Abstract:
PURPOSE: An ink and signature discriminating method using spectroscopy is provided to analyze the spectrum of a signature and an ink pad using the high performance resolution of Micro ATR-FTIR spectral equipment. CONSTITUTION: The location of the imprint of a seal is determined in an identify object sample(S105). An Micro ATR-FTIR(attenuated total reflectance Fourier transform infrared spectroscopy) about the background of the imprint of the seal is measured(S110). The Micro ATR-FTIR spectrum about a part of the imprint of the seal is measured(S120). A sample spectrum is obtained by eliminating the spectrum of the background from the spectrum of the part of the imprint of the seal(S130). A feature of the sample spectrum which is used as the search key of a database or library is selected(S140). An ink pad sample spectrum having equality more than a designated value is searched(S150). A searched result is outputted(S160).
Abstract:
본 발명은 분광분석법의 응용에 관한 것으로, 더욱 상세하게는 분광법을 이용한 볼펜 서명 감식 방법에 관한 것이다. 본 발명의 일 실시예에 따른 볼펜 서명 감식 방법은, 볼펜 서명(署名)의 배경에 대하여 분광 스펙트럼을 측정하는 단계와, 볼펜 서명 부분에 대하여 분광 스펙트럼을 측정하는 단계와, 볼펜 서명 부분의 분광 스펙트럼으로부터 배경의 분광 스펙트럼을 제거하여 볼펜 잉크의 분광 스펙트럼을 구하는 단계와, 볼펜 잉크의 분광 스펙트럼에서 검색 키로 사용할 특징을 선택하는 단계와, 볼펜 잉크 샘플 스펙트럼 데이터베이스에서 검색 키에 대하여 미리 정해진 값 이상의 동등성 조건을 만족하는 볼펜 잉크 샘플 스펙트럼을 검색하는 단계 및 검색된 결과에 기초하여 동등성 조건을 만족하는 볼펜 잉크 샘플의 발견 여부 및 발견된 볼펜 잉크 샘플의 출처 정보를 출력하는 단계를 포함한다.
Abstract:
PURPOSE: Provided is a vinyl carbamoyl azide derivative, which is more stable than a conventional carbamoyl azide derivative and has an effective sterilizing power against mold harmful to the crops. CONSTITUTION: The vinyl carbamoyl azide derivative represented by the formula 1 is produced by reacting an isocyanate compound(R1NCO) and hydrazoic acid(NH3) or sodium azide(NaN3). In the formula, R1 is at least one C1-C6 alkyl, or furyl or phenyl capable of being substituted by at least one substituent selected from the group consisting of halogen, C1-C6 alkoxy, and nitro.
Abstract:
PURPOSE: Provided is a manufacturing method for dialkyl(4-hydroxy-3,5-di(t-butyl)benzyl)phosphonate(DAP) in high yield , thereby mass-producing DAP without generating carcinogens not by using a strong base. CONSTITUTION: Dialkyl(4-hydroxy-3,5-di(t-butyl)benzyl)phosphonate is manufactured by reacting N, N-dialkyl-(4-hydroxy-3,5-di(t-butyl)benzyl)amine or its salt with dialkyl phosphate or trialkyl phosphate in the presence of an alkylating agent, at 60-120 deg.C.
Abstract:
PURPOSE: A COD(chemical oxygen demand) reducing technology for leachate from a reclamation site using biological treatment is provided to greatly reduce COD by using bacteria producing lignin decomposition and/or oxidation enzyme. CONSTITUTION: Using bacteria having lignin decomposing enzyme or oxidizing enzyme like monoxidase or dioxidase, lignin and cyclic compounds containing halogen, which are hardly decomposed under normal condition, are easily decomposed to reduce COD. The treated bacteria grow well without adding no nutrient in the leachate. Intake and decomposition by the bacteria reduce COD value and lower nutrients in the leachate.
Abstract:
PURPOSE: Provided are novel 1-β-methylcarbapenem derivatives substituted by pyrrolidine containing imidazoline ring which are strong antibiotics against resistant bacteria. CONSTITUTION: The compound is represented by chemical formula 1, where R is C1-6 low alkyl, aryl and benzyl group which are substituted by one or more groups from hydrogen, hydroxy, amine, sulfonyl and aminosulfonyl group. The process of preparing the compound consists of: converting diazoazetidione compound, chemical formula 2, to two ring keto ester under rhodium acetate catalyst and reacting at 0-5deg.C with diphenylchlorophosphate under base such as diisopropylethylamine; reacting the resultant with thiol derivative of chemical formula 3, and eliminating allyl group from the product by reacting with tributyltinhydride under tetrakisphosphine palladium(0) catalyst at room temp. for 2 hours. After reactions, distilled water is added to extract the water layer and it is freeze dried to get the final compound.
Abstract:
PURPOSE: 1-beta-methyl-2-thiol carageen derivatives having thiol derivatives in 2-position are prepared which has a stability for DHP-1 enzyme. CONSTITUTION: Trans-L-hydroxyproline and potassium cyanate are dehydrogenated to give cyclized 7-hydroxy-1,3-diazabicyclo(3.3.0)octan-2,4-dione, followed by alkylation with alkyl halide and calcium carbonate, and treated with methyl sulfonyl chloride in the presence of triethyl amine to give a compound(formula 3). Obtained compound(3) is treated with potassium thioacetate and hydrolyzed by 4N-NaOH to give thiol derivatives(formula 1; R is lower allyl containing hydrogen, methyl, ethyl, propyl, butyl, and alkyl group containing hydroxy group such as benzyl, ethyl alcohol etc. 1-beta-methyl-2-thiol carageen derivatives(formula 2) are prepared from the thiol derivatives.