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    PROCESS FOR THE SIMULTANEOUS PREPARATION OF 2,5-DIOXO-1,2-OXA-PHOSPHOLANES AND (BETA)-HALOGENPROPIONIC ACID HALIDE
    33.
    发明专利
    PROCESS FOR THE SIMULTANEOUS PREPARATION OF 2,5-DIOXO-1,2-OXA-PHOSPHOLANES AND (BETA)-HALOGENPROPIONIC ACID HALIDE 未知

    公开(公告)号：CA1086765A

    公开(公告)日：1980-09-30

    申请号：CA274323

    申请日：1977-03-18

    Applicant: HOECHST AG

    Inventor： RUPP WALTER ,  FINKE MANFRED

    IPC: C07C53/50 ,  C07C51/00 ,  C07C67/00 ,  C07F9/30 ,  C07F9/32 ,  C07F9/6571 ,  C07F9/6574

    Abstract: of the disclosure: 2,5-Dioxo-1,2-oxa-phospholanes of the formula (I) (I) wherein R1 is an organic radical and R2 and R3 each also means organic radicals or hydrogen, are prepared by reacting 2-halogeno-formylethyl-phosphinic acid halides of the formula (II) (II) wherein R1, R2 and R3 are defined as in formula (I) and X means Cl or Br, preferably Cl, with an approximately equimolar quantity of acrylic acid. The compounds (II) may also be produced in the reaction batch and in situ by reacting about equimolar quantities of a dihalogenophosphine of the formula (III) (III) with an .alpha.,.beta.-unsaturated acid (IV) CHR2=CR3-COOH (IV) In the formulae (III) and (IV) R1, R2, R3 and X are defined as indicated above. In the reaction there is formed, in addition to the compounds (I), practically exclusively .beta.-halogenopropionic acid and no free hydrogen halide. The phospholanes (I) are valuable flame retarding agents for plastics, intermediates, for example, for the synthesis of biocidals etc. - 1a

    37.
    发明专利
    未知

    公开(公告)号：AT139553T

    公开(公告)日：1996-07-15

    申请号：AT90111597

    申请日：1987-02-10

    Applicant: HOECHST AG

    Inventor： WALZ GERD ,  HOENEL MICHAEL ,  BRINDOEPKE GERHARD ,  SPRENGER WALTER ,  FINKE MANFRED ,  LENZ RUEDIGER

    IPC: C07D317/36 ,  C07C67/00 ,  C07C239/00 ,  C07C269/00 ,  C07C271/20 ,  C07D303/28 ,  C08G18/06 ,  C08G18/32 ,  C08G18/64 ,  C08G18/70 ,  C08G18/80 ,  C08G18/83 ,  C08G59/02 ,  C08G59/40 ,  C08G71/04 ,  C09D5/44 ,  C09D175/04 ,  C09D175/12

    Abstract: Amino-urethanes (I) claimed are of formula R3-N(Re)-A-R1-NH-C(O)-O-CH2-CH(OH)-CH2- R-CH2-CH(OH)-CH2-O-C(O)-NH- R1-A-N(R2)R3 R is residue of a diglycidyl ether or ester, or 2-18 alkylene gp.; R1 is opt. branched 2-18C alkylene; R2 is H, 1-8Calkyl, or 1-8C hydroxyalkyl; R3 is R2, or R3 with R2 can form cyclic ring, or, if R2 is H then R3 can be at least one gp. of formula (a) -C(O)-O-CH2-CH(R4)-CH2- (R-CH2-CH(R4)-CH2-OmB-(R4)n R4 is OH or -CONH-PI-NHCO R6; B is residue of a polyol; m is 1-3; n is 1-6; and PI is residue of a polyisocyanate and R6 is residue of (cylco)aliphatic, or alkylaromatic alcohol, an aminoalcohol, ketoxime, or a CH- or NH- acidic cpd.: b) R3 is gp. of formula (I) R5 is H or R4; R7 is 1-8Calkyl; and s is 1-6; c) -C(O)-NH-PI-NH-C(O)-O-B-d)R8-CHOH-CH2-O-CO-; e) R8-CHOH-CH2-; R8 is H, 1-18C alkyl, or residue of a glycidyl ester or ether; or f) PI'NHCO- PI' is residue of a partly capped polyisocyanate; and A 75 chemical bond or -R1NH)r-R1NH- r is 0-6. Prodn. of a (I) by heating an at least bifunctional 2-oxo-1,3-dioxolan (II) and a prim polyamine at 20-150 deg.C is claimed. Structural formulae are given for pref. R, viz. residues of a bisphenol diglycidyl ether opt. linked by residues of a diamine, diol, dicarboxylic acid, di-isocyanate, etc. Pref. (II) is bicyclic carbonate of specified formuls esp. derived from polyglycidyl ether of a polyphenol, or a epoxide-cyclic carbonate.

