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    METHODS FOR PRODUCING (METH)ACRYLIC ACID NORBORNYL ESTERS
    51.
    发明专利
    METHODS FOR PRODUCING (METH)ACRYLIC ACID NORBORNYL ESTERS 未知

    公开(公告)号：ZA201905540B

    公开(公告)日：2021-05-26

    申请号：ZA201905540

    申请日：2019-08-22

    Applicant: BASF SE

    Inventor： MISSKE ANDREA ,  FLECKENSTEIN CHRISTOPH ,  FLEISCHHAKER FRIEDERIKE

    Abstract: A method for preparing norbornyl (meth)acrylate by reacting norbornene with (meth)acrylic acid in the presence of boron trifluoride as catalyst, whereina) boron trifluoride is initially charged in (meth)acrylic acid or an organic solvent,b) the initial charge is heated to a temperature of 75 to 110° C.,c) norbornene is added or a mixture comprising norbornene and (meth)acrylic acid is added andd) the norbornyl (meth)acrylate obtained is isolated from the reaction mixture.

    PROCESS FOR PRODUCING GLYCEROL CARBONATE METHACRYLATE
    52.
    发明专利
    PROCESS FOR PRODUCING GLYCEROL CARBONATE METHACRYLATE 未知

    公开(公告)号：SG11202004117SA

    公开(公告)日：2020-07-29

    申请号：SG11202004117S

    申请日：2018-12-07

    Applicant: BASF SE

    Inventor： MISSKE ANDREA ,  FLECKENSTEIN CHRISTOPH ,  KLUEGLEIN MATTHIAS

    IPC: C07D317/38

    Abstract: A process for preparing glycerol carbonate methacrylate, wherein glycidyl methacrylate is reacted with carbon dioxide in the presence of a catalyst and a solvent,wherein the catalyst is potassium iodide, the solvent is acetonitrile, one or more monoalcohols, or any desired mixture of acetonitrile and one or more monoalcohols, and the reaction of glycidyl methacrylate with carbon dioxide is carried out at a pressure from 0.5 to 5 bar.

    Procedimiento para la preparación de di(met)acrilato de etoxilato de isosorbida
    53.
    发明专利
    Procedimiento para la preparación de di(met)acrilato de etoxilato de isosorbida 未知

    公开(公告)号：ES2745682T3

    公开(公告)日：2020-03-03

    申请号：ES16705967

    申请日：2016-02-24

    Applicant: BASF SE

    Inventor： MISSKE ANDREA ,  FLEISCHHAKER FRIEDERIKE ,  FLECKENSTEIN CHRISTOPH ,  KALLER MARTIN ,  STENGEL ULRIK ,  BLANCHOT MATHIEU ,  STOER CLAUDIA ,  NAIR RITESH

    IPC: C09J4/00 ,  C07D493/04 ,  C08F222/10 ,  C09J4/06

    Abstract: Procedimiento para la preparación de di(met)acrilato de etoxilato de isosorbida mediante transesterificación de (met)acrilato de alquilo con etoxilato de isosorbida, que comprende las etapas: (i) etoxilar isosorbida para dar etoxilato de isosorbida, (ii) dejar reaccionar (met)acrilato de alquilo con etoxilato de isosorbida en presencia de fosfato de potasio como catalizador y de un estabilizador y en presencia de un agente arrastrador, que forma un azeótropo con el alcohol unido en el (met)acrilato de alquilo, (iii) separar por destilación de manera continua el azeótropo constituido por agente arrastrador y alcohol, realizándose las etapas (ii) y (iii) al mismo tiempo hasta que haya reaccionado esencialmente de manera completa el etoxilato de isosorbida, (iv) separar el catalizador de la mezcla de producto que contiene di(met)acrilato de etoxilato de isosorbida, (v) separar por destilación el (met)acrilato de alquilo que no ha reaccionado y agente arrastrador de la mezcla de producto.

