METHOD FOR PRODUCING ACRYLIC ACID AND ACRYLIC ACID ESTERS.

    公开(公告)号:MY120567A

    公开(公告)日:2005-11-30

    申请号:MYPI9901164

    申请日:1999-03-26

    Applicant: BASF AG

    Abstract: A PROCESS FOR PREPARING ACRYLIC ACID AND/OR AN ACRYLATE COMPRISING THE FOLLOWING STAGE A AND, IF DESIRED, B AND, IF DESIRED, C: A: COOLING A GASEOUS REACTION MIXTURE WHICH COMPRISES ACRYLIC ACID AND IS OBTAINED IN THE GAS-PHASE OXIDATION TO PREPARE ACRYLIC ACID, USING AN ACRYLIC ACID CONTAINING NOT MORE THAN 5% BY WEIGHT OF WATER, TO GIVE A GASEOUS MIXTURE COMPRISING (METH)ACRYLIC ACID; B: SEPARATING THE GASEOUS MIXTURE COMPRISING ACRYLIC ACID TO GIVE A LOW-BOILING FRACTION AND A BOTTOM PRODUCT WHICH COMPRISES CRUDE ACRYLIC ACID, AND C: ESTERIFYING THE CRUDE ACRYLIC ACID OBTAINED IN STAGE B BY MEANS OF ONE OR MORE ALKANOLS, TO GIVE AN ESTERIFICATION MIXTURE COMPRISING ONE OR MORE ACRYLATES, ONE OR MORE ACETIC ESTERS, ONE OR MORE MALEIC ESTERS, AND OLIGOMERIC AND POLYMERIC ACRYLATES.

    4.
    发明专利
    未知

    公开(公告)号:ID27329A

    公开(公告)日:2001-03-29

    申请号:ID20000832

    申请日:2000-09-27

    Applicant: BASF AG

    Abstract: Phosphorus-free inhibitor compositions containing (a) N-oxyl radical(s) and (b) a phenol, optionally substituted with up to three 1-4C alkyl, 2-4C alkenyl or 7-10C aralkyl groups. Phosphorus-free inhibitor compositions (I) containing (a) N-oxyl radical(s) and (b) a compound of formula (X). n = 0-3; R = 1-4C alkyl, 2-4C alkenyl or 7-10C aralkyl. Independent claims are also included for: (i) a method for stabilizing materials containing ethylenic double bond(s) against unwanted polymerisation by adding (I) to the material; (ii) a mixture containing an ethylenically unsaturated compound and an effective amount of (I) as polymerisation inhibitor.

    RECTIFICATIVE SEPARATION OF FLUIDS COMPRISING (METH) ACRYLIC MONOMERS

    公开(公告)号:MY139338A

    公开(公告)日:2009-09-30

    申请号:MYPI20034795

    申请日:2003-12-15

    Applicant: BASF AG

    Abstract: A PROCESS FOR RECTIFICATIVELY SEPARATING FLUIDS COMPRISING (METH)ACRYLIC MONOMERS IN A RECTIFICATION COLUMN BY DIRECTLY COOLING THE VAPOR COMPRISING (METH)ACRYLIC MONOMERS RISING TO THE TOP OF THE RECTIFICATION COLUMN TO FORM TOP CONDENSATE COMPRISING (METH)ACRYLIC MONOMERS, THE CONDENSATION SPACE AT THE TOP OF THE COLUMN BEING SEPARATED FROM THE REGION OF THE RECTIFICATION COLUMN CONTAINING THE SEPARATING INTERNALS ONLY BY AT LEAST ONE CHIMNEY TRAY FROM WHICH THE TOP CONDENSATE FORMED IS REMOVED FROM THE RECTIFICATION COLUMN, WHICH COMPRISES EFFECTING THE DIRECT COOLING OF THE VAPOR IN THE CONDENSATION SPACE IN AT LEAST TWO SPRAY ZONES WHICH ARE SPATIALLY SUCCESSIVE AND ARE FLOWED THROUGH BY VAPOR BY SPRAYING SUPERCOOLED TOP CONDENSATE COMPRISING ADDED POLYMERIZATION INHIBITOR, AND THE TEMPERATURE OF THE SPRAYED SUPERCOOLED TOP CONDENSATE BECOMING LOWER FROM SPRAY ZONE TO SPRAY ZONE IN THE FLOW DIRECTION OF THE VAPOR.

    THERMAL SEPARATING PROCESS
    7.
    发明专利

    公开(公告)号:MY137951A

    公开(公告)日:2009-04-30

    申请号:MYPI20041366

    申请日:2004-04-14

    Applicant: BASF AG

    Abstract: (METH)ACRYLIC MONOMERS ARE SEPARATED BY A THERMAL SEPARATION PROCESS BY ASCENDING AT LEAST ONE ASCENDING GASEOUS STREAM IN A SEPARATING COLUMN CONTAINING A SEQUENCE OF MASS TRANSFER TRAYS AND A LIQUID STREAM THAT CONTAINS DISSOLVED POLYMERIZATION INHIBITOR WHICH DESCENDS IN THE SEPARATING COLUMN, AND IN AT LEAST ONE OF THE STREAMS BEING (METH)ACRYLIC MONOMERS; AND SPRAYING THE INNER SURFACE OF THE SEPARATING COLUMN WITH THE DESCENDING LIQUID STREAM THAT CONTAINS THE DISSOLVED POLYMERIZATION INHIBITOR, AND THE SEPARATING COLUMN HAVING INTERNALS, CERTAIN AREAS OF WHICH ARE SHADOW REGIONS OF THE SPRAYED DESCENDING LIQUID STREAM; AND WHICH SHADOW REGIONS ARE EQUIPPED BY COVERING MEANS (2) WHICH PREVENT CONTACT OF THE SHADOW REGIONS WITH (METH)ACRYLIC MONOMERS AND CONSEQUENTLY UNDESIRED POLYMERIZATION OF MONOMER.

    PROCESS FOR PREPARING N-SUBSTITUTED PYRAZOLES

    公开(公告)号:CZ268697A3

    公开(公告)日:1997-12-17

    申请号:CZ268697

    申请日:1996-02-27

    Applicant: BASF AG

    Abstract: PCT No. PCT/EP96/00790 Sec. 371 Date Aug. 20, 1997 Sec. 102(e) Date Aug. 20, 1997 PCT Filed Feb. 27, 1996 PCT Pub. No. WO96/27589 PCT Pub. Date Sep. 12, 1996A process for the preparation of an N-alkyl- or N-phenylalkyl-substituted pyrazole I by reacting the corresponding N-unsubstituted pyrazole II with an alcohol III of the formula R1-OH where R1 is the same alkyl or phenylalkyl group to be added to the unsubstituted nitrogen group -NH- of the pyrazole reactant. Both of the reactants, i.e. the pyrazole II and alcohol III compounds, are catalytically reacted in the liquid phase in a molar ratio of from 0.001:1 to 1:1, at temperatures of 50 DEG -400 DEG C. and under a subatmosheric pressure of from 0.8 bar up to a superatmospheric pressure of 250 bar. The catalyst required for this liquid phase reaction is selected as being at least one or more non-heterogeneous acid catalysts, their alkyl esters or their acid anhydrides.

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