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    신규 고리화합물과 이의 제조방법
    71.
    发明公开
    신규 고리화합물과 이의 제조방법 失效
    新型循环化合物及其制备方法

    公开(公告)号：KR1020090118417A

    公开(公告)日：2009-11-18

    申请号：KR1020080044182

    申请日：2008-05-13

    Applicant: 강원대학교산학협력단

    Inventor： 이필호 ,  강영진 ,  김현석

    IPC: C07D309/34 ,  C07D309/36

    Abstract: PURPOSE: A novel cyclic compound and a manufacturing method are provided to use as a good precursor in natural material synthesis or medicinal or pharmaceutical filed. CONSTITUTION: A cyclic compound is denoted by the chemical formula 1a. In the chemical formula 1a, D1-X1 is CX1 or CX1X2; D2-X2 is oxygen(O), CX1X2, or CX2; A is H or straight or branched C1-C10 alkyl; and R1 and R2 are same or different H, straight or branched C1-C10 alkyl or phenyl.

    Abstract translation: 目的：提供一种新型的环状化合物和制备方法，用作天然物质合成或药用或药物领域的良好前体。 构成：化学式1a表示环状化合物。 在化学式1a中，D1-X1为CX1或CX1X2; D2-X2是氧（O），CX1X2或CX2; A为H或直链或支链C 1 -C 10烷基; 并且R 1和R 2是相同或不同的H，直链或支链C 1 -C 10烷基或苯基。

    알릴알렌 유도체와 이의 제조방법
    72.
    发明公开
    알릴알렌 유도체와 이의 제조방법 失效
    ALLYL ALLENE化合物及其合成

    公开(公告)号：KR1020090077335A

    公开(公告)日：2009-07-15

    申请号：KR1020080003208

    申请日：2008-01-10

    Applicant: 강원대학교산학협력단

    Inventor： 이필호 ,  김진호 ,  이중연

    IPC: C07C11/14 ,  C07C11/21

    Abstract: A method for preparing an allyl allene derivative is provided to synthesize an allyl allene derivative at good yield by reacting an allyl indium reagent with a propargyl alcohol derivative without a separate refining process. A method for preparing an allyl allene derivative has a structure of chemical formula 1. In the chemical formula 1, R1 and R2 show C1-C6 alkyl group, or substituted or unsubstituted phenyl group, or R1 and R2 form 5-8-membered cycloalkyl ring; R3 and R4 show hydrogen atom, C1-C6 alkyl group, substituted or unsubstituted phenyl group, or phenyl-C1-C6 alkylene group. The substituted phenyl group is a phenyl group substituted with substituents selected from halide, hydroxyl, C1-C6 alkyl, C1-C6 alkoxy, ketone, ester, nitro, amide, aldehyde and amine.

    Abstract translation: 提供烯丙基丙烯衍生物的制备方法，通过使烯丙基铟试剂与炔丙醇衍生物反应而不用单独的精制方法，以良好的收率合成烯丙基全烯衍生物。 制备烯丙基全烯衍生物的方法具有化学式1的结构。在化学式1中，R 1和R 2表示C 1 -C 6烷基或取代或未取代的苯基，或R 1和R 2形成5-8元环烷基 环; R3和R4表示氢原子，C1-C6烷基，取代或未取代的苯基或苯基-C1-C6亚烷基。 取代的苯基是被选自卤素，羟基，C 1 -C 6烷基，C 1 -C 6烷氧基，酮，酯，硝基，酰胺，醛和胺的取代基取代的苯基。

    호모알렌일 알코올 유도체와 인듐을 이용한 이의 제조방법
    73.
    发明授权
    호모알렌일 알코올 유도체와 인듐을 이용한 이의 제조방법 失效
    均烯醇和它们的合成使用铟

    公开(公告)号：KR100906478B1

    公开(公告)日：2009-07-08

    申请号：KR1020080003212

    申请日：2008-01-10

    Applicant: 강원대학교산학협력단

    Inventor： 이필호 ,  김진호 ,  박찬수

    IPC: C07C69/66 ,  C07C11/14

    Abstract: A method for preparing a homoallenyl alcohol derivative is provided to selectively synthesize the homoallenyl alcohol derivative at high yield by reacting a synthesized organic indium reagent and an aldehyde compound. A method for preparing a homoallenyl alcohol derivative represented by chemical formula 1 comprises the steps of: reacting indium and propargyl chloride substituted with an ester group represented by chemical formula 2 to prepare an organic indium reagent; and adding an aldehyde compound represented by chemical formula 4. In chemical formula 1, 2 and 3, X is a halogen atom; R1 is a C1-C6 alkyl group; and R2 is a hydrogen atom, C1-C6 alkyl group, C3-C8 cycloalkyl group, phenyl group or phenyl-C1-C6 alkylene group. The benzene ring of phenyl or phenyl-C1-C6 alkylene group can be substituted or unsubstituted with 1-4 substituents selected from halogen, hydroxyl, nitro, C1-C6 alkyl, C1-C6 alkoxy, C1-C6 acyl and C1-C6 alkoxycarbonyl.