    СПОСОБ ПОЛУЧЕНИЯ ИЗОСОРБИДЭТОКСИЛАТДИ(МЕТ)АКРИЛАТА
    54.
    发明专利
    СПОСОБ ПОЛУЧЕНИЯ ИЗОСОРБИДЭТОКСИЛАТДИ(МЕТ)АКРИЛАТА 未知

    公开(公告)号：RU2702013C2

    公开(公告)日：2019-10-03

    申请号：RU2017133280

    申请日：2016-02-24

    Applicant: BASF SE

    Inventor： MISSKE ANDREA ,  FLAJSHKHAKER FRIDERIKE ,  FLEKKENSHTAJN KRISTOF ,  KALLER MARTIN ,  SHTENGEL ULRIK ,  BLANKHOT METYU ,  SHTER KLAUDIA ,  NAIR RITESH

    IPC: C07D493/04 ,  C09J4/02

    Abstract: Изобретениеотноситсяк способуполученияизосорбидэтоксилатди(мет)акрилатапутемпереэтерификацииалкил(мет)акрилата, выбранногоизметил- илиэтил(мет)акрилата, изосорбидэтоксилатом, включающемустадии: (i) этоксилированияизосорбидас образованиемизосорбидэтоксилата, (ii) взаимодействияупомянутогоалкил(мет)акрилатас изосорбидэтоксилатомв присутствиифосфатакалияв качествекатализатораи стабилизатораи вприсутствииазеотропообразователя, представляющегособойалкил(мет)акрилат, выбранногоизметил- илиэтил(мет)акрилата, которыйобразуетазеотропсоспиртом, связаннымв алкил(мет)акрилат, (iii) непрерывнойотгонкиазеотропаизазеотропообразователяи спирта, причемстадии (ii) и (iii) проводятодновременнодотехпор, покаизосорбидэтоксилатпосуществуполностьюнепрореагирует, (iv) отделениякатализатораизсмесипродуктов, содержащейизосорбидэтоксилатди(мет)акрилат, (v) отгонкинепрореагировавшегоалкил(мет)акрилатаи азеотропообразователяизсмесипродуктов. 6 з.п. ф-лы, 2 пр.

    PROCESS FOR PREPARING HEONONE (METH)ACRYLATE
    58.
    发明专利
    PROCESS FOR PREPARING HEONONE (METH)ACRYLATE 未知

    公开(公告)号：CA2968753A1

    公开(公告)日：2016-06-09

    申请号：CA2968753

    申请日：2015-11-30

    Applicant: BASF SE

    Inventor： MISSKE ANDREA ,  FLEISCHHAKER FRIEDERIKE ,  FLECKENSTEIN CHRISTOPH ,  KALLER MARTIN ,  STENGEL ULRIK ,  BLANCHOT MATHIEU ,  NAIR RITESH

    IPC: C07D263/38

    Abstract: The invention relates to a method for producing Heonon(meth)acrylate via the transesterification of alkyl(meth)acrylate with Heonon, comprising the following steps: (i) permitting alkyl(meth)acrylate to react with Heonon in the presence of a catalyst containing titanium (IV) or zirconium (IV) and a stabiliser in the presence of an entrainer, forming an azeotrope with the alcohol bonded in the alkyl(meth)alcylate; (ii) continuous distilling off of the azeotrope from the entrainer and alcohol, wherein steps (i) and (ii) are carried out simultaneously, until heonon is substantially completely converted; (iii) adding water to the product mixture obtained in steps (i) and (ii) and containing heonon(meth)acrylate, and separating the hydrolysate from the catalyst containing titanium (IV) or zirconium (IV) by means of filtration; (iv) distilling off of non-converted alkyl(meth)acrylate and entrainer from the product mixture; (v) distilling off of water from the product mixture, wherein step (iv) can also be carried out before step (iii), and the steps (iv) and (v) can also be carried out in a distillation step, characterised in that the steps (i) and (ii) are carried out in the presence of an inorganic or organic acid.

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