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    두채류의 재배방법
    3.
    发明授权
    두채류의 재배방법 失效
    두채류의재배방법

    公开(公告)号：KR100384694B1

    公开(公告)日：2003-05-22

    申请号：KR1020000083443

    申请日：2000-12-28

    Applicant: 한국과학기술연구원

    Inventor： 조정혁 ,  오창석 ,  오창현 ,  이기수

    IPC: A01G31/00

    Abstract: 본 발명은 인체에 해가 없는 살균제를 사용하여, 콩나물, 숙주나물 등의 두채류를 재배하는 방법에 관한 것이다. 본 발명의 두채류의 재배방법은 이산화염소계열의 살균제를 용해시킨 물에 콩을 침지하여 발아시키는 단계; 및, 발아된 콩에 이산화염소계열의 살균제를 용해시킨 물을 공급하며, 암실에서 재배하는 단계를 포함한다. 본 발명에 의하면, 인체에 해로운 물질이 두채류에 잔류되지 않는 살균제를 사용하여 두채류의 수확량 및 품질을 향상시킬 수 있을 것이다.

    Abstract translation: 目的：提供一种使用对男人安全的杀菌剂来生长豆芽和蔬菜如豆芽的方法。 杀菌剂残留物不留在豆芽中，而杀真菌剂则提高了豆芽的产量和质量。 组成：生长方法包括：通过将豆类浸泡在其中溶解有0.1-100ppm的基于二氧化氯的杀真菌剂的水中来发芽豆芽的步骤; 以及在供应其中溶解有0.01-10ppm二氧化氯基杀真菌剂的水的情况下在黑暗中生长发芽豆芽的步骤。

    Ｎ₂Ｓ₂ 리간드가 결합된 아릴피페라진 유도체 및 이의 제조방법
    7.
    发明公开
    Ｎ₂Ｓ₂ 리간드가 결합된 아릴피페라진 유도체 및 이의 제조방법 失效
    与N2S2配体连接的亚苄基衍生物及其制备方法

    公开(公告)号：KR1020000051075A

    公开(公告)日：2000-08-16

    申请号：KR1019990001313

    申请日：1999-01-18

    Applicant: 한국과학기술연구원

    Inventor： 조정혁 ,  오창현 ,  이기수 ,  유현진 ,  이명철 ,  정준기 ,  이동수 ,  정재민

    IPC: C07D211/64

    Abstract: PURPOSE: Arylpiperazine derivatives attached with an N2S2 ligand useful as an imaging compound for serotonin receptors and preparing process thereof are provided which have the advantage of labelling a technetium being free from amide hydrolysis and having high affinity with 5-HT1A. CONSTITUTION: A process for preparing tetrabenazine derivatives represented by the formula (1) comprises the steps of synthesizing arylpiperazine derivatives, synthesizing an N2S2 ligand and attaching the N2S2 ligand to the arylpiperazine derivatives. In formula, X denotes methoxy, trifluoromethyl, or chloro; Y denotes carbon or nitrogen; Z denotes carbon or nitrogen. The compound has the advantage of labeling a technetium having the radiochemically optimum physical conditions(manufacturing easiness, half-life period, radioactive strength and purchase easiness).

    Abstract translation: 目的：提供用作用作血清素受体成像化合物的N2S2配体附着的芳基哌嗪衍生物及其制备方法，其具有标记锝不含酰胺水解并且与5-HT1A具有高亲和力的优点。 构成：由式（1）表示的制备丁苯那嗪衍生物的方法包括合成芳基哌嗪衍生物，合成N 2 S 2配体并将N 2 S 2配体连接到芳基哌嗪衍生物的步骤。 在式中，X表示甲氧基，三氟甲基或氯; Y表示碳或氮; Z表示碳或氮。 该化合物具有标记具有放射化学最佳物理条件（制造容易度，半衰期，放射性强度和购买容易度）的锝的优点。

    사이클린 의존성 키나제（ＣＤＫ）의 억제제로 유용한 퓨린 유도
    8.
    发明公开
    사이클린 의존성 키나제（ＣＤＫ）의 억제제로 유용한 퓨린 유도 无效
    有益于循环激素（CDK）抑制剂的嘌呤衍生物

