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公开(公告)号：KR1020120061484A
公开(公告)日：2012-06-13
申请号：KR1020100122816
申请日：2010-12-03
Applicant: 현대자동차주식회사
Abstract: PURPOSE: A manufacturing method of a hydrophobic polymer-carbon support composite for a fuel cell electrode is provided to simplify manufacturing process, thereby mass producing water repellents for fuel battery air electrodes. CONSTITUTION: A manufacturing method of a hydrophobic polymer-carbon support composite for a fuel cell electrode comprises the following steps: manufacturing a dispersed solution by dispersing carbon support in a solvent; manufacturing a mixed solution which hydrophobic polymer is dispersed on surface of carbon support through mixing and ultrasonic dispersion after adding hydrophobic polymer in the dispersed solution; and heat-treating the mixed solution at 100-500 deg. Celsius. The carbon support has diameter of 10-1000 nano meters. 1-100.0 parts by weight of the hydrophobic polymer are used based on 100.0 parts by weight of carbon support.
Abstract translation: 目的：提供用于燃料电池电极的疏水性聚合物 - 碳载体复合材料的制造方法，以简化制造工艺，从而大量生产用于燃料电池空气电极的防水剂。 构成：用于燃料电池电极的疏水性聚合物 - 碳载体复合材料的制造方法包括以下步骤：通过将碳载体分散在溶剂中制造分散溶液; 通过在分散溶液中加入疏水性聚合物之后通过混合和超声分散制备疏水性聚合物分散在碳载体表面上的混合溶液; 并在100-500度下对混合溶液进行热处理。 摄氏度。 碳载体直径为10-1000纳米。 基于100.0重量份的碳载体使用1-100.0重量份的疏水性聚合物。
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公开(公告)号：KR1020110022431A
公开(公告)日：2011-03-07
申请号：KR1020090080025
申请日：2009-08-27
Applicant: 현대자동차주식회사
CPC classification number: H01M4/8668 , H01M4/8828 , H01M4/8882 , H01M4/92 , H01M2008/1095
Abstract: PURPOSE: A porous electrode catalyst layer for a fuel cell is provided to obtain an electrode with improved bindability with a hydrocarbon-based film by lowering a glass transition temperature of a hydrocarbon-based binder. CONSTITUTION: A porous electrode catalyst layer for a fuel cell comprises sulfonated hydrocarbon, porogen, and platinum catalyst. The sulfonated hydrocarbon is such that single or two or more hydrocarbons are sulfonated, wherein the hydrocarbon is selected from polysulfone, polyarylene ethersulfone, polyetherethersulfone, polyethersulfone, polyimide, polyimidazole, polybenzimidazole, polyether benzimidazole, polyarylene ethylene ketone, polyether ether ketone, and polystyrene.
Abstract translation: 目的：提供一种用于燃料电池的多孔电极催化剂层，以通过降低烃基粘合剂的玻璃化转变温度来获得具有改进的与烃类膜的粘合性的电极。 构成：用于燃料电池的多孔电极催化剂层包括磺化烃，致孔剂和铂催化剂。 所述磺化烃使得一个或两个以上的烃被磺化，其中烃选自聚砜，聚亚芳基醚砜，聚醚醚砜，聚醚砜，聚酰亚胺，聚咪唑，聚苯并咪唑，聚醚苯并咪唑，聚亚芳基乙烯酮，聚醚醚酮和聚苯乙烯。
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公开(公告)号：KR100986563B1
公开(公告)日：2010-10-07
申请号：KR1020090018829
申请日：2009-03-05
Applicant: 현대자동차주식회사 , 연세대학교 산학협력단
CPC classification number: H01M4/92 , B82Y30/00 , H01M4/926 , H01M2004/8689
Abstract: 본 발명은 내부식성이 우수한 연료전지용 촉매 제조 방법에 관한 것으로서, 더욱 상세하게는 탄소 나노케이지(Carbon Nanocage(CNC))를 이용하여 내부식성이 우수한 연료전지의 공기극 촉매를 제조할 수 있도록 한 내부식성이 우수한 연료전지용 촉매 제조 방법에 관한 것이다.
