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公开(公告)号:DE10301703A1
公开(公告)日:2004-07-29
申请号:DE10301703
申请日:2003-01-17
Applicant: BASF AG
Inventor: KUHRS CHRISTIAN , DANZ ECKEHARD , STEINER WOLFGANG , RAHN RALF-THOMAS , GRASLER THOMAS , GEIER REINER , HARTH KLAUS , HOELZLE MARKUS
IPC: C07D251/60 , B01J21/04 , B01J21/12
Abstract: Production of melamine by urea decomposition using a solid catalyst takes place in a main reactor containing a catalyst of low Lewis acidity and a post-reactor containing a catalyst of the same or higher (especially higher) Lewis acidity.
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公开(公告)号:CA2691642A1
公开(公告)日:2008-12-24
申请号:CA2691642
申请日:2008-06-20
Applicant: BASF AG
Inventor: ISELBORN STEFAN , GEIER REINER , HEPFER BENJAMIN , BECHTEL MARCUS , WILLE MICHAEL , DAISS ANDREAS
Abstract: The invention relates to a reactor (R) for performing a three-phase react ion of a fluid phase (1) and a gaseous phase (2) on a packed bed catalyst (F ), the packed bed catalyst (F) being disposed horizontally in the reactor (R ) and the fluid phase (1) and the gaseous phase (2) being fed through the re actor (R) from the bottom to the top, using a mixing and distributing device (MV) across the packed bed catalyst (F), characterized in that the mixing a nd distributing device (MV) comprises a trough distributor (TV) for the flui d phase (1) having trough-shaped channels (K) and drain tubes (A) in the tro ugh-shaped channels (K) for the fluid phase (1), and a distributor floor (B) disposed below and at a distance from the trough distributor (TV) in which vertical spouts (T) are disposed, having one or more openings (P1) for the i nlet of the gaseous phase (2) and one or more openings (P2) disposed below t he openings (P1) for the inlet of the gaseous phase, for the inlet of the fl uid phase (1) into the spouts (T), and the number and size of the openings ( P2) for the inlet of the fluid phase (1) being designed such that the fluid level on the distribution floor (B) is adjusted to be below the openings (P1 ) for the inlet of the gaseous phase (2) and above the openings (P2) for the inlet of the fluid phase (1) for a prescribedinlet flow of fluid.
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公开(公告)号:DE10337501A1
公开(公告)日:2005-04-14
申请号:DE10337501
申请日:2003-08-14
Applicant: BASF AG
Inventor: KUHRS CHRISTIAN , DANZ ECKEHARD , STEINER WOLFGANG , RAHN RALF-THOMAS , GRASLER THOMAS , GEIER REINER , HARTH KLAUS , HOELZLE MARKUS
IPC: C07D251/60
Abstract: Production of melamine by urea decomposition using a solid catalyst takes place in a main reactor containing a catalyst of low Lewis acidity and a post-reactor containing a catalyst of the same or higher (especially higher) Lewis acidity.
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公开(公告)号:DE10342566A1
公开(公告)日:2005-04-07
申请号:DE10342566
申请日:2003-09-15
Applicant: BASF AG
Inventor: MUELLER-EVERSBUSCH MAYKE , SCHOENFELDER HENDRIK , GEIER REINER , HOELZLE MARKUS , GRASLER THOMAS , KUHRS CHRISTIAN , RAHN RALF-THOMAS
IPC: B01J8/00 , B01J8/18 , C07D251/60
Abstract: Producing melamine by reacting urea at 350-450[deg]C and up to 20 bar in the presence of a catalyst in the form of a fluidized bed comprises using a fluidized bed reactor with a conical base (5). An independent claim is also included for a reactor for carrying out the above process, comprising a product gas outlet (20) in a top section (19) of the reactor and a fluidizing gas inlet (8) located beneath the contents of the reactor, where the reactor is conical.
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