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公开(公告)号：KR100257133B1
公开(公告)日：2000-05-15
申请号：KR1019980004741
申请日：1998-02-17
Applicant: 한국과학기술연구원
IPC: B01D71/02
Abstract: PURPOSE: Disclosed are an inorganic sinter filtering material containing thermosetting resin and a preparing method thereof. Inorganic particles such as zeolite or white clay and fine powder of thermosetting resin are well mixed to cast to a porous structure material. CONSTITUTION: Zeolite, white clay, charcoal, ferrite, or sand may be used as inorganic material and phenol resin, epoxy resin, melamine resin, or urea resin may also be used as thermosetting resin. The optimal particle size of inorganic material is 5-600μm and the content of resin is 5-50% of the total weight of filtering material. The filtering material is prepared by the following steps: the preparation step of raw materials, a mixing step of materials, and a casting step.
Abstract translation: 目的：公开了含有热固性树脂的无机烧结过滤材料及其制备方法。 无机颗粒如沸石或白粘土和热固性树脂的细粉充分混合以铸造成多孔结构材料。 构成：也可以使用沸石，白土，木炭，铁素体或砂等作为无机材料，也可以使用酚醛树脂，环氧树脂，三聚氰胺树脂或尿素树脂作为热固性树脂。 无机材料的最佳粒径为5-600μm，树脂含量为过滤材料总重量的5-50％。 过滤材料通过以下步骤制备：原料的制备步骤，材料的混合步骤和浇铸步骤。
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公开(公告)号：KR1020000020032A
公开(公告)日：2000-04-15
申请号：KR1019980038442
申请日：1998-09-17
Applicant: 한국과학기술연구원
IPC: C07C321/04
Abstract: PURPOSE: Title derivatives useful as radioactive pharmaceuticals are prepared which can extend a residual time in heart, and minimize a radioactive disturbance. CONSTITUTION: 1,12-Dodecane diol is alcohol-substituted by bromic acid to give 12-bromo-dodecane-1-ol, and protected by tetrahydropyrane. Obtained dodecane, 2-ethyl-4,4-dimethyl-2-oxazoline and n-butyl lithium are reacted to give 2(R/S)-(4,4-dimethyl-2-oxazoline-2-yl)-12-tetrahydropyranyl oxy-tetradecane, and esterified with sulfuric acid to give ethyl-2(R/S)-methyl-12-hydroxytetradecaneate. Obtained tetradecaneate is protected to give ethyl-2(R/S)-methyl-14-tetra butyl dimethyl silyloxy-tetradecaneate, followed by reduction with lithium aluminum hydride to give 2(R/S)-methyl-14-t-butyl dimethyl silyloxy-tetradecane-1-ol, tosylated by tosyl chloride, and to give 3(R/S)-methyl-15-t-butyl dimethyl silyloxy-pentadecane-nitrile by substituting with sodium cyanide. Obtained nitride is treated with 1N-hydrochloric acid, hydrolyzed and mesylated to give 16-methane sulfonyl-3-methyl-pentadecanic acid. The pentadecanic acid is brominated, followed by reaction of thiourea and NaOH to give 15-mercapto-3-methyl-pentadecanic acid(formula 1).
