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    23.
    发明专利
    未知

    公开(公告)号：BR0313247A

    公开(公告)日：2005-07-12

    申请号：BR0313247

    申请日：2003-07-30

    Applicant: BASF AG

    Inventor： ADAMI CHRISTOPH ,  KARL JOERN ,  HAUK ALEXANDER ,  BOEHLING RALF ,  PASTRE JOERG ,  LENZ ROBERT

    IPC: C07C51/09 ,  C07C51/43 ,  C07C51/44 ,  C07C53/02 ,  C07C53/06 ,  A23K3/03 ,  A23L1/304 ,  A61L9/00

    Abstract: A method for the production of formic acid-formates (I) involves (a) partial hydrolysis of methyl formate (MF) with water, (b) distillation to give formic acid and water (stream S1) and (c) combination of (S1) with the corresponding formate (F) to give a mixture of (I) and water. An Independent claim is also included for apparatus for the production of (I), comprising a reactor (A) for the hydrolysis of MF, a distillation column (B) for separating a stream containing MF, formic acid, methanol and water into MF, methanol and a stream (S1) containing formic acid and water, and a column (E) for removing water from S1.

    24.
    发明专利
    未知

    公开(公告)号：NO20050534L

    公开(公告)日：2005-03-02

    申请号：NO20050534

    申请日：2005-01-31

    Applicant: BASF AG

    Inventor： PASTRE JORG ,  KARL JORN ,  ADAMI CHRISTOPH ,  HAUK ALEXANDER ,  LENZ ROBERT ,  BOHLING RALF

    IPC: C07C51/09 ,  C07C51/43 ,  C07C51/44 ,  A23K3/03

    Abstract: A method for the production of formic acid-formates (I) involves (a) partial hydrolysis of methyl formate (MF) with water, (b) distillation to give formic acid and water (stream S1) and (c) combination of (S1) with the corresponding formate (F) to give a mixture of (I) and water. An Independent claim is also included for apparatus for the production of (I), comprising a reactor (A) for the hydrolysis of MF, a distillation column (B) for separating a stream containing MF, formic acid, methanol and water into MF, methanol and a stream (S1) containing formic acid and water, and a column (E) for removing water from S1.

    26.
    发明专利
    未知

    公开(公告)号：BR0308912A

    公开(公告)日：2005-01-04

    申请号：BR0308912

    申请日：2003-04-15

    Applicant: BASF AG

    Inventor： ADAMI CHRISTOPH ,  SLANY MICHAEL ,  KARL J RN ,  KAIBEL GERD ,  SCHOFER MARTIN ,  ZEHNER PETER ,  PER MICHAEL R

    IPC: C07C67/36 ,  C07C69/06

    Abstract: The invention relates to a process for the preparation of methyl formate by reacting methanol with carbon monoxide at a pressure of from 0.5 to 10 MPa abs. and a temperature of from 50 to 150° C. in the presence of a metal alkoxide as catalyst in a reactor, in which a gas stream is withdrawn from the reactor, entrained methyl formate is removed from this gas stream by condensation, and all or some of the remaining gas stream is returned to the reactor as circulating-gas stream and a mean gas superficial velocity of from 1 to 20 cm/s is set in at least one region of the reactor in which the gas flows essentially in one direction.

    27.
    发明专利
    未知

    公开(公告)号：DE10321733A1

    公开(公告)日：2004-12-02

    申请号：DE10321733

    申请日：2003-05-14

    Applicant: BASF AG

    Inventor： HAUK ALEXANDER ,  ADAMI CHRISTOPH ,  KARL JOERN ,  LENZ ROBERT

    IPC: C07C51/41 ,  C07C53/06

    Abstract: A process is proposed for preparing acid formates by providing a liquid stream I containing formic acid and a liquid stream II containing a metal formate, and mixing the liquid stream I with the liquid stream II, obtaining the corresponding acid formate, which comprises feeding, to the liquid stream I or a precursor thereof, to the liquid stream II or a precursor thereof, or to the mixture of the liquid streams I and II, a liquid stream III containing the following components at contents of in each case >0.1% by weight: metal formate, metal methoxide, methanol and MeFo (MeFo), which is produced in a process for preparing MeFo by carbonylating methanol in a reactor at a pressure up to 50 MPa absolute in the presence of a metal methoxide as homogeneous catalyst.

    Heterogeneously catalyzed gas-phase partial oxidation of acrolein to acrylic acid, used to produce polymers for adhesives, involves using active multimetal oxide material containing e.g. molybdenum and vanadium
    29.
    发明专利
    Heterogeneously catalyzed gas-phase partial oxidation of acrolein to acrylic acid, used to produce polymers for adhesives, involves using active multimetal oxide material containing e.g. molybdenum and vanadium 未知

    公开(公告)号：DE10246119A1

    公开(公告)日：2004-04-15

    申请号：DE10246119

    申请日：2002-10-01

    Applicant: BASF AG

    Inventor： HECHLER CLAUS ,  SCHINDLER GOETZ-PETER ,  PETZOLDT JOCHEN ,  ADAMI CHRISTOPH ,  MACHHAMMER OTTO ,  MUELLER-ENGEL KLAUS JOACHIM ,  MARTAN HANS

    IPC: C07C47/22 ,  C07C57/04 ,  C07C253/18 ,  C07C255/08 ,  C07D301/08 ,  C07D303/04

    Abstract: A heterogeneously catalyzed gas-phase partial oxidation of acrolein to acrylic acid over a catalytically active multimetal oxide material which contains the elements molybdenum and vanadium, tellurium or antimony, and elements consisting of niobium, tantalum, tungsten or titanium, whose X-ray diffraction pattern has no reflections with the peak position 2 theta = 50 +/- 0.30 but has reflections whose peaks are at specified diffraction angles. Heterogeneously catalyzed gas-phase partial oxidation of acrolein to acrylic acid over a catalytically active multimetal oxide material which contains the elements molybdenum and vanadium, tellurium or antimony, and elements consisting of niobium, tantalum, tungsten or titanium, whose X-ray diffraction pattern has no reflections with the peak position 2 theta = 50 +/- 0.30 but has reflections h, i and k whose peaks are at the diffraction angles (2 theta) 22.2 +/- 0.5 degrees (h), 27.3 +/- 0.50 (i) and 28.2 +/- 0.50 (k). The reflection (h ) is the one with the strongest intensity within the X-ray diffraction pattern and having a full width at half height of not more than 0.50; the intensity (Pi) of the reflection (i) and the intensity (Pk) of the reflection (k) fulfill the relationship that R is 0.65-0.85, where R is the intensity ratio defined by the formula R = Pi/(Pi + Pk); and the full width at half height of the reflection (i) and of the reflection (k) is in each case at most 10. The catalytically active multimetal oxide material is of formula (I). Mo1VaM1bM2cM3dOn (I). M1 = element(s) from the group consisting of Te and Sb; M2 = element(s) from the group consisting of Nb, Ti, W, Ta and Ce; M3 = element(s) consisting of Pb, Ni, Co, Bi, Pd, Ag, Pt, Cu, Au, Ga, Zn, Sn, In, Re, Ir, Sm, Sc, Y, Pr, Nd or Tb; a = 0.01-1; b = 0-1; c = 0-1; d = 0-0.5; n = number that is determined by the valency and frequency of the elements other than oxygen in formula (I).

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