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    METALLCARBAMATE AUS TOLYLENDIAMINEN
    7.
    发明公开
    METALLCARBAMATE AUS TOLYLENDIAMINEN 有权

    公开(公告)号：EP2265573A1

    公开(公告)日：2010-12-29

    申请号：EP09721886.1

    申请日：2009-03-18

    Applicant: BASF SE

    Inventor： LEITNER, Andreas ,  BAUMANN, Robert ,  SIEGEL, Wolfgang

    IPC: C07C271/28

    CPC classification number: C07C269/04 ,  C07C269/06 ,  C07C271/28

    Abstract: The object of the invention is metal carbamates of the general formula (I), where R
    1 and R
    2 are equal or different, and are an alkyl group with 1-18 carbon atoms and where M is an alkali metal atom.

    Abstract translation: 本发明的目的是通式（I）的金属氨基甲酸酯，其中R 1和R 2相同或不同，并且是具有1-18个碳原子的烷基，并且其中M是碱金属原子。

    VERFAHREN ZUR HERSTELLUNG VON 3-PENTENNITRIL DURCH HYDROCYANIERUNG VON 1,3-BUTADIEN
    8.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON 3-PENTENNITRIL DURCH HYDROCYANIERUNG VON 1,3-BUTADIEN 有权
    用于生产3-戊烯腈通过1,3-丁二烯的氢氰化

    公开(公告)号：EP2051960A1

    公开(公告)日：2009-04-29

    申请号：EP07788104.3

    申请日：2007-08-01

    Applicant: BASF SE

    Inventor： HADERLEIN, Gerd ,  ÄCHTNER, Tobias ,  LEITNER, Andreas ,  LUYKEN, Hermann ,  PFAB, Peter ,  SCHEIDEL, Jens ,  HAUNERT, Andrea ,  GENGER, Thomas

    IPC: C07C253/10 ,  C07C255/07

    CPC classification number: C07C253/10 ,  C07C255/07

    Abstract: Distillation of water, 1- and 2 butene and 1,3 butadiene containing a stabilizer in a distillation device K4 to obtain a stream 15 as a bottom product, containing dried 1,3-butadiene, 1- und 2-butene and the stabilizer, and a stream 16 as the top product, containing an azeotropic 1,3-butadiene/water mixture, condensation of the stream 16 in a condenser W, transfer of the obtained condensate (stream 17) in a phase separation device, recycling of the upper liquid phase (stream 18) consisting of 1,3-butadiene as a return flow to column K4 and removal of the lower aqueous phase (stream 19), (a) reaction of stream 15 in a reactor R1 with hydrogen cyanide on at least one catalyst (stream 6a) to obtain stream 1, containing 3-pentenenitrile, 2-methyle-3-butenenitrile, the at least one catalyst, unreacted 1,3-butadiene, 1- and 2-butene and optionally any remaining unreacted hydrogen cyanide, (b) distillation of stream 1 in a distillation device K1 to obtain a stream 2 as a top product, containing the majority of the 1,3-butadiene from stream 1 and to obtain a stream 3 as a bottom product, containing 3- pentenenitrile, the at least one catalyst, 2-methyl 3-butenenitrile, 1- and 2-butene and the remainder of the 1,3 butadiene from stream 1 that was not separated in stream 2, c) distillation of the stream 3 in a distillation device K2 to obtain a stream 5 in a side-tap of the column, said stream containing 3- pentenenitrile and 2-methyl-3-butenenitrile, a stream 6 as bottom product, containing the at least one catalyst and a stream 4 as a top product, d) compression of stream 4 in the compressor V1, separation of a gaseous partial stream 4b containing 1-and 2-butene, transfer of the compressed stream 4a to the condenser W1, common condensation with stream 2 from b) and transfer of the condensate as stream 9, partially as a return flow to column K1 (stream 9b), partially as areturn stream in the reactor R1 (stream 9a) and e) separation of stream 5 by distillation to obtain 3- pentenenitrile and 2-methyl-3-butenenitrile.

    VERBESSERTES VERFAHREN ZUR HERSTELLUNG VON NICKEL(0)-PHOSPHORLIGAND-KOMPLEXEN
    9.
    发明公开
    VERBESSERTES VERFAHREN ZUR HERSTELLUNG VON NICKEL(0)-PHOSPHORLIGAND-KOMPLEXEN 有权
    用于生产镍改进方法（0） - 磷络合物

    公开(公告)号：EP1988998A1

    公开(公告)日：2008-11-12

    申请号：EP07704548.2

    申请日：2007-02-13

    Applicant: BASF SE

    Inventor： HADERLEIN, Gerd ,  AECHTNER, Tobias ,  LEITNER, Andreas ,  PFAB, Peter ,  LUYKEN, Hermann ,  SCHEIDEL, Jens

    IPC: B01J31/24 ,  B01J31/18

    CPC classification number: B01J31/1845 ,  B01J31/24 ,  B01J2231/32 ,  B01J2531/847

    Abstract: Process for producing nickel(0)-phosphorus ligand complexes containing at least one nickel(0) central atom and at least one phosphorus-containing ligand, by reacting a nickel(II) compound with a reducing agent in the presence of the ligand to give a reaction mixture, characterized in that, a) in the reaction the molar ratio of reducing agent:nickel(II) compound is 1:1 to 1000:1, calculated as molar ratio of redox equivalents, b) in the reaction the molar ratio of phosphorus-containing ligand:nickel(II) compound is at most 30:1, calculated as molar ratio of P atoms:Ni atoms, c) in the resultant reaction mixture the nickel(0) content is at most 1.3% by weight, and d) the resultant reaction mixture is extracted by adding at least one dinitrile and at least one hydrocarbon, at least two immiscible phases forming.

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