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    ACRYLIC MODIFIED POLYMERIC OPACIFIERS FOR USE IN ORGANIC MEDIA
    2.
    发明申请
    ACRYLIC MODIFIED POLYMERIC OPACIFIERS FOR USE IN ORGANIC MEDIA 审中-公开

    公开(公告)号：WO2020205332A1

    公开(公告)日：2020-10-08

    申请号：PCT/US2020/024438

    申请日：2020-03-24

    Applicant: ARKEMA INC.

    Inventor： LUJAN, Donovan K. ,  DEVONPORT, Wayne

    IPC: C08J9/16 ,  C08F285/00 ,  C08L51/00

    Abstract: Disclosed are voided latex particles, useful as opacifying agents for coating compositions containing organic solvents. The particles have a hollow interior, which substantially maintains its integrity after the particles are placed in contact with an organic solvent at 25°C for 30 days. The particles also have a hydrophilic polymeric interior shell surrounding the hollow interior that is swellable with an aqueous swelling solution. The particles have first and second polymeric intermediate shells, surrounding the interior shell, formed from polymers that are different from each other and different from the interior shell polymer. Finally, the particles have an outer polymeric shell, surrounding the interior shells, which is formed from up to 100% by weight, as polymerized units, of methyl methacrylate. The interior shells and the outer shell each have a Tg greater than 60°C. Also disclosed is a multi-stage emulsion process for making the particles.

    VOIDED LATEX PARTICLES
    3.
    发明申请
    VOIDED LATEX PARTICLES 审中-公开
    空隙胶乳颗粒

    公开(公告)号：WO2016028512A1

    公开(公告)日：2016-02-25

    申请号：PCT/US2015/044120

    申请日：2015-08-07

    Applicant: ARKEMA INC.

    Inventor： LIU, Lily ,  DEVONPORT, Wayne ,  STARK, Daniel E. ,  BOUDREAUX, Matthew F.

    IPC: B32B5/16

    CPC classification number: C08F285/00 ,  C08F6/006 ,  C08L51/003

    Abstract: A process for forming voided latex particles is improved by combining swelling and polymerization of an outer shell into a single step. The process includes contacting multi-stage emulsion polymer particles comprising a core, at least one intermediate shell, with a swelling agent, and polymerizing an outer shell after said contacting with swelling agent wherein the core and the at least one intermediate shell are contacted with swelling agent in the presence of less than 0.5% monomer based on the weight of the multi-stage emulsion polymer particles, and substantially all of the swelling occurs during polymerization of the outer shell.

    Abstract translation: 通过将外壳的溶胀和聚合组合到单个步骤中，形成空隙胶乳颗粒的方法得到了改进。 该方法包括使包含芯，至少一个中间壳的多级乳液聚合物颗粒与溶胀剂接触，并且在所述接触后使外壳聚合于溶胀剂，其中使芯和至少一个中间壳与溶胀 在基于多级乳液聚合物颗粒的重量计小于0.5％单体存在的情况下，基本上所有的溶胀都发生在外壳的聚合期间。

    WATER RESISTANT VOIDED POLYMER PARTICLES
    4.
    发明申请
    WATER RESISTANT VOIDED POLYMER PARTICLES 审中-公开

    公开(公告)号：WO2019164786A1

    公开(公告)日：2019-08-29

    申请号：PCT/US2019/018456

    申请日：2019-02-19

    Applicant: ARKEMA INC.

    Inventor： LIU, Lily ,  ANDES, Keith J. ,  DEVONPORT, Wayne ,  BOUDREAUX, Matthew F.

    IPC: B01J13/14 ,  C08F8/12 ,  C08F265/00

    Abstract: Latex emulsions and a process of making the same that incorporates voided latex particles having a core with a hydrophilic component; at least one intermediate shell with, as polymerized units, one or more hydrophilic monoethylenically unsaturated monomer, one or more nonionic monoethylenically unsaturated monomer, or mixtures thereof; an outer shell formed of a polymer having a Tg of at least 60? C; and a surface treatment applied to the outer shell in which a plurality of silicone oligomers with reactive functional groups are cross-linked with one another in order to provide a cross-linked outer surface. The core and the at least one intermediate shell are contacted with a swelling agent in the presence of less than 0.5% monomer based on the overall weight of the voided latex particles. In addition, one or more of the core, the intermediate shell, or the outer shell includes a surfactant.

