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    MIXTURES OF OPTICAL BRIGHTENERS
    11.
    发明专利
    MIXTURES OF OPTICAL BRIGHTENERS 未知

    公开(公告)号：DE3160803D1

    公开(公告)日：1983-10-06

    申请号：DE3160803

    申请日：1981-02-25

    Applicant: HOECHST AG

    Inventor： MARTINI THOMAS DR ,  ROSCH GUNTER

    IPC: C09B57/00 ,  C09B67/22 ,  D06L3/12 ,  D06L4/65

    Abstract: Mixtures of optical brighteners consisting of (a) 1 to 99 weight % of one or several compounds of the formula 1 (1) (b) 99 to 1 weight % of one or several compounds of the formula 2 (2) wherein n is 0 or 1, X is oxygen or sulfur, B is a group of the formulae +TR and the other substituents are defined a specified in the description.

    Aliphatic per:fluoro-ketone(s) prepn. - from per:fluoro-carboxylic acid salt and per:fluoro-acyl fluoride, useful as heat transfer media or lubricant
    14.
    发明专利
    Aliphatic per:fluoro-ketone(s) prepn. - from per:fluoro-carboxylic acid salt and per:fluoro-acyl fluoride, useful as heat transfer media or lubricant 未知

    公开(公告)号：DE2704607A1

    公开(公告)日：1978-08-10

    申请号：DE2704607

    申请日：1977-02-04

    Applicant: HOECHST AG

    Inventor： MARTINI THOMAS DR

    IPC: C07D319/12 ,  C07C45/205 ,  C07C49/175

    Abstract: Aliphatic perfluoroketones (I) are prepd. by reacting a perfluorocarboxylic acid salt R1-CO2M (II) with a perfluoroacyl fluoride R2-CO-F (III) in a polar aprotic solvent at 20-200 degrees C. In the formulae M is Li, Na, K, Rb, Cs or Ag; R1 is 2-50C perfluoroalkyl opt. contg. ether-O-function(s) R2 is 1-50C perfluoroalkyl opt. contg. ether-O-function(s). (II) may be prepd. from R1COF and a salt of formic or oxalic acid or of a Gp. IIIA to VIIA element oxyacid which is less strong than CF3CO2H, esp. M2CO3. Prepn. is in a polar aprotic solvent at 20-200 degrees C. Alternatively a mixt. of (II) and (III) may be prepd. from (R1CO)2O and an alkali metal fluoride. Perfluorolefins (which are difficult to obtain) are not used. High boiling (I) may be prepd. (I) are inert to acids, oxidants and heat. They may be used as heat transfer media or lubricants. In an example perfluoro-2,4-bis-(3,6-dimethyl-1,4-dioxanyl-2-oxylpentan-3-one was prepd. from potassium perfluoro- alpha-(3,6-dimethyl-1,4-dioxanyl-2-oxylpropionate and the corresp. perfluoroacyl fluoride in tetraglyme.

    16.
    发明专利
    未知

    公开(公告)号：DE59201039D1

    公开(公告)日：1995-02-09

    申请号：DE59201039

    申请日：1992-01-18

    Applicant: HOECHST AG

    Inventor： MARTINI THOMAS DR ,  MEES BERNHARD DR ,  OPPITZ PETER

    IPC: C09B67/42 ,  C09B67/46 ,  C09K23/00 ,  C09K23/42 ,  C09K23/44 ,  C09K23/52 ,  B01F17/52 ,  B01F17/44 ,  B01F17/42

    Abstract: The invention relates to dispersing agents based on a mixture of at least one compound of the formula 1 in which Ar is benzene or naphthalene, X is -CH2-CH2- and/or -CH2-CH(CH3)-, 0 to (m-1) of the radicals A are hydrogen, 1 to m of the radicals A are benzoyl and/or naphthoyl, 1 to m of the radicals A are -CO-CM=CH-COOM and/or -CO-CH2-CH(SO3M)-COOM, M being a cation, R , R and R are hydrogen and/or alkyl having 1 to 14 carbon atoms, R is hydrogen and/or alkyl having 1 to 9 carbon atoms, n is a number from 1 to 150 and m is a number from 2 to 12, with compounds of the formula 2 in which R and R independently of one another are an alkyl group from methyl to butyl and are in the m-position relative to the hydroxyl group, R is hydrogen or methyl and Me is a cation, especially a proton or an alkali metal cation, alkaline earth metal cation or ammonium cation, and x and y are the numbers 0, 1 and 2, the total of these numbers being at least 1. The dispersing agents according to the invention are suitable for preparing dispersions of dyes, pigments, plant protection agents and pesticides and for preparing dyeing baths, padding baths and pastes for paper printing and textile printing.

