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公开(公告)号：WO2018020398A1
公开(公告)日：2018-02-01
申请号：PCT/IB2017/054475
申请日：2017-07-24
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： ELMORE, Douglas L. , GERLACH, Korbinian , KOBUSSEN, Gregory A. , LAI, Jack Wing , OXMAN, Joel D. , SCHMID, Rudolf , WELKER, Stefan K.
Abstract: Cure monitoring systems for and methods of monitoring polymerizable material to determine the degree of curing of the polymerizable material. A monitoring light source delivers visible monitoring light at one or more different visible wavelengths and a visible light detector detects the monitoring light diffusely reflected by the polymerizable material. The monitoring light has a wavelength of maximum emission (λmax-mon) that does not effectively induce polymerization of the polymerizable material. Change in intensity of the monitoring light reflected from the polymerizable material is used to determine when a selected degree of curing is reached in the polymerizable material.
Abstract translation: 用于监测可聚合材料以确定可聚合材料的固化程度的固化监测系统和方法。 监测光源以一种或多种不同的可见光波长发射可见监测光，可见光检测器检测由可聚合材料漫反射的监测光。 监测光具有不能有效引起可聚合材料聚合的最大发射波长（λmax-mon）。 使用从可聚合材料反射的监控光强度的变化来确定何时在可聚合材料中达到选定的固化程度。
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公开(公告)号：WO2019123260A2
公开(公告)日：2019-06-27
申请号：PCT/IB2018/060269
申请日：2018-12-18
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： KOBUSSEN, Gregory A. , ABUELYAMAN, Ahmed S. , HOMNICK, Paul J. , CRAIG, Bradley D. , LIN, Ying , SAHOUANI, Hassan , CAO, Chuntao , MOSER, William H. , WHITE, Kolby L. , RULE, Joseph D. , ZECH, Joachim
IPC: A61K6/083
Abstract: Disclosed herein are non-aqueous compositions including: a flowable Part A including at least one resin and Reactant A; and a flowable Part B including at least one resin and Reactant B; wherein at least one of flowable Part A and flowable Part B further includes a free radically polymerizable resin; wherein at least one of flowable Part A and flowable Part B further includes a free radical initiator system; wherein flowable Part A and flowable Part B are capable of being mixed to provide a flowable mixed composition; wherein when flowable Part A and flowable Part B are mixed, Reactant A and Reactant B are capable of interacting to cause a non-free radical reaction within a first staging time to provide a first staged stable consistency for the mixed composition; and wherein the mixed composition having the first staged stable consistency is capable of forming a hardened composition upon initiation of free radical polymerization.
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公开(公告)号：WO2010045096A2
公开(公告)日：2010-04-22
申请号：PCT/US2009/060082
申请日：2009-10-09
Inventor： KALGUTKAR, Rajdeep S. , KOBUSSEN, Gregory A.
IPC: A61K6/083
CPC classification number: A61K6/0023 , A61K6/0017 , A61K6/0073 , A61K6/0094 , A61K6/083 , C08L33/00
Abstract: The invention features a dental composition containing a fluorescent organic pigment, e.g. a hydroxyl substituted aryl guanamine an or a fluorescent compound encapsulated in a thermo plastic or thermo set polymer, in an amount that provides the composition with fluorescence resembling that of natural teeth.
Abstract translation: 本发明的特征在于含有荧光有机颜料的牙科组合物，例如， 羟基取代的芳基胍胺或封装在热塑性或热固性聚合物中的荧光化合物，其量使组合物具有类似于天然牙齿的荧光。
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4.发明申请
公开(公告)号：WO2021116859A1
公开(公告)日：2021-06-17
申请号：PCT/IB2020/061524
申请日：2020-12-04
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： WU, Tianyu , HUGHES, Gareth A. , SVENTEK, Bruce A. , STOLZENBURG, Fabian , CHEN, Jing , KOBUSSEN, Gregory A. , SMITHSON, Robert L. W.
Abstract: The present disclosure provides a polymer bond abrasive article formed of a continuous photocured polymer matrix having abrasive particles retained therein. The photocured polymer matrix includes at least one of an optical brightener or a light absorber, and the polymer bond abrasive article has a three-dimensional shape. An abrasive tool is also provided, including the abrasive article affixed to a shaft or a pad. Further, a method of making the polymer bond abrasive article is provided, including a) obtaining a photocurable composition liquid dispersion; b) selectively curing a portion of the photocurable composition; and repeating steps a) and b) to form the polymer bond abrasive article. The dispersion contains at least one photocurable component; abrasive particles; a photoinitiator; and at least one of an optical brightener or a light absorber.