이를 위해, 본 발명은 상기한 목적을 달성하기 위한 본 발명은 카본블랙(Carbon Black)류 탄소인 아세틸렌 블랙(Acetylene Black)을 사용하여 카본 나노케이지(Carbon Nanocage(CNC)) 제조하는 제1단계와; 용매이자 환원제 역할을 하는 에틸렌 글리콜(ethylene glycol)에 NaOH, 백금전구체, 카본(Carbon)을 일정량 넣어 교반하는 제2단계와; 상기 에틸렌 글리콜(ethylene glycol)을 산화시키면서 백금전구체를 환원시키는 제3단계와; pH 조절을 통해 백금의 담지율을 높이는 제4단계와; 세척 과정 및 열 건조를 거쳐 불필요한 유기물을 제거하는 제5단계; 를 포함하는 것을 특징으로 하는 내부식성이 우수한 연료전지용 촉매 제조 방법을 제공한다.
연료전지, 공기극, 부식, 내부식성, 평가 방법, 임피던스, 이산화탄소, CV 테스트, MEA, 촉매, 탄소 나노케이지, 카본블랙-
公开(公告)号：KR100969011B1
公开(公告)日：2010-07-09
申请号：KR1020080015339
申请日：2008-02-20
Applicant: 현대자동차주식회사 , 서강대학교산학협력단
IPC: H01M8/10
CPC classification number: C08J5/2275 , C08J2371/00 , C08J2381/06 , H01M8/1016 , H01M2300/0068 , H01M2300/0082 , H01M2300/0091 , Y02P70/56
Abstract: 3-아미노프로필트리에틸실란과 테트라에틸오소실리케이트의 기공 구조를 양말단에 포함하고 인산이 화학적으로 결합된, 주쇄가 폴리디메틸실록산(poly dimethyl siloxane)인 무기고분자로 이루어진 고분자 및 측쇄에 양이온 교환기를 갖는 양성자 전도성 고분자로 이루어진 고분자 블렌드 전해질 막 및 그 제조방법에 관한 것이다.
일반적으로, 양이온 전도성 전해질 막은 고온에서는 그 양이온 전도성이 급격히 떨어진다. 그러나, 효율성과 비용적인 이점이 있어, 고온에서도 양이온 전도성이 우수한 전해질 막이 요구되는 바, 본 발명에서는 고온용 고분자 블렌드 전해질 막과 이의 제조 방법을 제공하고자 한다.
연료전지, 전해질 막, 고분자 블렌드, 무기고분자, 인산-
公开(公告)号：KR1020090117124A
公开(公告)日：2009-11-12
申请号：KR1020080043030
申请日：2008-05-08
Applicant: 현대자동차주식회사 , 주식회사 동진쎄미켐
CPC classification number: C08G75/23 , C08G65/4012 , C08G65/4056 , C08J5/2256 , C08J2381/06 , C08L2205/05 , H01M8/1011 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M2300/0082 , Y02E60/523
Abstract: PURPOSE: A polymer electrolyte membrane is provided to improve membrane/electrode interface adhesion which improves H-ion conductivity and to secure long time stability of a hydrocarbon polymer membrane electrode assembly. CONSTITUTION: A polymer electrolyte membrane has 0.01-50 weight% of a polymer blend introduced to a proton-conducting hydrocarbon-based polymer which is a sulfonated polysulfone ketone copolymer. The sulfonated polysulfone ketone copolymer comprises an aromatic sulfone repeating unit, an aromatic ketone repeating unit, and an aromatic compound repeating unit which connects the repeating units by ether bond. At least one kind of the aromatic sulfone repeating unit and aromatic ketone repeating unit has a sulfonic acid or sulfonate substitution.