    1,4-Bis(cyano styryl) mixts. for optical brighteners - esp. for natural or (semi)synthetic high molecular organic material partic. polyester fibres
    17.
    发明专利
    1,4-Bis(cyano styryl) mixts. for optical brighteners - esp. for natural or (semi)synthetic high molecular organic material partic. polyester fibres 未知

    公开(公告)号：DE4219772A1

    公开(公告)日：1993-12-23

    申请号：DE4219772

    申请日：1992-06-17

    Applicant: HOECHST AG

    Inventor： AUTZE VOLKER DR ,  MARTINI THOMAS DR

    IPC: C07C255/51 ,  C09D7/12 ,  C11D3/42 ,  D06L3/12 ,  D06L4/65

    Abstract: Mixt. of at least three different cpd.s of formula (I) contains 30-90 wt% o,p-ionomers or 20-90 wt%, m,p-isomers are two other symmetrically and/or asymmetrically, substd. ionomers, p,p'-ionomers. Also claimed is the prepn. of the mixt. contg. below 5-50 wt% o,o'-, o,p'= and o,m'-ionomers of (I) by reacting terephthaldialdehyde (TPADA) with cpds. of formulae (II), (III) and (IV). Q = -CH2P(O)(OR2), -CH2-P(O)R(OR), -CH2-P(O)-R2 or -CH2-P+R3X; R = opt. substd. 1-6(1-4)C alkyl or aryl; and X = Cl or Br. 1 mol. equiv. TPADA is reacted with 1.05-1.5 and equiv. (II) then 0.05-0.5 (0.005-0.7) mol. equiv. (III) and 0.45-0.9 (0.25-0.7) mol. equiv. (IV). USE/ADVANTAGE - Used as optical brightness in natural or (semi)synthetic high monomer organic materials, partic. polyester fibres (claimed), as well as granulates, foams, fibre e.g. for use in textile webs, paper etc., coatings, etc.. Whitener is good and icd nuauces can be observed. Further uses include scintillators for e.g. electrophotography, spin-bath prepn. in the mfr. of e.g. wash-and-wear clothing and in mixts. contg. pigments for printing dyebaths.

    18.
    发明专利
    未知

    公开(公告)号：DE58905391D1

    公开(公告)日：1993-09-30

    申请号：DE58905391

    申请日：1989-12-21

    Applicant: HOECHST AG

    Inventor： MARTINI THOMAS DR ,  KEIL KARL-HEINZ DR ,  KARSUNKY ULRICH ,  STERNBERGER KLAUS

    IPC: D06P1/54 ,  D06P1/44 ,  D06P1/52 ,  D06P1/66 ,  D06P3/60 ,  D06P5/00 ,  D06P5/22

    Abstract: Process for dyeing textile material with pigment dyes, which comprises 1. pretreating the textile material with a polymer which consists wholly or partly of monomeric units of the formula I (I) where R1 and R2 are each hydrogen, (C1-C22)alkyl which may be interrupted by -CO-NH- or -NH-CO-, or C1-C4-hydroxyalkyl, R3 and R4 are each hydrogen or methyl, and Y-is a monovalent anion or one equivalent of a polyvalent anion, 2. then dyeing with a pigment dye in the presence of a leveling or dispersing agent by the exhaust method and if necessary 3. treating the dyeing in a liquor with a pigment binder and subsequently fixing it. This process makes it possible to dye textile material, in particular ready-made jeans garments, with pigment dyes by an exhaust method.

    19.
    发明专利
    未知

    公开(公告)号：BR9200156A

    公开(公告)日：1992-10-06

    申请号：BR9200156

    申请日：1992-01-17

    Applicant: HOECHST AG

    Inventor： MARTINI THOMAS DR ,  KEIL KARL-HEINZ DR ,  WIMMER IGNAZ

    IPC: C09K23/24 ,  B01J13/00 ,  C09K23/00 ,  C11D1/12 ,  C11D1/18 ,  C11D1/28 ,  C11D1/52 ,  C11D1/66 ,  C11D1/72 ,  C11D1/74 ,  C11D1/83 ,  C11D1/86

    Abstract: Stable and homogeneous aqueous formulations of surfactants with an HLB of less than or equal to 13, which additionally contain a compound of the formula I in which R is C1-C8-alkyl, C1-C8-alkenyl, phenyl, alkylphenyl or phenalkyl with, in each case, 1 to 4 C atoms in the alkyl chain or cyclohexyl, R is hydrogen, or one of the radicals mentioned for R or R and R together with the N atom denote a heterocyclic radical, M is an alkali metal or ammonium cation or an equivalent of an alkaline earth or aluminium cation, and m and n are each, independently of one another, numbers from 6 to 8. The presence of the compounds of the formula I makes it possible to prepare stable and homogeneous aqueous formulations even of those surfactants which are otherwise only sparingly soluble or even insoluble in water.

    20.
    发明专利
    未知

    公开(公告)号：DE3617451A1

    公开(公告)日：1987-11-26

    申请号：DE3617451

    申请日：1986-05-23

    Applicant: HOECHST AG

    Inventor： SCHINZEL ERICH DR ,  FRISCHKORN HANS DR ,  MARTINI THOMAS DR

    IPC: C07D263/62 ,  C07D263/64 ,  D06L3/12

    Abstract: Compounds of the general formula (1) in which n denotes 1 or 2, X denotes an OMe group, Me denotes a proton, an alkali metal cation or an optionally substituted ammonium cation, R denotes hydrogen, a lower alkyl group or halogen, and, in the event that n is 1, X also denotes an -NR1R2 group in which R1 and R2 represent hydrogen or a lower alkyl group, a process for their preparation and their use as optical brighteners, especially for polyamide fibers and wool.

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