VERFAHREN ZUR GEWINNUNG EINES ALIPHATISCHEN DIALDEHYD-MONOACETALS
    23.
    发明授权
    VERFAHREN ZUR GEWINNUNG EINES ALIPHATISCHEN DIALDEHYD-MONOACETALS 有权
    程序为获得脂肪二醛单缩醛

    公开(公告)号:EP1567514B1

    公开(公告)日:2008-07-23

    申请号:EP03811775.0

    申请日:2003-11-27

    Applicant: BASF SE

    Abstract: The invention relates to a method for producing a pure aliphatic dialdehyde monoacetal by reacting the corresponding aliphatic dialdehyde or a precursor of the corresponding aliphatic dialdehyde with one or more aliphatic monohydric or polyhydric alcohols, during which water is isolated by distillation while obtaining a reaction mixture that is separated by distillation. The invention is characterized in that the separation by distillation is continuously carried out in a partition column during which pure aliphatic dialdehyde monoacetal is obtained as a side-stream of the partition column or the separation by distillation is continuously carried out in two distillation columns during which crude aliphatic dialdehyde monoacetal is obtained as a side-stream in the first distillation column, the crude aliphatic dialdehyde monoacetal is fed to the second distillation column, and pure aliphatic dialdehyde monoacetal is obtained as a side-stream from the second distillation column.

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