Abstract translation: 目的：提供聚合物电解质膜以改善膜/电极界面的粘附，提高H离子传导性，并确保烃聚合物膜电极组件的长时间稳定性。 构成：聚合物电解质膜具有0.01-50重量％的引入质子传导烃基聚合物的聚合物共混物，其是磺化聚砜酮共聚物。 磺化聚砜酮共聚物包括芳族砜重复单元，芳族酮重复单元和通过醚键连接重复单元的芳族化合物重复单元。 至少一种芳香砜重复单元和芳香族酮重复单元具有磺酸或磺酸取代。
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Patent Agency Ranking
公开(公告)号：KR100925913B1
公开(公告)日：2009-11-09
申请号：KR1020070086677
申请日：2007-08-28
Applicant: 현대자동차주식회사
IPC: H01M8/10
CPC classification number: H01M8/0221 , H01M8/086 , H01M8/1011 , H01M8/1027 , H01M8/103 , H01M8/1048 , H01M8/1053 , H01M2008/1293 , Y02E60/523 , Y02P70/56
Abstract: 본 발명은 무가습 고분자 전해질 막에 산 용해 방지를 위하여 음이온 고정화 물질을 코팅층으로 도입하여 다층막으로 제조하는 연료전지용 무가습 고분자 전해질 막 및 이를 포함한 연료전지에 관한 것이다. 이를 더욱 상세하게 설명하면, 본 발명은 기존의 무가습 고분자 전해질 막에 음이온 고정화 물질을 코팅함으로써 다층막으로 형성된 고분자 전해질 막을 제공하고, 이를 이용하여 연료전지를 제조함으로써, 산의 용해를 방지하여 연료전지의 효과를 장기적, 지속적으로 유지시킬 수 있게 하고 이로 인해 경제적, 환경적 이득을 도모하고자 한다.
연료전지(Fuel Cell), 음이온 고정화 물질, 무가습 고분자 전해질 막(non-aqueous polymer electrolyte membrane), 다층 고분자 전해질 막, 산 용출 억제-
公开(公告)号：KR100844752B1
公开(公告)日：2008-07-07
申请号：KR1020070063045
申请日：2007-06-26
Applicant: 현대자동차주식회사
CPC classification number: H01M4/921 , H01M4/926 , H01M2008/1095
Abstract: A method for preparing a mixed electrode catalyst material for a solid electrolyte fuel cell is provided to reduce the amount of platinum required for producing a high-quality electrode catalyst, thereby reducing the manufacturing cost of an electrode catalyst and fuel cell. A method for preparing a mixed electrode catalyst material for a solid electrolyte fuel cell comprises the steps of: (a) dispersing a RuOs alloy material dispersed in the state of highly dispersed crystalline nanoparticles into water, injecting nitrogen thereto to remove undesired gases, and preliminarily injecting hydrogen thereto as a reducing agent; introducing a platinum precursor solution to the dispersion of RuOs alloy material and further injecting hydrogen thereto for 1 hour after the completion of the platinum precursor; and (c) washing and drying the resultant product after the completion of the hydrogen injection to obtain a powdery material.
Abstract translation: 提供一种制备用于固体电解质燃料电池的混合电极催化剂材料的方法，以减少生产高质量电极催化剂所需的铂的量，从而降低电极催化剂和燃料电池的制造成本。 制备用于固体电解质燃料电池的混合电极催化剂材料的方法包括以下步骤：（a）将分散在高度分散的结晶纳米颗粒状态的RuO x合金材料分散在水中，向其中注入氮气以除去不期望的气体， 将氢气注入其中作为还原剂; 向RuO合金材料的分散体中引入铂前体溶液，并在铂前体完成后进一步注入氢气1小时; 和（c）在完成氢气注入之后洗涤和干燥所得产物以获得粉状材料。
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公开(公告)号：KR100774746B1
公开(公告)日：2007-11-08
申请号：KR1020060092809
申请日：2006-09-25
Applicant: 현대자동차주식회사
IPC: B01J23/42
CPC classification number: B01J23/42 , B01J21/18 , B01J35/006 , B01J35/0066 , B01J37/16 , H01M4/92 , H01M4/926
Abstract: A preparation method of a highly dispersed Pt supported catalyst is provided to improve Pt particle size and dispersibility. A method for preparing a highly dispersed Pt supported catalyst comprises the steps of: preparing a complex reducing agent by mixing ethylene glycol with sodium borohydride at a molar ratio of 1:0.01 to 1:0.1 and a temperature of 0 to 50 deg.C for 30 minutes to 3 hours; dispersing a Pt precursor and a carbon support into a solvent at a molar ratio of 1:9 to 8:2; mixing the complex reducing agent with the dispersed solvent at 0 to 50 deg.C for 30 minutes to 2 hours to prepare a mixed solution of the Pt precursor, the carbon support and the complex reducing agent; heat-treating the mixed solution of the Pt precursor, the carbon support, and the complex reducing agent at 40 to 80 deg.C for 3 to 10 hours; and filtering and cleaning the mixture after mixing the heat-treated mixed solution of the Pt precursor, the carbon support and the complex reducing agent with an aqueous hydrochloric acid solution at a volume ratio of 1:0.5 to 1:2 and a temperature of 0 to 50 deg.C for 20 minutes to 2 hours.
