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公开(公告)号：JP2003252829A
公开(公告)日：2003-09-10
申请号：JP2002056097
申请日：2002-03-01
Applicant: KAO CORP
Inventor： SAWADA HIROKI , HASHIMOTO JIRO , OKA KOJI , MAEDA TOSHIJI
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing a monoglyceride directly from glycerol and a fatty acid in the absence of a catalyst without using an expensive concentration apparatus such as a molecular still, in a short time, with which a product having a high content of ≥55 wt.% monoglyceride is obtained. SOLUTION: The method for producing the monoglyceride by reacting glycerol with a fatty acid in the absence of a catalyst comprises mixing operation of glycerol and a fatty acid in which the peripheral speed of the tip of the blade of a stirrer is ≥3 m/s and the number of passes is ≥0.1 time/h. COPYRIGHT: (C)2003,JPO
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公开(公告)号：JPH0971595A
公开(公告)日：1997-03-18
申请号：JP23128995
申请日：1995-09-08
Applicant: KAO CORP
Inventor： OKA KOJI , TATE KENICHI
Abstract: PROBLEM TO BE SOLVED: To produce an alkyl glycoside which is a low-irritating nonionic surfactant and capable of acting as a foam stabilizer, etc., for an anionic surfactant in a short time by reacting a sugar with a higher alcohol in the presence of an acidic catalyst while applying ultrasonic waves to the reactional mixture. SOLUTION: A reactional vessel 1 having an external circulating line 8 equipped with an ultrasonic generator 2, an ultrasonic application chamber 3 and a rotary pump 4 is charged with a sugar such as glucose, a higher alcohol comprising a mixture, etc., of decyl alcohol with lauryl alcohol and myristyl alcohol and an acidic catalyst such as p-toluenesulfonic acid and the circulation is started to start the application of ultrasonic waves. The pressure in the system is decompressed with a vacuum device to start the heat-up. Water produced by the reaction is efficiently removed to carry out the reaction. Thereby, the objective alkyl glycoside which is a low-irritating nonionic surfactant and capable of not only producing stable bubbles by itself but also acting as a foam stabilizer on an anionic surfactant is obtained by the reaction in a short time.
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公开(公告)号：JPH06336492A
公开(公告)日：1994-12-06
申请号：JP12593893
申请日：1993-05-27
Applicant: KAO CORP
Inventor： SHIBATA KENGO , OKA KOJI , AIMONO KIYOSHI
Abstract: PURPOSE:To provide a method for fractionating a sucrose fatty acid ester having a specific composition from a reaction mixture of sucrose fatty acid esters by a simple operation without using an organic solvent. CONSTITUTION:Sucrose fatty acid esters composed of a mixture of [SME], [SDE] and [SPE] ([SME] is a sucrose fatty acid ester having 1 ester exchange degree, [SDE] is a sucrose fatty acid ester having 2 ester exchange degree and [SPE] is a sucrose fatty 7 acid ester having >=3 ester exchange degree) are mixed with fats and oils under heating and the prepared heated mixture is incorporated with water to extract a sucrose fatty acid ester having high [SME] content. The prepared water phase and the oil phase are separated to give a sucrose fatty acid ester having high [SME] content and sucrose fatty acid esters having high [SDE] and [SPE] contents.
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公开(公告)号：JP2005120036A
公开(公告)日：2005-05-12
申请号：JP2003357849
申请日：2003-10-17
Inventor： SHIRASAWA TAKESHI , MAEDA TOSHIJI , OKA KOJI
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing fully deodorized glyceryl ether.
SOLUTION: The method for producing the glyceryl ether comprises a step (1) of subjecting glycidyl ether to hydrolysis reaction to form glyceryl ether, a step (2) of adjusting the acid value of the reaction solution to -400 to 0 mmol/kg, and a step (3) of distilling the reaction solution to obtain glyceryl ether.
COPYRIGHT: (C)2005,JPO&NCIPIAbstract translation: 要解决的问题：提供一种完全除臭的甘油醚的制备方法。 解决方案：制备甘油醚的方法包括使缩水甘油醚进行水解反应以形成甘油醚的步骤（1），将反应溶液的酸值调节至-400至0mmol的步骤（2） / kg，以及蒸馏反应溶液以获得甘油醚的步骤（3）。 版权所有（C）2005，JPO＆NCIPI
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公开(公告)号：JPH11124391A
公开(公告)日：1999-05-11
申请号：JP28807997
申请日：1997-10-21
Applicant: KAO CORP
Inventor： OKA KOJI
IPC: C07H15/04
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an alkyl glycoside by which an alkyl glycoside is decolored to a light color and the alkyl glycoside good in hue as an ingredient of a shampoo or the like is obtained. SOLUTION: This method for producing an alkyl glycoside comprises irradiating an alkyl glycoside having
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Patent Agency Ranking
公开(公告)号：JPH06319973A
公开(公告)日：1994-11-22
申请号：JP11192093
申请日：1993-05-13
Applicant: KAO CORP
Inventor： OKA KOJI , MAEDA TOSHIJI , AIMONO KIYOSHI
Abstract: PURPOSE:To provide a method for preparation of a surfactant wherein impurities which causes change of smell for the worse, deterioration of hue and irritation can be extracted and eliminated efficiently by using an extractant (an extracting solvent) and an inexpensive apparatus and a surfactant with a high quality can be obtd. CONSTITUTION:The title method has a purification process wherein a water soln. of a surfactant contg. a component to be extracted is fed from a tower head part 5A of an extracting apparatus having a cylindrical extracting tower 1A and a plurality of perforated plates 2A arranged horizontally and in the longitudinal direction in the extracting tower 1A and an extractant for extracting a component to be extracted is fed from the tower bottom part 6A and extraction of the component to be extracted is performed while the interfacial position between the water soln. of the surfactant and the extractant is controlled so as to be kept it below the middle stage perforated plate 2A among the plurality of perforated plates 2A.
