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    71.
    发明专利
    未知

    公开(公告)号：PT788475E

    公开(公告)日：2000-04-28

    申请号：PT95917966

    申请日：1995-04-26

    Applicant: BASF AG

    Inventor： ALBRECHT HARREUS DR ,  HARTMANN HORST ,  NORBERT GOTZ DR ,  HARALD RANG DR ,  HEIMANN FRANK ,  BORCHERS DIRK ,  MAYWALD VOLKER ,  BUSCHULTE THOMAS

    IPC: B01J23/02 ,  B01J31/02 ,  C07B61/00 ,  C07C239/20 ,  C07C249/12 ,  C07C251/54 ,  C07C309/66

    Abstract: PCT No. PCT/EP95/01581 Sec. 371 Date Nov. 4, 1996 Sec. 102(e) Date Nov. 4, 1996 PCT Filed Apr. 26, 1995 PCT Pub. No. WO95/30648 PCT Pub. Date Nov. 16, 1995Preparation of mixtures of O-phenoxyalkylhydroxylamines Ia and Ib (Ia): H2NOCH2CH(R1)OAr (Ib): H2NOCH(R1)CH2OAr and the corresponding salt mixtures by a) converting mixtures of isomers of O-(2-hydroxyethyl)oximes IIa and IIb (IIa): (III): into a mixture of sulfonates IVa and IVb (IVa): (IVb): b) reacting this mixture of IVa and IVb with a phenol HO-Ar (V) to give a mixture of O-phenoxyalkoximes VIa and VIb (VIa): (VIb): c) hydrolyzing this mixture in the presence of an acid and, if desired d) liberating the O-phenoxyalkylhydroxylamines Ia and Ib from the resulting salts using a mineral acid. Compounds Ia/Ib and VIa/VIb are important intermediates for crop protection agents.

    5-(DIOXABICYCLOHEPT-6-YL)-CYCLOHEXENONE OXIME ETHERS, THEIR PREPARATION AND THEIR USE
    73.
    发明专利
    5-(DIOXABICYCLOHEPT-6-YL)-CYCLOHEXENONE OXIME ETHERS, THEIR PREPARATION AND THEIR USE 未知

    公开(公告)号：CA2277019A1

    公开(公告)日：1998-07-16

    申请号：CA2277019

    申请日：1997-12-19

    Applicant: BASF AG

    Inventor： MAYWALD VOLKER ,  RHEINHEIMER JOACHIM ,  WESTPHALEN KARL-OTTO ,  MISSLITZ ULF ,  KARDORFF UWE ,  WALTER HELMUT

    IPC: A01N43/90 ,  C07D493/04

    Abstract: The invention concerns 5-(dioxabicyclohept-6-yl)-cyclohexenone oxime ethers of formula (I) in which the substituents have the following meanings: R1 is hydrogen, the equivalent of an agriculturally useful cation, C1-C10 alkylcarbonyl, C1-C10 alkylsulphonyl, C1-C10 alkylphosphonyl, benzoyl, benzene sulphonyl or benzene phosphonyl; R2 is C1-C6 alkyl; R3, in each case independently of each other, is hydrogen or C1-C4 alkyl; Z is a C1-C6 alkylene, C3-C6 alkenylene or C3-C6 alkinylene chain which can carry an exomethylene substituent (=CH2) and/or in each case a further one to three substituents selected from a group comprising C1-C3 alkyl substituents and halogen atoms; a C3-C6 alkylene or C4-C6 alkenylene chain which can carry between one and three C1-C3 alkyl substituents and which, in addition to methylene or methine units, contains one of the following bridge members: oxygen, sulphur, -SO-, -SO2- or -N(Ri)-, Ri standing for hydrogen, C1-C4 alkyl, C3-C6 alkenyl or C3-C6 alkinyl; R4 is hydrogen, halogen, phenyl, wherein the phenyl group can be unsubstituted, partially or completely halogenated, and, if it is not completely halogenated, can carry between one and three substituents having the meaning given in the claims. The invention also concerns the preparation of these substances and their use.

