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    22.
    发明专利
    未知

    公开(公告)号：DE10358799A1

    公开(公告)日：2005-07-14

    申请号：DE10358799

    申请日：2003-12-12

    Applicant: BASF AG

    Inventor： ANGEL MAXIMILIAN ,  BOUILLO NATHALIE ,  LANGE RONALD FRANS MARIA ,  SCHAEFER ANDRE

    IPC: A61K9/48 ,  C08F216/06 ,  C08F218/04 ,  C08F220/28 ,  C08F261/04 ,  C08F271/02 ,  B01J13/14

    Abstract: The invention relates to hard capsules produced from water-dispersible copolymers (A), wherein the copolymers are obtained by radically initiated polymerization of 20 to 80 weight percent of a monomer mixture consisting of i) 50 to 100 weight percent hydroxy-C1-C6-alkyl(meth); ii) 0 to 50 weight % of one or more compounds of formula (I) or (II) wherein R = C1-C6-Alkyl, R2 = H, CH3, R3 = C1-C24-Alkyl; iii) optionally 0 to 20 weight percent of other polymerizable compounds, in the presence of 20 to 80 weight percent polyvinyl alcohol or polyvinylpyrrolidone or mixtures thereof, with the proviso that the sum of i), ii) and iii) equals 100 weight percent.

    Preparation of water soluble or dispersible copolymer, useful as solubilizer for the preparation of the aqueous active or effective composition, comprises polymerizing a polymer with an anhydride reactive group and an amide compound
    23.
    发明专利
    Preparation of water soluble or dispersible copolymer, useful as solubilizer for the preparation of the aqueous active or effective composition, comprises polymerizing a polymer with an anhydride reactive group and an amide compound 未知

    公开(公告)号：DE102005026711A1

    公开(公告)日：2007-02-01

    申请号：DE102005026711

    申请日：2005-06-09

    Applicant: BASF AG

    Inventor： DIETSCHE FRANK ,  BOUILLO NATHALIE ,  HUEFFER STEPHAN ,  LANGE RONALD FRANS MARIA ,  PINNEKER OLGA ,  DROHMANN CHRISTIAN

    IPC: C08F299/00 ,  A61K8/06 ,  A61K8/81 ,  C08F2/00 ,  C08F210/10 ,  C08F226/00 ,  C09K23/52

    Abstract: Preparation of water soluble or water dispersible copolymer comprises either polymerizing at least a polymer (P1) having at least an anhydride reactive group, and at least a compound containing alpha , beta -ethylenically unsaturated amide group, or reacting at least a hydrolysis product of P1 with a polyolefin (P2) containing at least a anhydride group, where the reaction step takes place using a shear force. Preparation of water soluble or water dispersible copolymer comprises either polymerizing at least a polymer (P1) having at least an anhydride reactive group, and at least a compound (M1) containing alpha , beta -ethylenically unsaturated amide group of formula (R1>-C(=O)-NR2>R3>), or reacting at least a hydrolysis product of P1 with a polyolefin (P2) containing at least a anhydride group, where the reaction step takes place using a shear force. R2>CH2=CR4>; R4>H or 1-4C-alkyl; and either R1>, R3>H, (cyclo)alkyl, heterocycloalkyl or (hetero)aryl; or R1>R3>NH2lactam with 5 to 8 ring atoms. Independent claims are included for: (1) the copolymer obtained by the above process; (2) an active or effective composition comprising the copolymer and at least an active or effective material with an solubility of 10 g/l in water at 25[deg]C and 1013 mbar; (3) a method for the preparation of the aqueous active or effective composition comprising either preparing homogeneous, non-aqueous mixture containing the copolymer and the active or effective material and dispersing the obtained mixture in water, or preparing a solution of the active or effective material and the copolymer in an organic solvent having boiling point less than water, mixing the obtained mixture and removing the organic agent, or preparing the active or effective material in an aqueous solution copolymer at a temperature above the melt temperature of the active agent; and (4) a cosmetic, pharmaceutical or plant protective agent comprising the copolymer, at least the cosmetic active or effective material and optionally at least an auxiliary material.

