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    Process for the preparation of mixtures of dinitroanthraquinones with a high content of 1,5- and 1,8- dinitroanthraquinone
    231.
    发明授权
    Process for the preparation of mixtures of dinitroanthraquinones with a high content of 1,5- and 1,8- dinitroanthraquinone 失效
    制备二硝基蒽醌与高含量1,5-和1,8-二硝基蒽醌的混合物的方法

    公开(公告)号：US4259248A

    公开(公告)日：1981-03-31

    申请号：US49708

    申请日：1979-06-18

    Applicant: Walter Hohmann ,  Klaus Wunderlich

    Inventor： Walter Hohmann ,  Klaus Wunderlich

    IPC: C07C205/47 ,  C07C20060101 ,  C07C67/00 ,  C07C201/00 ,  C07C97/12

    CPC classification number: C07C225/34

    Abstract: A process has been developed for the preparation of mixtures of dinitroanthraquinones with a high content of 1,5- and 1,8- dinitroanthraquinone by nitration with nitric acid in the presence of sulphuric acid with heating wherein anthraquinone, 1-nitroanthraquinone or a mixture of them is treated with about 1.5 to about 2.5 times the amount by weight of nitric acid, relative to the feed material, in the presence of about 0.75 times to twice the amount by weight, relative to nitric acid, of sulphuric acid, the temperature first being kept in the range from room temperature to about 50.degree. C. until at least 50% of the starting material or materials has been dinitrated, then adjusting the temperature to about 50.degree. C. to about 70.degree. C. to complete the dinitration.

    Abstract translation: 已经开发了一种通过硝酸在硫酸存在下通过加热制备二硝基蒽醌与高含量1,5-和1,8-二硝基蒽醌的混合物的方法，其中蒽醌，1-硝基蒽醌或 在相对于原料的硝酸的量的约1.5至约2.5倍的条件下，相对于硝酸，硫酸的重量的约0.75倍至2倍的量处理它们，温度先 保持在室温至约50℃的范围内，直到起始材料或材料的至少50％已被硝化，然后将温度调节至约50℃至约70℃以完成二硝化。

    Process for producing phenoxycarboxylic acid derivative
    232.
    发明授权
    Process for producing phenoxycarboxylic acid derivative 失效
    生产苯氧基羧酸衍生物的方法

    公开(公告)号：US4254262A

    公开(公告)日：1981-03-03

    申请号：US84164

    申请日：1979-10-12

    Applicant: Wataro Koike ,  Tadashi Sasuga ,  Chihiro Yazawa

    Inventor： Wataro Koike ,  Tadashi Sasuga ,  Chihiro Yazawa

    IPC: C07C69/66 ,  A01N37/10 ,  B01J31/00 ,  C07B61/00 ,  C07C51/00 ,  C07C51/367 ,  C07C59/125 ,  C07C59/60 ,  C07C59/68 ,  C07C59/70 ,  C07C67/00 ,  C07C69/612 ,  C07C201/00 ,  C07C205/38 ,  C07C253/00 ,  C07C255/54 ,  C07D213/57 ,  C07C61/08 ,  C07C69/767

    CPC classification number: C07C51/367

    Abstract: A phenoxycarboxylic acid derivative having the formula ##STR1## wherein R represents ##STR2## and X.sub.1 represents a hydrogen atom, a halogen atom, a lower alkyl group, trifluoromethyl group, nitro group or cyano group and X.sub.2 represents a hydrogen atom, a halogen atom, a lower alkyl group, nitro group or cyano group, R' represents ##STR3## and R.sub.1 and R.sub.2 are the same and different and respectively represent hydrogen atom or a lower alkyl group, is produced by reacting a phenol compound having the formula ##STR4## with a halogen compound havingX--R'wherein X represents a halogen atom in the presence of a base. The reaction is carried out in the presence of a quarternary ammonium salt or a quaternary phosphonium salt in a nonpolar solvent.

    Abstract translation: 具有下式的式（III）的苯氧基羧酸衍生物，其中R表示“IMA”，X 1表示氢原子，卤素原子，低级烷基，三氟甲基，硝基或氰基，X 2表示氢原子， 卤素原子，低级烷基，硝基或氰基，R'表示“IMA”，R1和R2相同且不同，分别表示氢原子或低级烷基，是通过使苯酚 具有式（I）的化合物与具有XR'的卤素化合物反应，其中X表示卤素原子。 反应在非极性溶剂中在季铵盐或季鏻盐存在下进行。

    3-Benzoyl-2-nitrophenylacetic acids, metal salts, amides and esters
    233.
    发明授权
    3-Benzoyl-2-nitrophenylacetic acids, metal salts, amides and esters 失效
    3-苯甲酰基-2-硝基苯基乙酸，金属盐，酰胺和酯

    公开(公告)号：US4254146A

    公开(公告)日：1981-03-03

    申请号：US86195

    申请日：1979-10-18

    Applicant: David A. Walsh

    Inventor： David A. Walsh

    IPC: A61K31/165 ,  A61K31/12 ,  A61K31/19 ,  A61K31/195 ,  A61K31/215 ,  A61K31/24 ,  A61P29/00 ,  C07C67/00 ,  C07C201/00 ,  C07C205/56 ,  C07C233/00 ,  C07C233/11 ,  C07C235/78 ,  C07C79/46

    CPC classification number: C07C205/56 ,  C07C205/45

    Abstract: 3-Benzoyl-2-nitrophenylacetic acids, metal salts, amides and esters are disclosed having the formula: ##STR1## wherein R.sub.1 is hydrogen or lower alkyl; R.sub.2 is OH, OM, O-lower alkyl, NH.sub.2, NH-lower alkyl or N,N-dilower alkyl; X is hydrogen, halogen, lower alkyl, lower alkoxy, trifluoromethyl or nitro and M is a pharmaceutically acceptable cation or a fraction thereof when the cation is multivalent, hydrates thereof and n is 1-3 inclusive. The compounds have anti-inflammatory activity and methods and pharmaceutical compositions for use thereof are disclosed.

