A method of preparing purified alkanesulfonic acid
    1.
    发明公开
    A method of preparing purified alkanesulfonic acid 失效
    埃尔弗哈伦·赫尔斯特朗·赫雷斯特恩·阿尔坎苏伦斯

    公开(公告)号:EP0505692A1

    公开(公告)日:1992-09-30

    申请号:EP92101629.1

    申请日:1992-01-31

    CPC classification number: C07C303/44 Y02P20/582 C07C309/04

    Abstract: A process of preparing purified alkanesulfonic acid from crude aqueous alkanesulfonic acid containing oxidizable impurities wherein the crude material is treated with a sufficient amount of chlorine to convert the oxidizable impurities to alkanesulfonyl chloride and then hydrolyzing said alkanesulfonyl chloride to alkanesulfonic acid by heating.

    Abstract translation: 从含有可氧化杂质的粗制烷基磺酸水溶液中制备纯化的链烷磺酸的方法,其中用足够量的氯处理粗物质以将可氧化杂质转化为烷基磺酰氯,然后通过加热将所述烷烃磺酰氯水解成烷烃磺酸。

    Process for the preparation of alkane- and arenesulfonamides
    4.
    发明公开
    Process for the preparation of alkane- and arenesulfonamides 失效
    Verfahren zur Herstellung von Alkan- und Arensulfonamiden。

    公开(公告)号:EP0439687A1

    公开(公告)日:1991-08-07

    申请号:EP90120562.5

    申请日:1990-10-26

    CPC classification number: C07C303/38 C07C311/03

    Abstract: A process for the preparation of alkane- and arenesulfonamides in high purity and yield is provided. Ammonia or alkylamine is reacted under boiling conditions with an alkane- or arenesulfonyl halide in the absence of an added solvent. The heat of reaction is dissipated by the heat of vaporization of the ammonia or alkylamine.

    Abstract translation: 提供了一种以高纯度和高产量制备烷烃和芳烃磺酰胺的方法。 在不存在加入的溶剂的情况下,氨或烷基胺在沸腾条件下与烷烃或芳烃磺酰卤反应。 反应的热量由氨或烷基胺的蒸发热消散。

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