    HYDROLYSIS RESISTANT VINYL ESTER CONTAINING LATEXES
    5.
    发明申请
    HYDROLYSIS RESISTANT VINYL ESTER CONTAINING LATEXES 审中-公开
    含水解抗水解乙烯基酯

    公开(公告)号：WO2017222979A1

    公开(公告)日：2017-12-28

    申请号：PCT/US2017/038124

    申请日：2017-06-19

    Applicant: ARKEMA INC.

    Inventor： LIU, Lily ,  DEVONPORT, Wayne ,  STARK, Daniel E. ,  BOUDREAUX, Matthew F.

    IPC: C08F285/00 ,  C08F265/04 ,  C08F265/06 ,  C08L51/00

    Abstract: A method of forming latex composite polymer particles produces hydrolysis resistant, composite polymer particles that can be used in aqueous latex compositions. Each of the latex composite polymer particles includes a first phase comprising a vinyl ester oligomer or polymer; optionally, an intermediate phase; and at least one second phase comprising an acrylic oligomer or polymer, a styrene oligomer or polymer, an acrylic-styrene copolymer, or mixtures thereof. The second phase and/or the intermediate phase at least partially encapsulates the first phase. The intermediate and second phases are more hydrophobic than the first phase. Optionally, the first phase, the second phase, and/or the intermediate phase may further comprise a cross-linking agent.

    Abstract translation: 形成胶乳复合聚合物颗粒的方法产生可用于含水胶乳组合物中的耐水解复合聚合物颗粒。 每个胶乳复合聚合物颗粒包括含有乙烯基酯低聚物或聚合物的第一相; 任选地，中间阶段; 和至少一个第二相，所述第二相包含丙烯酸低聚物或聚合物，苯乙烯低聚物或聚合物，丙烯酸 - 苯乙烯共聚物或其混合物。 第二阶段和/或中间阶段至少部分地包封第一阶段。 中间相和第二相比第一相更具疏水性。 任选地，第一阶段，第二阶段和/或中间阶段可以进一步包含交联剂。

    QUICK-SETTING COATING COMPOSITIONS WITH LOW PH STABILITY AND WATER RESISTANCE
    6.
    发明申请
    QUICK-SETTING COATING COMPOSITIONS WITH LOW PH STABILITY AND WATER RESISTANCE 审中-公开
    具有低PH稳定性和耐水性的快速涂层组合物

    公开(公告)号：WO2016209692A1

    公开(公告)日：2016-12-29

    申请号：PCT/US2016/037753

    申请日：2016-06-16

    Applicant: ARKEMA INC.

    Inventor： GROVE, Jeremy L. ,  KIM, Kyu-Jun ,  HU, Rong ,  DEVONPORT, Wayne

    IPC: C08L79/00 ,  C08L79/02 ,  C09D179/00 ,  C09D179/02

    CPC classification number: C08G73/024 ,  C08G65/2624 ,  C08L25/14 ,  C08L33/04 ,  C08L33/08 ,  C08L35/02 ,  C08L79/02 ,  C09D179/02 ,  C09J7/38 ,  C09J179/02

    Abstract: A latex product composition that includes an anionically-stabilized latex and one or more water soluble, polymers or polymeric adducts that have a backbone with a plurality of amine functional groups and hydroxyl functional groups. The polymers or polymeric adducts may be an addition product formed from at least one multifunctional amine compound reacted with one or more polyfunctional epoxy compounds, one or more monofunctional epoxy compounds, or a combination thereof. The amine compound and the one or more epoxy compounds are reacted to form polymers or polymeric adducts with the molar equivalent ratio of 1.3 to 3.8 amine functional group per epoxy functional group. The addition product may be present in about 0.1 to 15.0 wt. % and the at least one volatile base compound is present in about 1.0 wt. % to 10.0 wt. % based on the weight of the particles present in the anionically-stabilized latex.

