-
公开(公告)号:WO02081436A2
公开(公告)日:2002-10-17
申请号:PCT/EP0203656
申请日:2002-04-03
Applicant: BASF AG , HENNIG GUNNAR , BECHTEL MARCUS , FREUDENTHALER EVA , EIERMANN MATTHIAS
Inventor: HENNIG GUNNAR , BECHTEL MARCUS , FREUDENTHALER EVA , EIERMANN MATTHIAS
IPC: C07C319/24 , C07C321/14
CPC classification number: C07C319/24 , C07C321/14
Abstract: Disclosed is a method for producing organic disulphide by oxidation of the corresponding thiol with sulphur disolved in organic disulphide using an amine as a catalyst in a reaction column (K). The thiol used is a crude thiol flow from catalytic reaction of the corresponding primary alcohol with hydrogen sulphide and the bases of the reaction column (K) are temperable.
Abstract translation: 它提出了一种方法,用于通过相应的硫醇与使用胺作为在反应塔(K)的催化剂溶解于有机二硫化物硫的氧化,制备有机二硫化物,其中,从一个催化转化相应的粗硫醇流的硫醇 伯醇被用于与硫化氢和反应塔(K)上设置有可加热的地板。
-
公开(公告)号:AU2002308119A1
公开(公告)日:2002-10-21
申请号:AU2002308119
申请日:2002-04-03
Applicant: BASF AG
Inventor: HENNIG GUNNAR , FREUDENTHALER EVA , BECHTEL MARCUS , EIERMANN MATTHIAS
IPC: C07C319/24 , C07C321/14 , B01D3/16
-
公开(公告)号:CA2691642A1
公开(公告)日:2008-12-24
申请号:CA2691642
申请日:2008-06-20
Applicant: BASF AG
Inventor: ISELBORN STEFAN , GEIER REINER , HEPFER BENJAMIN , BECHTEL MARCUS , WILLE MICHAEL , DAISS ANDREAS
Abstract: The invention relates to a reactor (R) for performing a three-phase react ion of a fluid phase (1) and a gaseous phase (2) on a packed bed catalyst (F ), the packed bed catalyst (F) being disposed horizontally in the reactor (R ) and the fluid phase (1) and the gaseous phase (2) being fed through the re actor (R) from the bottom to the top, using a mixing and distributing device (MV) across the packed bed catalyst (F), characterized in that the mixing a nd distributing device (MV) comprises a trough distributor (TV) for the flui d phase (1) having trough-shaped channels (K) and drain tubes (A) in the tro ugh-shaped channels (K) for the fluid phase (1), and a distributor floor (B) disposed below and at a distance from the trough distributor (TV) in which vertical spouts (T) are disposed, having one or more openings (P1) for the i nlet of the gaseous phase (2) and one or more openings (P2) disposed below t he openings (P1) for the inlet of the gaseous phase, for the inlet of the fl uid phase (1) into the spouts (T), and the number and size of the openings ( P2) for the inlet of the fluid phase (1) being designed such that the fluid level on the distribution floor (B) is adjusted to be below the openings (P1 ) for the inlet of the gaseous phase (2) and above the openings (P2) for the inlet of the fluid phase (1) for a prescribedinlet flow of fluid.
-
公开(公告)号:DE10139587A1
公开(公告)日:2003-02-20
申请号:DE10139587
申请日:2001-08-11
Applicant: BASF AG
Inventor: BECHTEL MARCUS , THIEL JOACHIM
IPC: B01D3/00
Abstract: A distillation column has a liquid distributor fabricated of glass. The distributor has one or more liquid distributor gullies into which one or more glass tubes are secured by heat partial-melting. Each glass tube has one or more lateral 3 mm drill holes clear of the gully and facilitating fluid flow.
-
公开(公告)号:DE10139588A1
公开(公告)日:2003-02-27
申请号:DE10139588
申请日:2001-08-11
Applicant: BASF AG
Inventor: BECHTEL MARCUS , THIEL JOACHIM
IPC: B01D3/00 , B01D3/20 , C07C303/44 , C07C309/04 , C07C303/02
Abstract: Glass apparatus to gather and distribute fluid in a column (1) has a gutter system (2) with blades (3) to collect the fluid, and a central tube (4) as an outflow for the fluid. The glass distributor (5) has several distribution gutters with fused glass tube(s) that project over the base of the gutters. Glass apparatus to gather and distribute fluid in a column (1) has a gutter system (2) with blades (3) to collect the fluid, and a central tube (4) as an outflow for the fluid. The glass distributor (5) has several distribution gutters with fused glass tube(s) that project over the base of the gutters, with a side opening for the fluid to flow into them with a drilling diameter of .