    CURING AGENT FOR SYNTHETIC RESINS, CURABLE MIXTURES CONTAINING THIS CURING AGENT AND ITS USE
    38.
    发明专利
    CURING AGENT FOR SYNTHETIC RESINS, CURABLE MIXTURES CONTAINING THIS CURING AGENT AND ITS USE 未知

    公开(公告)号：CA1334960C

    公开(公告)日：1995-03-28

    申请号：CA594408

    申请日：1989-03-22

    Applicant: HOECHST AG

    Inventor： HOENEL MICHAEL ,  FINKE MANFRED ,  WALZ GERD ,  ZIEGLER PETER

    IPC: C08G18/32 ,  C08G18/38 ,  C08G18/64 ,  C08G18/80 ,  C09D5/44 ,  C09D175/00 ,  C09D175/04 ,  C07C271/08 ,  C08G18/10

    Abstract: A curing agent (A) for resins (B) which can be cured by means of isocyanates, which has an amine number of 20 to 150 mg of KOH/g and an OH number of not more than 20 mg of KOH/g and which contains per molecule at least two masked isocyanate groups which are reactive under the conditions of curing, obtained by reacting (a) an amine which contains at least one .beta.-hydroxyalkyl group per molecule and has an OH number of 100 to 1,200 mg of KOH/g and an amine number of 100 to 1,200 mg of KOH/g and which, if appropriate, also contains NHCO groups, if appropriate as a mixture with another OH-functional and/or NH-functional compound, with (b) a partly masked isocyanate, if appropriate as a mixture with an at least difunctional, OH-reactive and/or NH-reactive compound. These curing agents are readily dispersible in aqueous systems, if appropriate after neutralization, and frequently increase stability in aqueous paint formulations.

    AMINOURETHANES
    40.
    发明专利
    AMINOURETHANES 未知

    公开(公告)号：AU598231B2

    公开(公告)日：1990-06-21

    申请号：AU6872787

    申请日：1987-02-12

    Applicant: HOECHST AG

    Inventor： WALZ GERD ,  HONEL MICHAEL ,  BRINDOPKE GERHARD ,  SPRENGER WALTER ,  FINKE MANFRED ,  LENZ RUDIGER

    IPC: C07D317/36 ,  C07C67/00 ,  C07C239/00 ,  C07C269/00 ,  C07C271/20 ,  C07D303/28 ,  C08G18/06 ,  C08G18/32 ,  C08G18/64 ,  C08G18/70 ,  C08G18/80 ,  C08G18/83 ,  C08G59/02 ,  C08G59/40 ,  C08G71/04 ,  C09D5/44 ,  C09D175/04 ,  C09D175/12 ,  C08L75/12 ,  C08L75/04 ,  C07C87/14 ,  C07C91/12 ,  C09D3/72 ,  C07C101/24

    Abstract: Amino-urethanes (I) claimed are of formula R3-N(Re)-A-R1-NH-C(O)-O-CH2-CH(OH)-CH2- R-CH2-CH(OH)-CH2-O-C(O)-NH- R1-A-N(R2)R3 R is residue of a diglycidyl ether or ester, or 2-18 alkylene gp.; R1 is opt. branched 2-18C alkylene; R2 is H, 1-8Calkyl, or 1-8C hydroxyalkyl; R3 is R2, or R3 with R2 can form cyclic ring, or, if R2 is H then R3 can be at least one gp. of formula (a) -C(O)-O-CH2-CH(R4)-CH2- (R-CH2-CH(R4)-CH2-OmB-(R4)n R4 is OH or -CONH-PI-NHCO R6; B is residue of a polyol; m is 1-3; n is 1-6; and PI is residue of a polyisocyanate and R6 is residue of (cylco)aliphatic, or alkylaromatic alcohol, an aminoalcohol, ketoxime, or a CH- or NH- acidic cpd.: b) R3 is gp. of formula (I) R5 is H or R4; R7 is 1-8Calkyl; and s is 1-6; c) -C(O)-NH-PI-NH-C(O)-O-B-d)R8-CHOH-CH2-O-CO-; e) R8-CHOH-CH2-; R8 is H, 1-18C alkyl, or residue of a glycidyl ester or ether; or f) PI'NHCO- PI' is residue of a partly capped polyisocyanate; and A 75 chemical bond or -R1NH)r-R1NH- r is 0-6. Prodn. of a (I) by heating an at least bifunctional 2-oxo-1,3-dioxolan (II) and a prim polyamine at 20-150 deg.C is claimed. Structural formulae are given for pref. R, viz. residues of a bisphenol diglycidyl ether opt. linked by residues of a diamine, diol, dicarboxylic acid, di-isocyanate, etc. Pref. (II) is bicyclic carbonate of specified formuls esp. derived from polyglycidyl ether of a polyphenol, or a epoxide-cyclic carbonate.

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