    Abstract translation: 一种乳胶产品组合物，其包含阴离子稳定的胶乳和一种或多种具有多个胺官能团和羟基官能团的骨架的水溶性聚合物或聚合物加合物。 聚合物或聚合物加合物可以是由至少一种与一种或多种多官能环氧化合物，一种或多种单官能环氧化合物或其组合反应的多官能胺化合物形成的加成产物。 胺化合物和一种或多种环氧化合物反应形成聚合物或聚合物加合物，其摩尔当量比为每个环氧官能团1.3-3.8胺官能团。 加成产物可以以约0.1至15.0wt。 ％，并且至少一种挥发性碱性化合物以约1.0wt。 ％〜10.0重量％ 基于存在于阴离子稳定的胶乳中的颗粒的重量％。

    VOIDED LATEX PARTICLES
    7.
    发明申请
    VOIDED LATEX PARTICLES 审中-公开
    无声LATEX颗粒

    公开(公告)号：WO2016028511A1

    公开(公告)日：2016-02-25

    申请号：PCT/US2015/044119

    申请日：2015-08-07

    Applicant: ARKEMA INC.

    Inventor： LIU, Lily ,  DEVONPORT, Wayne ,  STARK, Daniel E. ,  BOUDREAUX, Matthew F.

    IPC: B32B3/00

    CPC classification number: C08J9/224 ,  C08F6/006 ,  C08F285/00 ,  C08J9/16 ,  C08J9/28 ,  C08J2201/04 ,  C08J2333/12 ,  C08J2433/12 ,  C08L51/003

    Abstract: A process for forming voided latex particles is improved by combining swelling and polymerization of an outer shell into a single step. The process includes contacting multi-stage emulsion polymer particles comprising a core, at least one intermediate shell, with a swelling agent, and polymerizing an outer shell after said contacting with swelling agent wherein the core and the at least one intermediate shell are contacted with swelling agent in the presence of less than 0.5% monomer based on the weight of the multi-stage emulsion polymer particles, and substantially all of the swelling occurs during polymerization of the outer shell.

    Abstract translation: 通过将外壳的溶胀和聚合结合到单一步骤中，可以改善形成空隙胶乳颗粒的方法。 该方法包括将包含核心，至少一个中间体外壳和溶胀剂的多级乳液聚合物颗粒接触，并且在与溶胀剂接触之后聚合外壳，其中芯部和至少一个中间壳体与膨胀物接触 基于多阶段乳液聚合物颗粒的重量，在小于0.5％的单体存在的情况下，基本上所有的溶胀都发生在外壳聚合过程中。

    VOIDED LATEX PARTICLES
    9.
    发明公开
    VOIDED LATEX PARTICLES 审中-公开
    空隙胶乳颗粒

    公开(公告)号：EP3194156A1

    公开(公告)日：2017-07-26

    申请号：EP15833136.3

    申请日：2015-08-07

    Applicant: Arkema, Inc.

    Inventor： LIU, Lily ,  DEVONPORT, Wayne ,  STARK, Daniel E. ,  BOUDREAUX, Matthew F.

    IPC: B32B3/00

    CPC classification number: C08J9/224 ,  C08F6/006 ,  C08F285/00 ,  C08J9/16 ,  C08J9/28 ,  C08J2201/04 ,  C08J2333/12 ,  C08J2433/12 ,  C08L51/003

    Abstract: A process for forming voided latex particles is improved by combining swelling and polymerization of an outer shell into a single step. The process includes contacting multi-stage emulsion polymer particles comprising a core, at least one intermediate shell, with a swelling agent, and polymerizing an outer shell after said contacting with swelling agent wherein the core and the at least one intermediate shell are contacted with swelling agent in the presence of less than 0.5% monomer based on the weight of the multi-stage emulsion polymer particles, and substantially all of the swelling occurs during polymerization of the outer shell.

    Abstract translation: 通过将外壳的溶胀和聚合结合成单一步骤来改进形成空隙胶乳颗粒的方法。 该方法包括使包含芯，至少一个中间壳的多级乳液聚合物颗粒与溶胀剂接触，并且在所述接触后使外壳聚合于溶胀剂，其中使芯和至少一个中间壳与溶胀 试剂在基于多级乳液聚合物颗粒的重量计小于0.5％的单体存在下进行，并且基本上所有的溶胀发生在外壳的聚合过程中。

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