-
公开(公告)号:DE10116817A1
公开(公告)日:2002-10-17
申请号:DE10116817
申请日:2001-04-04
Applicant: BASF AG
Inventor: HENNIG GUNNAR , BECHTEL MARCUS , FREUDENTHALER EVA , EIERMANN MATTHIAS
IPC: C07C319/24 , C07C321/14
Abstract: Disclosed is a method for producing organic disulphide by oxidation of the corresponding thiol with sulphur disolved in organic disulphide using an amine as a catalyst in a reaction column (K). The thiol used is a crude thiol flow from catalytic reaction of the corresponding primary alcohol with hydrogen sulphide and the bases of the reaction column (K) are temperable.
-
公开(公告)号:MY140932A
公开(公告)日:2010-02-12
申请号:MYPI20060062
申请日:2006-01-06
Applicant: BASF AG
Inventor: PESCHEL WERNER DR , KUMMER MATTHIAS DR , BECHTEL MARCUS
IPC: B01D3/42
Abstract: PROCESS FOR THE PREPARATION OF ON-SPEC PHTHALIC ANHYDRIDE BY THE DISTILLATIVE PURIFICATION OF CRUDE PHTHALIC ANHYDRIDE AT REDUCED PRESSURE, WHERE THE CRUDE PHTHALIC ANHYDRIDE IS PASSED TO THE DISTILLATION COLUMN ABOVE A SIDE TAKE-OFF, THE LOW-BOILING COMPONENTS ARE REMOVED AT THE TOP OF THE COLUMN OR IN THE VICINITY OF THE TOP OF THE COLUMN AND THE ON-SPEC PHTHALIC ANHYDRIDE IS REMOVED FROM THE SIDE TAKE-OFF OF THE COLUMN, IN WHICH A DISTILLATION COLUMN IS USED WHOSE NUMBER OF THEORETICAL PLATES LOCATED ABOVE THE SUPPLY OF THE CRUDE PHTHALIC ANHYDRIDE INTO THE DISTILLATION COLUMN IS 10 TO 20 AND THE COLUMN IS OPERATED AT A REFLUX RATIO OF FROM 0.1 TO 0.5.
-
公开(公告)号:MX2007008175A
公开(公告)日:2007-08-06
申请号:MX2007008175
申请日:2005-12-31
Applicant: BASF AG
Inventor: PESCHEL WERNER , KUMMER MATTHIAS , BECHTEL MARCUS
IPC: B01D3/42 , C07C51/573 , C07D307/89
Abstract: Proceso para la preparacion de anhidrido ftalico segun especificaciones, mediante purificacion por destilacion del anhidrido ftalico crudo a presion reducida, donde el anhidrido ftalico crudo se hace pasar a la columna de destilacion por arriba de un lado de separacion, los componentes de bajo punto de ebullicion se retiran por la parte superior de la columna o en la vecindad de la parte superior de la columna y el anhidrido ftalico segun especificaciones se retira del lado de separacion de la columna, en el que se utiliza una columna de destilacion cuyo numero de las platos teoricos localizados por arriba del suministro de anhidrido ftalico crudo en la columna de destilacion es de 10 a 20 y la columna es opera a una razon de reflujo de desde 0.1 a 0.5.
-
公开(公告)号:DE102005000957A1
公开(公告)日:2006-07-20
申请号:DE102005000957
申请日:2005-01-07
Applicant: BASF AG
Inventor: PESCHEL WERNER , KUMMER MATTHIAS , BECHTEL MARCUS
IPC: C07D307/89 , B01D3/10
Abstract: Process for the preparation of on-spec phthalic anhydride by the distillative purification of crude phthalic anhydride at reduced pressure, where the crude phthalic anhydride is passed to the distillation column above a side take-off, the low-boiling components are removed at the top of the column or in the vicinity of the top of the column and the on-spec phthalic anhydride is removed from the side take-off of the column, in which a distillation column is used whose number of theoretical plates located above the supply of the crude phthalic anhydride into the distillation column is 10 to 20 and the column is operated at a reflux ratio of from 0.1 to 0.5.
-
-
-
-
-
-
-
-