公告)日：2020-11-03

申请号：CA2871345

申请日：2013-05-15

Applicant: BASF SE

Inventor： REINHARD ROBERT ,  CHIODO TIZIANA ,  WOLF BERND ,  SCHERER STEFAN ,  BRATZ MATTHIAS ,  WITSCHEL MATTHIAS ,  NEWTON TREVOR WILLIAM ,  SEITZ THOMAS

IPC: C07D413/04 ,  A01N43/90

Abstract: The present invention relates to a novel crystalline form B of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione (Formula 1). The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione. (see formula I)

公开(公告)号：CA2871315C

公开(公告)日：2020-11-03

申请号：CA2871315

申请日：2013-05-15

Applicant: BASF SE

Inventor： REINHARD ROBERT ,  CHIODO TIZIANA ,  WOLF BERND ,  SCHERER STEFAN ,  BRATZ MATTHIAS ,  WITSCHEL MATTHIAS ,  NEWTON TREVOR WILLIAM ,  SEITZ THOMAS

IPC: C07D413/04 ,  A01N43/84 ,  A01P13/00

Abstract: The present invention relates to a novel crystalline form A of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4- dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione. The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3- oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5- triazinane-2,4-dione.

公开(公告)号：AU2013265471B2

公开(公告)日：2017-03-02

申请号：AU2013265471

申请日：2013-05-15

Applicant: BASF SE

Inventor： REINHARD ROBERT ,  CHIODO TIZIANA ,  WOLF BERND ,  SCHERER STEFAN ,  BRATZ MATTHIAS ,  WITSCHEL MATTHIAS ,  NEWTON TREVOR WILLIAM ,  SEITZ THOMAS

IPC: C07D413/04 ,  A01N43/84 ,  A01P13/00

Abstract: The present invention relates to a novel crystalline form A of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4- dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione. The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3- oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5- triazinane-2,4-dione.

公开(公告)号：IN2342MUN2014A

公开(公告)日：2015-08-14

申请号：IN2342MUN2014

申请日：2014-11-18

Applicant: BASF SE

Inventor： REINHARD ROBERT ,  CHIODO TIZIANA ,  WOLF BERND ,  SCHERER STEFAN ,  BRATZ MATTHIAS ,  WITSCHEL MATTHIAS ,  NEWTON TREVOR WILLIAM ,  SEITZ THOMAS

IPC: C07D413/04 ,  A01N43/84 ,  A01P13/00

Abstract: The present invention relates to a novel crystalline form A of 1 5 dimethyl 6 thioxo 3 (2 2 7 trifluoro 3 oxo 4 (prop 2 ynyl) 3 4 dihydro 2H benzo[b][1 4]oxazin 6 yl) 1 3 5 triazinane 2 4 dione. The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1 5 dimethyl 6 thioxo 3 (2 2 7 trifluoro 3 oxo 4 (prop 2 ynyl) 3 4 dihydro 2H benzo[b][1 4]oxazin 6 yl) 1 3 5 triazinane 2 4 dione.

公开(公告)号：NZ576639A

公开(公告)日：2012-03-30

申请号：NZ57663907

申请日：2007-11-05

Applicant: BASF SE

Inventor： SAXELL HEIDI EMILIA ,  ERK PETER ,  TARANTA CLAUDE ,  KROHL THOMAS ,  COX GERHARD ,  DESIRAJU GAUTAM R ,  BANERJEE RAHUL ,  BHATT PRASHANT M ,  SUKOPP MARTIN ,  SCHERER STEFAN ,  OJALA ANTTI

IPC: A01N25/00 ,  A01N47/02 ,  A01P7/00

Abstract: Disclosed is a process for preparing solid fipronil comprising at least 85 percent by weight of the crystalline modification I of fipronil being present in the monoclinic system having the centrosymmetric space group C2/c comprising the steps of: step i) preparing a solution of a solid form of fipronil being different from the crystalline modification I in a solvent S comprising at least one acetonitrile, dimethylsulfoxide, or at least one benzene derivative; step ii) effecting crystallization of fipronil; and step iii) isolating the resulting precipitate wherein, in case the solvent S is pure acetonitrile, the crystallization step ii) is conducted at temperatures below 40 degrees Celsius and in case the solvent S is pure dimethylsulfoxide, the crystallization step ii) is conducted at temperatures below 80 degrees Celsius.