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公开(公告)号：WO2018020443A1
公开(公告)日：2018-02-01
申请号：PCT/IB2017/054546
申请日：2017-07-26
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： ELMORE, Douglas L. , GERLACH, Korbinian , KOBUSSEN, Gregory A. , LAI, Jack Wing , OXMAN, Joel D. , SCHMID, Rudolf , WELKER, Stefan
Abstract: Dental curing light systems capable of monitoring the degree of curing of polymerizable dental material. A monitoring light source delivers visible monitoring light at one or more different visible wavelengths and a visible light detector detects the monitoring light diffusely reflected by the polymerizable dental material. The monitoring light has a wavelength of maximum emission (λmax-mon) that does not effectively induce polymerization of the polymerizable dental material. Change in intensity of the monitoring light reflected from the polymerizable dental material is used to determine when a selected degree of curing is reached in the polymerizable dental material.
Abstract translation: 能够监测可聚合牙科材料固化程度的牙科固化灯系统。 监测光源以一种或多种不同的可见波长传递可见监测光，并且可见光检测器检测由可聚合牙科材料漫反射的监测光。 监控光具有不能有效引起可聚合牙科材料聚合的最大发射波长（λmax-mon）。 使用可聚合牙科材料反射的监控光强度的变化来确定何时在可聚合牙科材料中达到选定的固化程度。
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Patent Agency Ranking
公开(公告)号：WO2019123260A3
公开(公告)日：2019-06-27
申请号：PCT/IB2018/060269
申请日：2018-12-18
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： KOBUSSEN, Gregory A. , ABUELYAMAN, Ahmed S. , HOMNICK, Paul J. , CRAIG, Bradley D. , LIN, Ying , SAHOUANI, Hassan , CAO, Chuntao , MOSER, William H. , WHITE, Kolby L. , RULE, Joseph D. , ZECH, Joachim
Abstract: Disclosed herein are non-aqueous compositions including: a flowable Part A including at least one resin and Reactant A; and a flowable Part B including at least one resin and Reactant B; wherein at least one of flowable Part A and flowable Part B further includes a free radically polymerizable resin; wherein at least one of flowable Part A and flowable Part B further includes a free radical initiator system; wherein flowable Part A and flowable Part B are capable of being mixed to provide a flowable mixed composition; wherein when flowable Part A and flowable Part B are mixed, Reactant A and Reactant B are capable of interacting to cause a non-free radical reaction within a first staging time to provide a first staged stable consistency for the mixed composition; and wherein the mixed composition having the first staged stable consistency is capable of forming a hardened composition upon initiation of free radical polymerization.
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7.发明申请DENTAL COMPOSITIONS COMPRISING NANOPARTICLES PROVIDING A REFRACTIVE INDEX DIFFERENTIAL BETWEEN POLYMERIZABLE RESIN AND FILLER 审中-公开包含纳米粒子的牙科组合物在可聚合树脂和填充剂之间提供折射率差异
公开(公告)号：WO2017136374A1
公开(公告)日：2017-08-10
申请号：PCT/US2017/015928
申请日：2017-02-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： CRAIG, Bradley D. , DUNBAR, Timothy D. , DEDE, Karsten , ECKERT, Adrain S. , ABUELYAMAN, Ahmed S. , KOBUSSEN, Gregory A. , THALACKER, Christoph H. , HOMNICK, Paul J.
CPC classification number: A61K6/0005 , A61K6/0008 , A61K6/0073 , A61K6/0094 , A61K6/024 , A61K6/083 , C08L33/08 , C08L33/10
Abstract: Dental compositions and methods of formulating a dental composition are described. In one embodiment, the dental composition comprises a polymerizable resin comprising one or more ethylenically unsaturated monomers or oligomers and nanoparticles. The nanoparticles have a refractive index of at least 1.600 and an average discrete or aggregate particle size of no greater than 100 nm. The dental composition further comprises inorganic metal oxide filler having a discrete or aggregate average particle size of at least 200 nm. The nanoparticles are present at a concentration to provide a refractive index differential between the cured polymerizable resin and inorganic metal oxide filler such that the contrast ratio of the dental composition is at least 40.