    Abstract translation: 提供一种制备均聚烯醇衍生物的方法，通过使合成的有机铟试剂和醛化合物反应，以高产率选择性地合成均聚烯醇衍生物。 制备由化学式1表示的均烯醇衍生物的方法包括以下步骤：使由化学式2表示的酯基取代的铟和炔丙基反应制备有机铟试剂; 并加入由化学式4表示的醛化合物。在化学式1,2和3中，X是卤原子; R1是C1-C6烷基; 并且R 2是氢原子，C 1 -C 6烷基，C 3 -C 8环烷基，苯基或苯基-C 1 -C 6亚烷基。 苯基或苯基-C 1 -C 6亚烷基的苯环可以被1-4个选自卤素，羟基，硝基，C 1 -C 6烷基，C 1 -C 6烷氧基，C 1 -C 6酰基和C 1 -C 6烷氧基羰基的取代基取代或未取代 。

    다이하이드로퓨란 유도체와 금 촉매를 이용한 이의제조방법
    74.
    发明公开
    다이하이드로퓨란 유도체와 금 촉매를 이용한 이의제조방법 失效
    二氢呋喃衍生物及其制备方法，使用所有催化剂

    公开(公告)号：KR1020090061510A

    公开(公告)日：2009-06-16

    申请号：KR1020070128538

    申请日：2007-12-11

    Applicant: 강원대학교산학협력단

    Inventor： 이필호 ,  박용광 ,  김선대

    IPC: C07D307/28

    Abstract: A method for manufacturing a dihydrofuran derivative using a gold catalyst is provided to manufacture the dihydrofuran derivative with high yield under the presence of gold (Au) catalyst through cyclization of allenine-1,6-diol derivative. A dihydrofuran derivative of the chemical formula 1 is produced by cyclization of allenine-1,6-diol derivative of the chemical formula 2 under the presence of gold (Ag). In the chemical formula 1, A and B is hydrogen atom; C1-C6 alkyl group, C5-C8 cycloalkyl group; and phenyl group substituted with halogen, nitro, C1-C6 alkoxy, C2-C6 alkylcarbonyl, C2-C6 alkoxycarbonyl or C2-C6 alkanoate or non-substituted; phenyl-C1-C6 alkylene group; or 5-8 angular heterocyclic group containing oxygen. The gold (Au) catalyst is a compound containing Au^+ or Au^3+. The gold (Au) catalyst is used as 0.01-0.5 equivalent weight range to the allenine-1,6-diol derivative of the chemical formula 3.

    Abstract translation: 提供使用金催化剂制造二氢呋喃衍生物的方法，通过环烯-1,6-二醇衍生物的环化在金（Au）催化剂的存在下以高产率制备二氢呋喃衍生物。 化学式1的二氢呋喃衍生物是通过在金（Ag）存在下环化化学式2的联苯-1,6-二醇衍生物来制备的。 在化学式1中，A和B是氢原子; C1-C6烷基，C5-C8环烷基; 被卤素，硝基，C 1 -C 6烷氧基，C 2 -C 6烷基羰基，C 2 -C 6烷氧基羰基或C 2 -C 6链烷酸酯取代的苯基或未取代的苯基; 苯基-C 1 -C 6亚烷基; 或含有氧的5-8个杂环基。 金（Au）催化剂是含Au ^ +或Au ^ 3 +的化合物。 金（Au）催化剂的使用量与化学式3的联苯-1,6-二醇衍生物的0.01-0.5当量重。

    설파이드 화합물 및 유기 황-인듐 착물을 이용한설파이드화합물 제조방법
    75.
    发明公开
    설파이드 화합물 및 유기 황-인듐 착물을 이용한설파이드화합물 제조방법 有权
    硫酸盐合成方法，使用三硝基酚钠

    公开(公告)号：KR1020090055390A

    公开(公告)日：2009-06-02

    申请号：KR1020070122293

    申请日：2007-11-28

    Applicant: 강원대학교산학협력단

    Inventor： 이필호 ,  이재영

    IPC: C07C321/02 ,  C07C321/10

    CPC classification number: C07C319/14 ,  C07C321/30 ,  C07C321/20 ,  C07C323/61 ,  C07C323/62

    Abstract: A method for manufacturing sulfide compound is provided to synthesize a sulfide compound with good yield, to obtain quantitative yield even if an indium triorganothiolate reagent is used in only equivalent, and to produce by-products. A method for manufacturing sulfide compound using indium triorganothiolate comprises the steps of: inducing R^1 and R from electronphile represented by formula 3: R^1-Xm and indium triorganothiolate represented by formula 2: In(SR)3; and preparing a sulfide compound represented by formula 1: R^1(SR)n by using a transition metal. R^1 of chemical formula 1 is induced from R^1 of chemical formula 3 and is phenyl, an aromatic compound having C1-6 linear or branched alkyl group, an aromatic compound having C1-6 linear or branched alkoxy group, and an aromatic compound having halide, ester, nitro, aldehyde, ketone, cyanide, amide and carboxylic acid.

    Abstract translation: 提供硫化物化合物的制造方法，以合成具有良好收率的硫化物化合物，即使仅使用三氧硫酸铟试剂，也可生产副产物而获得定量产率。 使用三有机硫酸铟制造硫化物化合物的方法包括以下步骤：从由式3表示的电子诱导R 1和R 3：R 1-X m和由式2表示的三有机硫酸铟：In（SR）3; 并用过渡金属制备由式1表示的硫化物：R 1（SR）n。 化学式1的R 1是从化学式3的R 1'引发的，并且是苯基，具有C 1-6直链或支链烷基的芳族化合物，具有C 1-6直链或支链烷氧基的芳族化合物和芳香族 具有卤化物，酯，硝基，醛，酮，氰化物，酰胺和羧酸的化合物。

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