    Surface-modified metal oxides, method for production and use thereof in cosmetic preparations
    24.
    发明专利
    Surface-modified metal oxides, method for production and use thereof in cosmetic preparations 未知

    公开(公告)号：AU2006254151A1

    公开(公告)日：2006-12-07

    申请号：AU2006254151

    申请日：2006-05-30

    Applicant: BASF AG

    Inventor： RIEGER JENS ,  KISSEL JUTTA ,  BOUILLO NATHALIE ,  ANDRE VALERIE

    IPC: C09C3/10 ,  A61K8/27 ,  A61K8/29 ,  A61Q17/04 ,  C09C1/04 ,  C09C1/24 ,  C09C1/36 ,  C09C1/40

    Abstract: The present invention relates to surface-modified nanoparticulate metal oxides where the metal is chosen from the group consisting of aluminum, cerium, iron, titanium, zinc and zirconium, wherein the surface modification comprises a coating with a copolymer P comprising, as monomers, A) 1 to 99 mol % of a N-vinylamide N-vinylpyrrolidone and B) 99 to 1 mol % of a monomer comprising, per molecule, a free-radically polymerizable α,&bgr;-ethylenically unsaturated double bond and an anionogenic and/or anionic group, with the proviso that the copolymer P must comprise no further monomers chosen from the group consisting of C8-C30-alkyl esters of monoethylenically unsaturated C3-C8-carboxylic acids, N-alkyl- or N,N-dialkyl-substituted amides of acrylic acid or of methacrylic acid with C8-C18-alkyl radicals, or vinyl esters of aliphatic C8-C30-carboxylic acids.

    25.
    发明专利
    未知

    公开(公告)号：DE102004058952A1

    公开(公告)日：2006-06-14

    申请号：DE102004058952

    申请日：2004-12-07

    Applicant: BASF AG

    Inventor： BOUILLO NATHALIE ,  ROESLER GERHARD

    IPC: C08F2/04 ,  A61K8/81 ,  A61K9/32 ,  A61K47/32 ,  C08F2/06 ,  C08F2/10 ,  C08F6/24 ,  C08F220/10 ,  C08F220/56 ,  C08F226/02 ,  C08F226/06 ,  C08J3/12

    Abstract: Production (P1) of aqueous secondary dispersions of water-insoluble copolymers involves providing monomer (M) comprising monoethylenically unsaturated monomer and hydrophilic, monoethylenically unsaturated, nonionic monomer, in an organic, water-miscible solvent; and replacing the solvent by water, where toward the end of the polymerization, composition of hydrophilic, monoethylenically unsaturated, nonionic monomer is added. Production (P1) of aqueous secondary dispersions of water-insoluble copolymers involves: (A) providing ethylenically unsaturated monomers (M) in an organic, water-miscible solvent or in a mixture of water with an organic, water-miscible solvent as a free-radical polymerization medium. (M) Comprises at least one monoethylenically unsaturated monomer (M1) with a solubility in water of not > 30 g/l at 25[deg]C and 1 bar, and at least one hydrophilic, monoethylenically unsaturated, nonionic monomer with a solubility in water of at least 80 g/l at 25[deg]C and 1 bar; and (B) removing the organic solvent and adding water, where toward the end of the polymerization of step (A), a monomer composition comprising at least one hydrophilic, monoethylenically unsaturated, nonionic monomer is added to the polymerization medium. An independent claim is included for producing (P2) aqueous secondary dispersions of water-insoluble polymers, where the polymers are produced by free-radical polymerization of ethylenically unsaturated monomer (M) involving: i) adding at least one monoethylenically unsaturated monomer with a solubility of not > 10 g/l at 25[deg]C in water and 1 bar, and at least one hydrophilic, monoethylenically unsaturated, nonionic monomer with a solubility of at least 80 g/l at 25[deg]C in water and 1 bar, to an organic, water-miscible solvent or a mixture of water and an organic, water-miscible solvent, where 85 - 97 wt.% of (M) is added to provide a primary polymerization medium; ii) providing a monomer composition comprising one hydrophilic, monoethylenically unsaturated, nonionic monomer (at least 90 wt.%) with a solubility of at least 80 g/l at 25[deg]C and 1 bar in water, and adding the monomer composition to the primary polymerization medium; and iii) removing the organic solvent and adding water following the addition of the monomer composition to the polymerization medium.

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