    Abstract translation: 公开了具有下式的3-苯甲酰基-2-硝基苯基乙酸，金属盐，酰胺和酯：其中R 1是氢或低级烷基; R2是OH，OM，O-低级烷基，NH2，NH-低级烷基或N，N-二氟烷基; X为氢，卤素，低级烷基，低级烷氧基，三氟甲基或硝基，当阳离子为多价时，M为药学上可接受的阳离子或其分数，其水合物为n为1-3。 该化合物具有抗炎活性，并且公开了用于其的方法和药物组合物。

    Phenoxyphenoxyalkanecarboxylic acid esters
    235.
    发明授权
    Phenoxyphenoxyalkanecarboxylic acid esters 失效
    苯氧基苯氧基羧酸酯

    公开(公告)号：US4221581A

    公开(公告)日：1980-09-09

    申请号：US953236

    申请日：1978-10-20

    Applicant: Otto Rohr ,  Georg Pissiotas ,  BoBeat

    Inventor： Otto Rohr ,  Georg Pissiotas ,  BoBeat

    IPC: A01N39/02 ,  A01N39/04 ,  C07C67/00 ,  C07C201/00 ,  C07C205/38 ,  C07C253/00 ,  C07C255/53 ,  C07C255/54 ,  C07C325/00 ,  C07C327/22 ,  C07D241/10 ,  A01N9/12 ,  A01N9/20 ,  A01N9/24

    CPC classification number: C07C205/38 ,  A01N39/02 ,  A01N39/04 ,  C07C327/00

    Abstract: The present invention relates to novel herbicidally active phenoxyphenoxyalkanecarboxylic acid esters, compositions which contain these compounds as active ingredient, and a method of selectively controlling weeds in crops of cultivated plants or of regulating plant growth which comprises the use of these compounds.The phenoxyphenoxyalkanecarboxylic acid esters have the formula ##STR1## wherein R.sub.1 is hydrogen, halogen or cyano,R.sub.2 is hydrogen or lower alkyl,R.sub.3 is a radical OR.sub.4 or SR.sub.5,R.sub.4 is a substituted alkyl radical, an alkenyl, alkynyl, cycloalkyl radical, a substituted or unsubstituted phenyl or benzyl radical or a 5- to 6-membered heterocyclic radical, andR.sub.5 is an unsubstituted alkyl radical or has the same meaning as R.sub.4.

    Abstract translation: 本发明涉及新颖的除草活性苯氧基苯氧基羧酸酯，其含有这些化合物作为活性成分的组合物，以及选择性地控制栽培植物作物或调节植物生长的杂草的方法，其包括使用这些化合物。 苯氧基苯氧基羧酸酯具有下式：其中R 1是氢，卤素或氰基，R 2是氢或低级烷基，R 3是基团OR 4或SR 5，R 4是取代的烷基，烯基，炔基，环烷基， 取代或未取代的苯基或苄基或5-至6-元杂环基，R 5为未取代的烷基或具有与R 4相同的含义。

    Process for the manufacture of indigoid dyes
    237.
    发明授权
    Process for the manufacture of indigoid dyes 失效
    靛蓝染料的制造方法

    公开(公告)号：US4151170A

    公开(公告)日：1979-04-24

    申请号：US751223

    申请日：1976-12-16

    Applicant: Jacques Gosteli

    Inventor： Jacques Gosteli

    IPC: C09B7/00 ,  C07C67/00 ,  C07C201/00 ,  C07C205/45 ,  C09B7/02 ,  D06P1/28 ,  D06P3/60

    CPC classification number: C09B7/02

    Abstract: A process for the manufacture of indigoid dyes, wherein a functional derivative of the anthranilic acid of the general formula I ##STR1## in which A completes a mono- or polynuclear, substituted or unsubstituted aromatic ring,X represents a hydrogen atom or a protective group for the free amino group which can form an anhydro derivative with the carboxyl group in the ortho-position,Is reacted with nitromethane in the presence of a base or with a salt of nitroacetic acid to give the .omega.-nitro-o-amino-acetophenone derivative of the general formula II ##STR2## in which A and X are as defined in formula I, and this intermediate is condensed by heating with acids to give the indigo compound of the general formula III ##STR3## in which A is as defined in formula I.

    Abstract translation: 靛蓝染料的制备方法，其中通式Ⅰ的邻氨基苯甲酸的功能性衍生物（I）其中A完成单或多核，取代或未取代的芳环，X表示氢原子或 可以在邻位形成具有羧基的脱水衍生物的游离氨基的保护基，在碱存在或与硝酸盐存在下与硝基甲苯反应以产生ω-NITRO-O- 其中A和X如式I所定义的通式II（II）的氨基 - 乙炔酮衍生物，并且该中间体通过与酸加热而缩合，得到通式III的靛蓝化合物（IMAGE）（ III）其中A如式I所定义。

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