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公开(公告)号：JPH04308599A
公开(公告)日：1992-10-30
申请号：JP7148191
申请日：1991-04-04
Applicant: KAO CORP
Inventor： TSUYUTANI SHINJI , AIMONO KIYOSHI , OKA KOJI
IPC: C07H15/04
Abstract: PURPOSE:To obtain the title compound useful for low-irritating surfactant without deterioration of smell by reacting a sugar with a higher alcohol while irradiating the reaction system with light having specific wavelength, and then carrying out removal of unreacted higher alcohol and decoloration by light irradiation. CONSTITUTION:When a sugar is reacted with a higher alcohol or the sugar is firstly reacted with a lower alcohol and then reacted with a higher alcohol to produce an alkylglycoside, the above-mentioned reaction is carried out while irradiating the reaction system with light having 100-800nm wavelength, and unreacted higher alcohol is removed from the resultant unreacted higher alcohol- containing alkylglycoside or the unreacted higher alcohol-containing alkylglycoside is once more irradiated with light having 100-800nm wavelength and then unreacted higher alcohol is removed, or an alkylglycoside solution after removing unreacted higher alcohol is irradiated with light having 100-800nm wavelength to provide the objective decolored alkylglycoside having good hue.
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公开(公告)号：JPH04224598A
公开(公告)日：1992-08-13
申请号：JP40660990
申请日：1990-12-26
Applicant: KAO CORP
Inventor： OKA KOJI , AIMONO KIYOSHI , TSUYUTANI SHINJI , FUJITA TADAAKI
IPC: C07H15/04
Abstract: PURPOSE:To improve productivity by producing a high-quality alkylglycoside excellent in hue and recycling separated unreacted sugar for the reaction. CONSTITUTION:In production of an alkylglycoside using a sugar and a higher alcohol, the sugar is reacted with the higher alcohol using an acid catalyst and unreacted solid sugar is subsequently separated from a reaction mixture containing the unreacted solid sugar. The resultant clean reaction solution is further subjected to an aging reaction using a thin membrane reactor, etc., thus giving the objective alkylglycoside containing
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公开(公告)号：JP2006111575A
公开(公告)日：2006-04-27
申请号：JP2004300726
申请日：2004-10-14
Inventor： SHIRASAWA TAKESHI , TANAHASHI SHINICHIRO , OKA KOJI
IPC: C07D301/26 , C07D303/22
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing a high-purity glycidyl ether of good layer separability, enabling byproducts formation leading to the final product's quality deterioration to be reduced.
SOLUTION: The method for producing the glycidyl ether comprises the following process: A specified halohydrin ether as a compound of the general formula(I) and an alkali-containing aqueous solution are made to flow through a flow path with a cross-section area of 300-50,000μm
2 to carry out a reaction under the mutual contact of the compound and the alkali with each other.
COPYRIGHT: (C)2006,JPO&NCIPIAbstract translation: 要解决的问题：为了提供具有良好的层分离性的高纯度缩水甘油醚的制备方法，能够使副产物形成导致最终产品的质量劣化降低。 解决方案：制备缩水甘油醚的方法包括以下方法：使具有通式（I）的化合物的特定的卤代醇醚和含碱的水溶液流过具有交联剂的流路， 截面积为300-50,000μm
2 ，在化合物和碱的相互接触下进行反应。 版权所有（C）2006，JPO＆NCIPI -
公开(公告)号：JP2006111574A
公开(公告)日：2006-04-27
申请号：JP2004300723
申请日：2004-10-14
Inventor： SHIRASAWA TAKESHI , TANAHASHI SHINICHIRO , OKA KOJI
Abstract: PROBLEM TO BE SOLVED: To provide a method for easily producing the ring-opened product of an epoxy compound in high yield through preventing superheating by the heat of reaction and suppressing side reactions.
SOLUTION: The method comprises the following process: The epoxy compound and a hydroxy group-containing compound are made to flow through a flow path with a cross-section area of of 300-1,000,000μm
2 to bring both the compounds into contact with each other to carry out a ring-opening addition reaction.
COPYRIGHT: (C)2006,JPO&NCIPIAbstract translation: 待解决的问题：提供一种通过防止反应热过度并抑制副反应而容易地以高产率制备环氧化合物的开环产物的方法。 解决方案：该方法包括以下方法：使环氧化合物和含羟基化合物流过横截面积为300-1,000,000μm
2 的流路， 使两种化合物彼此接触以进行开环加成反应。 版权所有（C）2006，JPO＆NCIPI
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