公开(公告)号：KR101225448B1

公开(公告)日：2013-01-24

申请号：KR1020120099051

申请日：2012-09-07

Applicant: 재단법인나주시천연염색문화재단

Inventor： 허북구 ,  윤여정 ,  김윤희 ,  김길수 ,  이승진 ,  김대국 ,  이은석

IPC: C09B67/38 ,  C09B61/00

CPC classification number: C09B7/00 ,  C09B61/00 ,  C09B67/0002 ,  C09B67/0003

Abstract: PURPOSE: An indigo composition is provided to be harmful for human body, to have high fastness when dyeing, to be used in dyeing without indigo pre-treatment and to have excellent dyeing effect. CONSTITUTION: A manufacturing method of an indigo composition comprises: a step of extracting polygonum indigo by hot water, pulverizing the extract condensation, freeze-drying and crushing the extract to manufacture an indican powder; a step of polygonum leaf in the shade and pulverizing the polygonum leaf to manufacture polygonum powder; a step of drying and pulverizing a gall tannin and glucose powder; a step of storing the mixture of the indican powder, the polygonum powder and the mixture of the gall tannin and glucose powder at room temperature; and a step of adding water to the mixture and oxidizing the mixture. [Reference numerals] (AA) Process; (BB) Harvesting polygonum trinctorium leaves; (CC) Extracting; (DD) Evaporating and powder storing; (EE) Storing; (FF) Indican+dried polygonum trinctorium leaf powder+glucose; (GG) Adding water; (HH) Indoxyl; (II) Hairdye and paint; (JJ) Oxidization; (KK) Indigo; (LL) Contents; (MM) Fresh polygonum trinctorium leaves contain indican and indican hydrolase; (NN) Inactivating the indican hydrolase by hot water-extracting at 80-100°C; (OO) Freeze-drying using a decompression evaporator and pulverizing(1,800-2,000 mesh); (PP) Sealing and storing at room temperature(storing thickened products at 1-5°C); (QQ) Sealing and storing after the moisture content of the indican+the dried polygonum trinctorium leaf powder+the glucose powder+nutgall tannin becomes 3% or less; (RR) Adding water to decompose inactivated indican with the hydrolase such that the moisture content of a composition become in 70-80%; (SS) Generating indoxyl and glucose by hydrolyzing the indican with the hydrolase; (TT) Using the indoxyl as paint or hairdye; (UU) Oxidizing in the air; (VV) Oxidizing the indoxyl to become blue and insoluble

Abstract translation: 目的：提供对人体有害的靛蓝组合物，染色时具有高坚牢度，用于无靛蓝预处理的染色中，具有优异的染色效果。 构成：靛蓝组合物的制造方法包括：通过热水提取ind靛的步骤，粉碎提取物的冷凝，冷冻干燥并粉碎提取物以制造指甲粉; 在树荫下一步um叶，粉碎um叶以制造um粉; 干燥并粉碎胆汁单宁和葡萄糖粉末的步骤; 在室温下储存指示剂粉末，um粉和胆汁单宁和葡萄糖粉末的混合物的混合物的步骤; 以及向混合物中加入水并氧化混合物的步骤。 （附图标记）（AA）工艺; （BB）收获um ium叶; （CC）提取; （DD）蒸发和粉末储存; （EE）存储; （FF）Indican +干um叶粉+葡萄糖; （GG）加水; （HH）吲哚基; （二）头发和油漆; （JJ）氧化; （KK）靛蓝; （LL）内容; （MM）新鲜um叶含有an an和indic an水解酶; （NN）在80-100℃下通过热水提取来灭活印度水解酶; （OO）使用减压蒸发器冷冻干燥并粉碎（1,800-2,000目）; （PP）室温密封保存（1-5℃保存加厚产品）; （QQ）标记水分含量+干燥um叶粉+葡萄糖+甘草单宁后的密封保存量为3％以下; （RR）加水分解水解酶的灭活指示剂，使组合物的水分含量达到70-80％; （SS）通过用水解酶水解标记产生吲哚和葡萄糖; （TT）使用indoxyl作为油漆或发丝; （UU）在空气中氧化; （VV）氧化吲哚氧基成蓝色和不溶