Abstract translation: 目的：制备用作放射性药物的标题衍生物，其可以延长心脏中的残留时间，并使放射性干扰最小化。 构成：1,12-十二烷二醇被溴酸醇取代，得到12-溴 - 十二烷-1-醇，并用四氢吡喃保护。 获得的十二烷，2-乙基-4,4-二甲基-2-恶唑啉和正丁基锂反应，得到2（R / S） - （4,4-二甲基-2-恶唑啉-2-基） 四氢呋喃基氧基十四烷，并用硫酸酯化，得到乙基-2（R / S） - 甲基-12-羟基十四烷酸酯。 得到的十四烷酸乙酯得到乙基-2（R / S） - 甲基-14-四丁基二甲基甲硅烷氧基 - 十四烷酸酯，然后用氢化铝锂还原，得到2（R / S） - 甲基-14-叔丁基二甲基 甲硅烷氧基 - 十四烷-1-醇，用甲苯磺酰氯甲磺酰化，并用氰化钠代替得到3（R / S） - 甲基-15-叔丁基二甲基甲硅烷氧基 - 十五烷腈。 得到的氮化物用1N盐酸处理，水解和甲磺酰化得到16-甲磺酰基-3-甲基 - 十五烷酸。 将十五烷酸溴化，随后用硫脲和NaOH反应，得到15-巯基-3-甲基 - 十五烷酸（式1）。
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公开(公告)号：KR100378117B1
公开(公告)日：2003-03-29
申请号：KR1020000001329
申请日：2000-01-12
Applicant: 한국과학기술연구원
IPC: A01N29/00
Abstract: PURPOSE: A removing method for noxious tide using chlorine dioxide is provided, which can remove noxious tide effectively without secondary pollution by spreading chlorine dioxide solution on a sea area with red tide or green tide. CONSTITUTION: The chlorine dioxide is produced by reacting sodium chlorite with chlorine; 2NaClO2 + Cl2 → 2ClO2 + 2NaCl, which exists as a yellow-green gas at normal temperature, is used in an aqueous solution by dissolving in water to make the concentration at a ratio of 0.1-1ppm, and removes noxious tide with microorganisms(such as Cochlodinium, Chaetoceros, Mesodinium, Gymnodinium, and Gyrodinium) as well as toxic substances produced by them due to strong oxidizing power thereof. But a halogenide is not produced as a by-product, and the chlorine dioxide is easily resolved into oxygen molecule and chlorine ion by sunlight.
Abstract translation: 目的：提供一种利用二氧化氯的有毒潮汐的去除方法，该方法通过在赤潮或绿潮的海域散布二氧化氯溶液来有效去除有害潮汐而无二次污染。 组成：二氧化氯由亚氯酸钠与氯反应产生; 2NaClO 2 + Cl 2＆amp; 在常温下以黄绿色气体形式存在的2ClO 2 + 2NaCl在水溶液中使用，通过溶解在水中使浓度达到0.1-1ppm，并用微生物（如Cochlodinium，Chaetoceros ，中子，（Mesodinium），Gymnodinium和Gyrodinium）以及由于其强氧化能力而产生的有毒物质。 但是，卤化物不作为副产物产生，并且二氧化氯通过日光很容易分解成氧分子和氯离子。
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公开(公告)号：KR1020020059042A
公开(公告)日：2002-07-12
申请号：KR1020000087302
申请日：2000-12-30
Applicant: 한국과학기술연구원
IPC: C07F9/38
CPC classification number: C07F9/40
Abstract: PURPOSE: Provided is a manufacturing method for dialkyl(4-hydroxy-3,5-di(t-butyl)benzyl)phosphonate(DAP) in high yield , thereby mass-producing DAP without generating carcinogens not by using a strong base. CONSTITUTION: Dialkyl(4-hydroxy-3,5-di(t-butyl)benzyl)phosphonate is manufactured by reacting N, N-dialkyl-(4-hydroxy-3,5-di(t-butyl)benzyl)amine or its salt with dialkyl phosphate or trialkyl phosphate in the presence of an alkylating agent, at 60-120 deg.C.
Abstract translation: 目的：提供高收率的（4-羟基-3,5-二（叔丁基）苄基）膦酸二烷基酯（DAP）的制造方法，从而大量生产DAP而不产生致癌物质而不是使用强碱。 构成：通过使N，N-二烷基 - （4-羟基-3,5-二（叔丁基）苄基）胺反应制得二（2,4-羟基-3,5-二（叔丁基）苄基） 其盐与磷酸二烷基酯或磷酸三烷基酯在烷基化剂存在下，在60-120℃。
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Patent Agency Ranking
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公开(公告)号：KR1020010073625A
公开(公告)日：2001-08-01
申请号：KR1020000002389
申请日：2000-01-19
Applicant: 한국과학기술연구원
IPC: C07D401/12
Abstract: PURPOSE: An arylpiperazine compound and a producing method thereof are provided. The arylpiperazine compound can label technetium and F-18 with no having disadvantages of prior arts. CONSTITUTION: The arylpiperazine compound is represented by formula (1), in which R is methanesulfonyl, paratoluenesulfonyl or trifluoromethanesulfonyl. A compound of formula (1a) is produced by treating a compound of formula (7) with mesyl chloride under triethylamine. A compounds of formula (1b) is produced by reacting a compound of formula (13) with sodium hydrogen and the compound of formula (7) to produce a compound of formula (14); and dissolving the compound of formula (14) in anhydrous anisole and reacting with anhydrous trifluoro acetic acid, in which the compound of formula (13) is produced by dissolving a compound of formula (9) into trifluoro acetic acid and reacting with triphenylmethanol to produce a compound of formula (10); reacting the compound of formula (10) with triethylamine and bromoacetyl bromide to produce a compound of formula (11); reacting the compound of formula (11) with triphenylmethanol under trifluoro acetic acid to produce a compound of formula (12); and reacting the compound of formula (12) with 3-bromopropionyl chloride. The formula (1b), (9) to (14) are described as in the description.