    76.
    发明专利
    未知

    公开(公告)号：BR9507611A

    公开(公告)日：1997-08-19

    申请号：BR9507611

    申请日：1995-04-26

    Applicant: BASF AG

    Inventor： RANG HARALD ,  GOETZ NORBERT ,  HARREUS ALBRECHT ,  BORCHERS DIRK ,  HARTMANN HORST ,  MAYWALD VOLKER ,  HEIMANN FRANK ,  BUSCHULTE THOMAS

    IPC: B01J23/02 ,  B01J31/02 ,  C07B61/00 ,  C07C239/20 ,  C07C249/12 ,  C07C251/54 ,  C07C309/66

    Abstract: PCT No. PCT/EP95/01581 Sec. 371 Date Nov. 4, 1996 Sec. 102(e) Date Nov. 4, 1996 PCT Filed Apr. 26, 1995 PCT Pub. No. WO95/30648 PCT Pub. Date Nov. 16, 1995Preparation of mixtures of O-phenoxyalkylhydroxylamines Ia and Ib (Ia): H2NOCH2CH(R1)OAr (Ib): H2NOCH(R1)CH2OAr and the corresponding salt mixtures by a) converting mixtures of isomers of O-(2-hydroxyethyl)oximes IIa and IIb (IIa): (III): into a mixture of sulfonates IVa and IVb (IVa): (IVb): b) reacting this mixture of IVa and IVb with a phenol HO-Ar (V) to give a mixture of O-phenoxyalkoximes VIa and VIb (VIa): (VIb): c) hydrolyzing this mixture in the presence of an acid and, if desired d) liberating the O-phenoxyalkylhydroxylamines Ia and Ib from the resulting salts using a mineral acid. Compounds Ia/Ib and VIa/VIb are important intermediates for crop protection agents.

    PROCESS FOR THE PREPARATION OF HYDROXYLAMINE ETHERS AND THEIR SALTS AND INTERMEDIATES FOR THIS PURPOSE
    78.
    发明专利
    PROCESS FOR THE PREPARATION OF HYDROXYLAMINE ETHERS AND THEIR SALTS AND INTERMEDIATES FOR THIS PURPOSE 未知

    公开(公告)号：CA2151817A1

    公开(公告)日：1994-07-07

    申请号：CA2151817

    申请日：1993-12-17

    Applicant: BASF AG

    Inventor： HARREUS ALBRECHT ,  GOETZ NORBERT ,  MAYWALD VOLKER ,  RANG HARALD ,  MISSLITZ ULF ,  KLEIN ULRICH

    IPC: C07C239/20 ,  C07C251/54 ,  C07C253/30 ,  C07C255/54 ,  C07C259/06 ,  C07C255/64

    Abstract: In order to prepare hydroxylamine-ethers having formula (I), in which X stands for NO2, CN, halogen, alkyl and halogen alkyl; Y stands for H, NO2, CN, halogen, alkyl and halogen alkyl; n equals 0 to 2 or 1 to 4 when Y and all X's stand for halogen; alk stands for possibly substituted alkylene, as well as their salts with mineral acids or strong organic acids, either a hydroxyimino compound having formula (II), in which R1 stands for alkyl, R2 stands for alkyl, alkoxy or R1 + R2 stand for an alkylene chain, is reacted in the presence of an alkali metal hydroxide, alkali metal alcoholate, alkali metal hydrogen carbonate or alkali metal carbonate as bases, or the corresponding anion of (II) is directly reacted with an alkilating agent having formula (III), in which R3 stands for possibly substituted alkyl or phenyl, so that an oximino derivate having formula (IV) is produced. The oximino derivative (IV) is split by a mineral acid or a strong organic acid into a salt of (I), and if desired the latter is converted into the free compound (I) by means of a base. The hydroxilamine-ethers (I) constitute intermediate products for plant protecting and pharmaceutical agents.

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