    公开(公告)号：KR1020000050975A

    公开(公告)日：2000-08-05

    申请号：KR1019990001184

    申请日：1999-01-16

    Applicant: 한국과학기술연구원

    Inventor： 조정혁 ,  오창현 ,  이수철 ,  이기수

    IPC: C07D473/00

    Abstract: PURPOSE: Provided are purine derivatives useful as an inhibitor of the cycline-dependent kinases(CDK) and a preparation method thereof. The purine derivatives are useful as an anti-cancer agent and an inhibitor of CDK because of their high selectivity to the CDK. CONSTITUTION: A purine derivatives are represented by formula(1), wherein R1 is methyl, isopropyl, allyl, cyclopropyl; and R2 is 4-(2-hydroxyethyl)piperazine, 4-hydroxypiperidine, thiomorpholin, 2-hydroxymethylpyrrolidine. Adenine is used as a starting material to prepare the purine derivatives instead of 2, 6-dichloropurine thereby being easy to handle and cutting down expenses.

    Abstract translation: 目的：提供可用作循环依赖性激酶（CDK）的抑制剂的嘌呤衍生物及其制备方法。 嘌呤衍生物由于其对CDK的高选择性而可用作抗癌剂和CDK抑制剂。 构成：嘌呤衍生物由式（1）表示，其中R 1是甲基，异丙基，烯丙基，环丙基; R2是4-（2-羟乙基）哌嗪，4-羟基哌啶，硫代吗啉，2-羟甲基吡咯烷。 腺嘌呤被用作制备嘌呤衍生物而不是2,6-二氯嘌呤的起始原料，因此易于处理和降低费用。

    메틸렌디포스폰산의제조방법
    9.
    发明公开
    메틸렌디포스폰산의제조방법 失效
    甲基二磷酸的制备方法

    公开(公告)号：KR1020000020033A

    公开(公告)日：2000-04-15

    申请号：KR1019980038443

    申请日：1998-09-17

    Applicant: 한국과학기술연구원

    Inventor： 조정혁 ,  오창현 ,  이기수 ,  이창식 ,  이명철 ,  정준기 ,  이동수 ,  정재민

    IPC: C07F9/00 ,  C07F9/38

    Abstract: PURPOSE: A preparation method of methylene diphosphonic acid by using diidomethane having a higher boiling point than reaction temperature is provided which produces the title compound in high yield, improves high productivity and is very economic by reusing trialkylphosphate as a starting material. CONSTITUTION: A process is disclosed for preparing methylene diphosphonic acid(1) which comprises: (a)preparing tetralkylmethylenediphosphonic acid ester(4) by reacting trialkyl phosphate(2) with diiodomethane(3); (b)separating the compound(4) from the reactant by removing alkyl iodine; (c)recovering excess trialkylphosphate by distillation at 180°C and recycling to the process(a); (d)removing alkyl groups by thermal-cracking the ester at 200-210°C and recrystallizing. In formula, R is allyl, isopropyl, t-butyl, isobutyl. The compound is useful as raw material of radioactive pharmaceuticals for diagnosis.

    Abstract translation: 目的：提供通过使用沸点比反应温度高的二甲基亚甲基二膦酸的制备方法，其以高产率产生标题化合物，提高高生产率，并且通过重复使用三烷基磷酸酯作为起始原料是非常经济的。 公开：制备亚甲基二膦酸（1）的方法，其包括：（a）通过使三烷基磷酸酯（2）与二碘甲烷（3）反应制备四烷基亚甲基二膦酸酯（4）; （b）通过除去烷基碘将化合物（4）与反应物分离; （c）通过在180℃下蒸馏回收过量的三烷基磷酸酯并再循环至方法（a）; （d）通过在200-210℃下热裂解酯并重结晶来除去烷基。 在式中，R是烯丙基，异丙基，叔丁基，异丁基。 该化合物可用作放射性药物的诊断原料。

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