Abstract translation: 目的：提供芳基哌嗪化合物及其制备方法。 芳基哌嗪化合物可以标记锝和F-18，没有现有技术的缺点。 构成：芳基哌嗪化合物由式（1）表示，其中R是甲磺酰基，对甲苯磺酰基或三氟甲磺酰基。 通过在三乙胺下用甲磺酰氯处理式（7）化合物来制备式（1a）化合物。 通过使式（13）化合物与氢钠和式（7）化合物反应制备式（14）化合物来制备式（1b）化合物; 并将式（14）化合物溶于无水苯甲醚中，与无水三氟乙酸反应，其中式（13）化合物通过将式（9）化合物溶解在三氟乙酸中并与三苯基甲醇反应产生 式（10）的化合物; 使式（10）化合物与三乙胺和溴乙酰溴反应生成式（11）化合物; 在三氟乙酸下使式（11）化合物与三苯基甲醇反应，生成式（12）化合物; 并使式（12）化合物与3-溴丙酰氯反应。 公式（1b），（9）〜（14）在说明书中进行说明。
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公开(公告)号：KR100281827B1
公开(公告)日：2001-04-02
申请号：KR1019980038443
申请日：1998-09-17
Applicant: 한국과학기술연구원
Abstract: 본 발명은 유기 아민의 아실화 방법에 있어서, 아실화제로서 다음 화학식 1을 갖는 N,N-디아실이미다졸론 유도체를 사용하는 아실화 방법을 제공한다:
화학식 1.
식 중에서,
R
1 과 R
2 는 같거나 다르고, 메틸, 에틸 또는 C
3 -C
19 의 직쇄 또는 치환된 알킬기, 페닐, 헤테로 사이클릭 화합물, 알콕시기 및 유기산 치환기로 이루어진 군 중에서 선택되며;
R
3 와 R
4 는 같거나 다르고, 수소 원자, 메틸 또는 에틸, 페닐, 치환된 페닐 및 알콕시카보닐기로 이루어진 군 중에서 선택되거나, R
3 와 R
4 는 이들이 결합되어 있는 탄소 원자와 함께 다음 구조를 갖는 R 치환 벤젠 고리를 형성함
(여기서, R은 수소 원자, 카르복실기 또는 설폰산기임).-
公开(公告)号：KR100154354B1
公开(公告)日：1998-11-16
申请号：KR1019940013194
申请日：1994-06-11
Applicant: 한국과학기술연구원
IPC: C07D487/04 , A61K31/43 , C07D207/00 , C07D477/04
Abstract: 본 발명에서는 다음 일반식(Ⅰ)의 피롤리디닐티오계 카바페넴 유도체가 개시된다.
본 발명의 카바페넴 유도체는 내성균에 효과가 있으며 DHP-1 효소에 대한 안정성이 우수하다.-
公开(公告)号：KR1019950014061A
公开(公告)日：1995-06-15
申请号：KR1019930023229
申请日：1993-11-03
Applicant: 한국과학기술연구원
IPC: C07C251/32 , C07C249/08
Abstract: 본 발명은 1단계 또는 2단계 반응에 의한 의학 진단용 시약인 (RR/SS)-4, 8-디아지-3, 6, 6, 9- 테트라 메틸 운데칸-3, 8-디엔-2, 10-디온 비스 옥심의 제조방법에 관한 것이다. 본 발명에 의해 d, 1-HM-PAO가 효과적으로 얻어질 수 있다.
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