Abstract translation: 提供高度分散的Pt负载催化剂的制备方法以改善Pt粒度和分散性。 制备高度分散的Pt负载催化剂的方法包括以下步骤：通过将乙二醇与硼氢化钠以1:0.01至1:0.1的摩尔比和0至50℃的温度混合来制备络合还原剂，用于 30分钟至3小时; 将Pt前体和碳载体以1:9至8:2的摩尔比分散在溶剂中; 在0〜50℃下将复合还原剂与分散溶剂混合30分钟〜2小时，制备Pt前体，碳载体和络合物还原剂的混合溶液; 将Pt前体，碳载体和络合物还原剂的混合溶液在40〜80℃下热处理3〜10小时; 并将该Pt前体，碳载体和络合还原剂的热处理混合溶液与盐酸水溶液以体积比为1:0.5至1:2并且温度为0℃混合后过滤和清洗混合物 至50℃，持续20分钟至2小时。
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公开(公告)号：KR101935051B1
公开(公告)日：2019-01-04
申请号：KR1020160147819
申请日：2016-11-08
Applicant: 현대자동차주식회사 , 기아자동차주식회사 , 엘에스오토모티브테크놀로지스 주식회사
IPC: B60R25/31 , B60R21/015 , B60R16/03
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公开(公告)号：KR1020120107397A
公开(公告)日：2012-10-02
申请号：KR1020110025067
申请日：2011-03-21
Applicant: 현대자동차주식회사 , 서울대학교산학협력단
CPC classification number: H01M4/8825 , H01M4/8807 , H01M4/8892 , H01M2008/1095 , Y02E60/50
Abstract: PURPOSE: A manufacturing method of an electrode for a fuel cell is provided to continuously maintain a catalyst layer and a porous structure for operation of a fuel cell, to be able to manufacture a pore structure with various sizes and distributions, and to facilitate control of the catalyst layer and the porous structure. CONSTITUTION: A manufacturing method of a Catalyst layer-combined electrode for a polymer electrolyte membrane fuel cell comprises: a step of providing plate-like porous metal foam(2,2a,2b) or a metal aerogel having a porous structure of nanometer or micron size; a step of manufacturing a catalyst layer-integrated electrode by fixing a catalyst to the metal foam or metal aerogel. The manufacturing method additionally comprises a step of impregnating an ion-conducting material into the catalyst layer-integrated electrode. [Reference numerals] (AA,EE) Gas; (BB,FF) Liquid; (CC) Large pores; (DD) Small pores; (GG,JJ) Electron; (HH, II) Ion
Abstract translation: 目的：提供一种用于燃料电池的电极的制造方法，以连续地维持燃料电池的催化剂层和多孔结构，以能够制造各种尺寸和分布的孔结构，并且有助于控制 催化剂层和多孔结构。 构成：用于聚合物电解质膜燃料电池的催化剂层组合电极的制造方法包括：提供板状多孔金属泡沫（2,2a，2b）或具有纳米或微米多孔结构的金属气凝胶的步骤 尺寸; 通过将催化剂固定到金属泡沫或金属气凝胶来制造催化剂层一体化电极的步骤。 该制造方法还包括将离子传导材料浸渍到催化剂层一体化电极中的步骤。 （标号）（AA，EE）气体; （BB，FF）液体; （CC）大孔; （DD）小孔; （GG，JJ）电子; （HH，II）离子
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