Abstract translation: 描述了牙科组合物和配制牙科组合物的方法。 在一个实施方案中，牙科组合物包含含有一种或多种烯键式不饱和单体或低聚物和纳米颗粒的可聚合树脂。 纳米粒子具有至少1.600的折射率和不大于100nm的平均离散或聚集粒度。 牙科组合物还包含具有至少200nm的离散或聚集平均粒度的无机金属氧化物填料。 纳米颗粒以一定浓度存在，以提供固化的可聚合树脂和无机金属氧化物填料之间的折射率差异，使得牙科组合物的对比率至少为40。
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公开(公告)号：WO2008083275A2
公开(公告)日：2008-07-10
申请号：PCT/US2007/089045
申请日：2007-12-28
Inventor： CRIAG, Bradley D. , KOBUSSEN, Gregory A.
CPC classification number: A61K6/0055 , A61K6/0005 , A61K6/005 , A61K6/0052 , A61K6/024 , A61K6/083 , A61K6/087 , A61K6/09 , C08L29/04 , C08L33/10 , C08L33/08 , C08L71/02 , C08L63/00 , C08L75/04
Abstract: A dental filler is disclosed. The filler is produced by admixing a metal oxide sol and a water-soluble organic binder; drying said mixed sol into a dried product; and calcining said dried product; wherein said filler is a substantially amorphous cluster. The filler can be mixed into a hardenable resin to provide radiopaque dental materials having desirable strength and aesthetic character.
Abstract translation: 公开了牙科填料。 填料通过混合金属氧化物溶胶和水溶性有机粘合剂而制备; 将所述混合溶胶干燥成干燥的产品; 并煅烧所述干燥产品; 其中所述填料是基本无定形的团簇。 可以将填料混合成可硬化的树脂，以提供具有期望的强度和美学特征的不透射线的牙科材料。
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公开(公告)号：WO2019123333A1
公开(公告)日：2019-06-27
申请号：PCT/IB2018/060371
申请日：2018-12-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： KOBUSSEN, Gregory A. , ABUELYAMAN, Ahmed S. , HOMNICK, Paul J. , CRAIG, Bradley D. , LIN, Ying , SAHOUANI, Hassan , CAO, Chuntao , MOSER, William H. , WHITE, Kolby L. , RULE, Joseph D. , ZECH, Joachim
IPC: A61K6/08
Abstract: Disclosed herein are non-aqueous compositions including: a flowable Part A including at least one resin and Reactant A; and a flowable Part B including at least one resin and Reactant B; wherein at least one of flowable Part A and flowable Part B further includes a free radically polymerizable resin; wherein at least one of flowable Part A and flowable Part B further includes a free radical initiator system; wherein flowable Part A and flowable Part B are capable of being mixed to provide a flowable mixed composition; wherein when flowable Part A and flowable Part B are mixed, Reactant A and Reactant B are capable of interacting to cause a non-free radical reaction within a first staging time to provide a first staged stable consistency for the mixed composition; wherein Reactant A comprises an acid and Reactant B comprises a base, and upon mixing flowable Part A and flowable Part B, the Reactant A acid is capable of reacting with the Reactant B base in an ionic acid-base reaction; and wherein the mixed composition having the first staged stable consistency is capable of forming a hardened dental composition upon initiation of free radical polymerization.
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10.发明申请
公开(公告)号：WO2019048963A1
公开(公告)日：2019-03-14
申请号：PCT/IB2018/056371
申请日：2018-08-22
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： PARKAR, Zeba , HANSEN, James D. , WU, Tianyu , FRANKE, Carsten , DUNBAR, Timothy D. , KOBUSSEN, Gregory A. , ABUELYAMAN, Ahmed S. , CRAIG, Bradley D.
IPC: A61C13/087 , A61K6/083 , A61K6/06 , A61C19/00 , C08K3/013 , C08F22/10 , C08F222/10 , B33Y10/00 , B33Y70/00 , B33Y80/00 , B29C64/124
Abstract: A radiation curable composition including at least one radiation hardenable component, a photo-initiator, and a filler material having a population of particulates in an amount greater than or equal to 50% by weight of the printable composition. The population of particulates exhibits a median diameter (D50) of greater than or equal to 0.3 micrometer on a volume-average basis as determined using the Particle Size Test Method, and the radiation curable composition exhibits a viscosity of less than or equal to 150 Pa s when measured using the Viscosity Test Method. A method, apparatus, and systems for producing composite articles by selectively exposing a portion of the radiation curable composition to a source of actinic radiation to at least partially cure the exposed portion of the radiation curable composition, thereby forming a hardened layer, preferably by an additive manufacturing process such as stereophotolithography, are also described. The composite articles may include composite dental restorations.
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