METHOD FOR THE PRODUCTION OF FORMIC ACID FORMATES
    1.
    发明申请
    METHOD FOR THE PRODUCTION OF FORMIC ACID FORMATES 审中-公开
    用于生产酸甲

    公开(公告)号:WO2005044771A3

    公开(公告)日:2005-07-28

    申请号:PCT/EP2004012543

    申请日:2004-11-05

    CPC classification number: C07C51/412 C07C53/06 C07C53/02

    Abstract: The invention relates to a method for the production of formic acid formates, wherein a flowing liquid (I) containing formic acid, and a flowing liquid (II) containing a metal formate, are provided. The flowing liquids (I) and (II) are guided to a rectification column such that a higher or equal guiding point for the liquid flow (II) is selected for the rectification column for the liquid flow (I). The liquid flows (I) and (II) in the rectification column are mixed by separating water via the head of the rectification column and the liquid flow is withdrawn from the rectification column, said liquid flow containing the formic acid formate. The invention is characterised in that the liquid flow is obtained as a melt containing at least 0.5 wt. % water.

    Abstract translation: 公开了一种用于制备酸甲酸盐的方法,它包括:含有甲酸和(II)含有金属甲酸盐提供,液体流的液体流(I)中的液体流(I)和(II)精馏塔所以 被选择用于液体物流(II)供给具有较高或相同的进料点为液体流(I)中,液体流(I)和(II)中经由精馏柱的顶部与水分离的精馏塔混合精馏塔 和从精馏塔包含酸甲酸盐的塔底物流,减,其特征在于,一个重量%水,胜塔底流含有小于0.5的熔体。

    3.
    发明专利
    未知

    公开(公告)号:DE502004004050D1

    公开(公告)日:2007-07-19

    申请号:DE502004004050

    申请日:2004-11-05

    Applicant: BASF AG

    Abstract: A process is proposed for preparing acid formates in which a liquid stream I comprising formic acid and a liquid stream II comprising a metal formate are prepared, the liquid streams I and II are fed to a rectification column in such a manner that a higher or identical feed point to the rectification column is chosen for the liquid stream II than for the liquid stream I, the liquid streams I and II are mixed in the rectification column, with water being removed overhead from the rectification column and a bottoms stream comprising the acid formate is taken off from the rectification column, which comprises the bottoms stream being produced as melt comprising less than 0.5% by weight of water.

    Preparing solid sodium formate, useful as fodder additive for animal fodder, comprises preparing aqueous solution having sodium formate and formic acid, reacting solid phase with base to form mixture, mixing mixture with formic acid

    公开(公告)号:DE102005062931A1

    公开(公告)日:2007-07-05

    申请号:DE102005062931

    申请日:2005-12-29

    Applicant: BASF AG

    Abstract: Preparation of a solid sodium formate preparation comprises (i) preparing an aqueous solution, which exhibits formic acid, sodium formate and water; (ii) subjecting the aqueous solution to crystallization and separating a solid phase from mother liquor; (iii) supplying the mother liquor during the production of the aqueous solution, to a distilling device; (iv) mixing the mother liquor with a sodium-containing base to form a mixture containing sodium formate and formic acid; (v) mixing the mixture with formic acid; and (vi) removing the water by withdrawing from the distilling device. Preparation of a solid sodium formate preparation with a content of at least 35 wt.% of formic acid, comprises: (i) at increased temperature, preparing an aqueous solution, which exhibits a molar ratio of formic acid and sodium formate of more than 1.5:1 and a molar ratio of formic acid and water of at least 1.1:1; (ii) subjecting the aqueous solution to crystallization and separating a solid phase from mother liquor; (iii) supplying the mother liquor, optionally after removal of a partial quantity of the mother liquor, during the production of the aqueous solution, to a distilling device; (iv) mixing the mother liquor with a sodium-containing base to form a mixture containing sodium formate and formic acid; (v) mixing the mixture with formic acid under receipt of the aqueous solution; and (vi) removing the water that is not needed for the production of the aqueous solution, by withdrawing from the distilling device.

    PREPARATION OF ACID FORMATES
    6.
    发明专利

    公开(公告)号:MY136031A

    公开(公告)日:2008-07-31

    申请号:MYPI20044509

    申请日:2004-11-01

    Applicant: BASF AG

    Abstract: A PROCESS IS PROPOSED FOR PREPARING ACID FORMATES IN WHICH - A LIQUID STREAM I COMPRISING FORMIC ACID AND - A LIQUID STREAM II COMPRISING A METAL FORMATE ARE PREPARED, THE LIQUID STREAMS I AND II ARE FED TO A RECTIFICATION COLUMN IN SUCH A MANNER THAT A HIGHER OR IDENTICAL FEED POINT TO THE RECTIFICATION COLUMN IS CHOSEN FOR THE LIQUID STREAM II THAN FOR THE LIQUID STREAM I,THE LIQUID STREAMS I AND II ARE MIXED IN THE RECTIFICATION COLUMN, WITH WATER BEING REMOVED OVERHEAD FROM THE RECTIFICATION COLUMN AND A BOTTOMS STREAM COMPRISING THE ACID FORMATE IS TAKEN OFF FROM THE RECTIFICATION COLUMN,WHICH COMPRISES THE BOTTOMS STREAM BEING PRODUCED AS MELT COMPRISING LESS THAN 0.5% BY WEIGHT OF WATER.(FIG 1)

    PROCEDIMIENTO PARA LA OBTENCION DE FORMIATOS DE ACIDO FORMICO.

    公开(公告)号:ES2286693T3

    公开(公告)日:2007-12-01

    申请号:ES04797653

    申请日:2004-11-05

    Applicant: BASF AG

    Abstract: Procedimiento para la obtención de formiatos de ácido fórmico, según el cual - se pone a disposición una corriente líquida I, que contiene ácido fórmico, y - una corriente líquida II, que contiene un formiato metálico, las corrientes líquidas I y II se alimentan a una columna de rectificación de modo que para la corriente líquida II se selecciona un punto de alimentación más elevado, o el mismo que para la corriente líquida I para la columna de rectificación, las corrientes líquidas I y II se mezclan en la columna de rectificación bajo separación de agua a través de la columna de rectificación, y de la columna de rectificación se extrae una corriente de cola que contiene el formiato de ácido fórmico, caracterizado porque se obtiene la corriente de cola como fusión, que contiene menos de un 0, 5 % en peso de agua.

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