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    METHOD FOR THE PRODUCTION OF N-SUBSTITUTED (3-DIHALOMETHYL-1-METHYL-PYRAZOLE-4-YL) CARBOXAMIDES
    11.
    发明专利
    METHOD FOR THE PRODUCTION OF N-SUBSTITUTED (3-DIHALOMETHYL-1-METHYL-PYRAZOLE-4-YL) CARBOXAMIDES 未知

    公开(公告)号：CA2686659A1

    公开(公告)日：2008-12-04

    申请号：CA2686659

    申请日：2008-05-30

    Applicant: BASF SE

    Inventor： ALTENHOFF ANSGAR GEREON ,  CHALLAND NINA ,  SMIDT SEBASTIAN PEER ,  RACK MICHAEL ,  RHEINHEIMER JOACHIM ,  SCHMIDT-LEITHOFF JOACHIM ,  ZIERKE THOMAS

    IPC: C07D231/14

    Abstract: The present invention relates to a method for the production of n-substit uted (3-dihalomethyl-1-methyl-pyrazole-4-YL) carboxamides of the formula (I) , wherein R1 stands for optionally substituted phenyl or C3-C7-cycloalkyl, R 1a stands for hydrogen or fluorine, or R1a together with R1 stands for optio nally substitutedC3-C5-alkyandiyl or C5-C7-cycloalkandiyl, R2 stands for C1- C6-alkyl, C2-C6-alkenyl, C2-C6-alkinyl or C1-C4-alkoxy-C1-C2-alkyl, X stands for F or Cl, and n stands for 0, 1, 2, or 3, said method comprising A) prov iding a compound of the formula (II), wherein X stands for F or Cl, Y for Cl or Br, and R2 has one of the above-mentioned meanings, and B) the reaction of a compound of the formula (II) with carbon monoxide and a compound of the formula (III), wherein R1, R1a and n have one of the above-mentioned meanin gs; in the presence of a palladium catalyst; the intermediate products used for the production according to the inventive method; and methods for the pr oduction thereof.

    Proceso continuo para preparar neral en forma pura
    12.
    发明专利
    Proceso continuo para preparar neral en forma pura 未知

    公开(公告)号：ES2560453T3

    公开(公告)日：2016-02-19

    申请号：ES08760728

    申请日：2008-06-09

    Applicant: BASF SE

    Inventor： HEYDRICH GUNNAR ,  KASHANI-SHIRAZI NAWID ,  JÄKEL CHRISTOPH ,  SCHMIDT-LEITHOFF JOACHIM

    IPC: C07C45/82 ,  B01D3/14 ,  C07C45/83 ,  C07C47/21

    Abstract: Proceso continuo para producir neral de la fórmula (I)**Fórmula** en forma pura con un contenido de neral mayor o igual a 95% en peso, respecto de la cantidad total, mediante separación por destilación de neral a partir de mezclas de sustancias que contienen neral y geranial de la fórmula (II)**Fórmula** en cuyo caso la separación por destilación se realiza en una columna de pared divisoria o en una interconexión de dos columnas de destilación en forma de un acoplamiento térmico con 80 hasta 200 platos teóricos y uno o varios sitios de extracción lateral a una presión absoluta de operación de 5 hasta 200 mbar, caracterizado porque se emplea una mezcla de sustancias que está compuesta en 30 hasta 70 % en peso de neral, en 70 hasta 30 % en peso de geranial y en 0 hasta 5 % en peso de otros componentes, en cuyo caso los datos porcentuales suman 100% en peso.

    METHOD FOR PRODUCING SUBSTITUTED BIPHENYLS
    14.
    发明专利
    METHOD FOR PRODUCING SUBSTITUTED BIPHENYLS 未知

    公开(公告)号：ZA201100589B

    公开(公告)日：2012-03-28

    申请号：ZA201100589

    申请日：2011-01-24

    Applicant: BASF SE

    Inventor： MAYALD VOLKER ,  WISSEL-STOLL KATHRIN ,  SCHMIDT-LEITHOFF JOACHIM ,  ALTENHOFF ANSGAR GEREON ,  KEIL MICHAEL ,  SMIDT SEBASTIAN PEER

    IPC: C07C20060101

    Abstract: Preparation of substituted biphenyl compounds (I), comprises reacting halobenzene compounds (II) with phenyl boronic acid compounds (IVa) and/or diphenyl boronic acid compounds (IVb) in a solvent or a diluent in the presence of a base and a palladium catalyst, which comprises palladium and a bidentate phosphorus ligand (III). Preparation of substituted biphenyl compounds of formula (I), comprises reacting halobenzene compounds of the formula (II) with phenyl boronic acid compounds of formula (IVa) and/or diphenyl boronic acid compounds of formula (IVb) in a solvent or diluent in the presence of a base and a palladium catalyst, which comprises palladium and a bidentate phosphorus ligand of formula (((Ar1) 2P-CH 2-)(R5)C(R4)(-CH 2-P(Ar1) 2)) (III). R1 : NO 2or NH 2; R2 : CN, halo, 1-4C-haloalkyl, 1-4C-haloalkoxy or 1-4C-haloalkylthio; R3 : H, CN or halo; Hal : Cl or Br; Ar1 : phenyl, which optionally contains 1-3 substituents comprising CH 3, CH 3O, F or Cl; either R4, R5 : 1-5C-alkyl or 3-6C-cycloalkyl; or R4R5 : 2-7-membered bridge, which optionally carries 1-8C-alkyl; and n : 0-3. An independent claim is included for 3,4,5-trifluoro-2'-nitrobiphenyl. [Image].

    Method for the production of n-substituted (3-dihalomethyl-1-methyl-pyrazole-4-YL) carboxamides
    17.
    发明专利
    Method for the production of n-substituted (3-dihalomethyl-1-methyl-pyrazole-4-YL) carboxamides 未知

    公开(公告)号：AU2008257515A1

    公开(公告)日：2008-12-04

    申请号：AU2008257515

    申请日：2008-05-30

    Applicant: BASF SE

    Inventor： SCHMIDT-LEITHOFF JOACHIM ,  SMIDT SEBASTIAN PEER ,  CHALLAND NINA ,  ALTENHOFF ANSGAR GEREON ,  RACK MICHAEL ,  RHEINHEIMER JOACHIM ,  ZIERKE THOMAS

    IPC: C07D231/14

    Abstract: The present invention relates to a process for preparing N-substituted (3-dihalomethylpyrazol-4-yl)carboxamides of the formula (I) in which R1 is optionally substituted phenyl or C3-C7-cycloalkyl, R1a is hydrogen or fluorine, or R1a together with R1 is optionally substituted C3-C5-alkanediyl or C5-C7-cycloalkanediyl, R2 is C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkynyl or C1-C4-alkoxy-C1-C2-alkyl, X is F or Cl and n is 0, 1, 2 or 3; which comprises A) providing a compound of the formula (II) in which X is F or Cl, Y is Cl or Br and R2 has one of the meanings given above and B) reacting a compound of the formula (II) with carbon monoxide and a compound of the formula (III) in which R1, R1a and n have one of the meanings given above; in the presence of a palladium catalyst; to intermediates used for the preparation according to the process according to the invention, and also to processes for their preparation.

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