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公开(公告)号：WO03000704A3
公开(公告)日：2003-05-01
申请号：PCT/EP0206903
申请日：2002-06-21
Applicant: BASF AG , VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
CPC classification number: C07F9/3813
Abstract: The invention relates to a method for producing N-phosphonomethylglycine from an aqueous mixture containing N-phosphonomethylglycine, ammonium halogenides and alkali halides or earth alkali halides and optionally, organic impurities in a dissolved form. According to the invention, (a) the pH-value of the mixture is regulated to a value of 2 - 8, (b) the mixture is separated by means of a selective nano-filtration membrane, to obtain a retentate rich in N-phosphonomethylglycine and poor in halogenides and a permeate rich in halogenides and poor in N-phosphonomethylglycine and (c) the N-phosphonmethylglycine is prepared from the retentate. The inventive method enables the production of N-phosphonomethylglycine by simultaneously separating the halogenide salts thereof.
Abstract translation: 本发明涉及一种方法，用于N-膦酰甲基甘氨酸的从含有N-膦酰，卤化铵和碱金属或碱土金属的卤化物以及任选的溶解的有机杂质的含水混合物，其包含（a）所述混合物的pH至一个值的恢复 在2至8的范围内设定，（b）将该混合物在选择性纳米过滤膜的分离使得得到的N-膦酰甲基甘氨酸渗透物中卤化物在N-膦酰甲基甘氨酸更丰富和更差的以卤化物渗余物和更丰富和更差的 和（c）从渗余物中回收N-膦酰基甲基甘氨酸。 本发明的方法允许回收N-膦酰基甲基甘氨酸并同时除去卤化物盐。
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公开(公告)号：DK1401846T3
公开(公告)日：2005-04-11
申请号：DK02754734
申请日：2002-06-21
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , ORSTEN STEFAN , WULFF CHRISTIAN , VOSS HARTWIG
Abstract: The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
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公开(公告)号：DE50201799D1
公开(公告)日：2005-01-20
申请号：DE50201799
申请日：2002-06-21
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
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公开(公告)号：IN2042CH2003A
公开(公告)日：2004-12-11
申请号：IN2042CH2003
申请日：2003-12-03
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
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公开(公告)号：BR0210569A
公开(公告)日：2004-08-03
申请号：BR0210569
申请日：2002-06-21
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
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Patent Agency Ranking
公开(公告)号：CA2451507C
公开(公告)日：2010-02-09
申请号：CA2451507
申请日：2002-06-21
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The invention relates to a method for producing N-phosphonomethylglycine from an aqueous mixture containing N-phosphonomethylglycine, ammonium halogenides and alkali halides or earth alkali halides and optionally, organic impurities in a dissolved form. According to the invention, (a) the pH-value of the mixture is regulated to a value of 2 - 8, (b) the mixture is separated by means of a selective nano-filtration membrane, to obtain a retentate rich in N-phosphonomethylglycine and poor in halogenides and a permeate rich in halogenides and poor in N-phosphonomethylglycine and (c) the N-phosphonmethylglycine is prepared from the retentate. The inventive method enables the production of N-phosphonomethylglycine by simultaneously separating the halogenide salts thereof.
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公开(公告)号：DE102005060784A1
公开(公告)日：2007-06-28
申请号：DE102005060784
申请日：2005-12-16
Applicant: BASF AG
Inventor： PAPP RAINER , VANDENMERSCH HUGUES , BEY OLIVER , ZEHNER PETER , VOS HARTWIG , MACKEWITZ THOMAS , PACIELLO ROCCO , ZELLER EDGAR
IPC: B01J31/40
Abstract: Extraction of a metal-complex catalyst enriched stream comprises dissolving e.g. reaction products and by-products, in a reaction medium by an agent containing phosphorous and/or nitrogen atoms, modified organic metal complex catalyst; distillating the catalyst free stream of the reaction discharge; separating high boiling and non-distilled components of the reaction discharge and the sump product of the distillation into a permeate- and retentate- stream and recycling the retentate stream enriched, completely or partially into the metal-complex-catalyst. Extraction of a metal-complex catalyst enriched streams, obtained from the liquid discharge of a metal complex catalyst reaction comprises dissolving reaction products, by-products, non-converted educt, solvent, homogeneous or colloid in a reaction medium by an agent containing one or more phosphorous and/or nitrogen atoms, modified organic metal complex catalyst with a molecular weight of greater than 200 D and free ligands; distillating the catalyst free stream containing low boiling components of the reaction discharge at atmospheric pressure or low pressure; separating high boiling and non-distilled components of the reaction discharge and the sump product of the distillation into a permeate- and retentate- stream, by a membrane-separator device and recycling the retentate stream enriched with the metal-complex catalyst, completely or partially into the metal-complex-catalyst.
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公开(公告)号：AT284890T
公开(公告)日：2005-01-15
申请号：AT02754734
申请日：2002-06-21
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
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公开(公告)号：DE10130136A1
公开(公告)日：2003-01-02
申请号：DE10130136
申请日：2001-06-22
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The invention relates to a method for producing N-phosphonomethylglycine from an aqueous mixture containing N-phosphonomethylglycine, ammonium halogenides and alkali halides or earth alkali halides and optionally, organic impurities in a dissolved form. According to the invention, (a) the pH-value of the mixture is regulated to a value of 2 - 8, (b) the mixture is separated by means of a selective nano-filtration membrane, to obtain a retentate rich in N-phosphonomethylglycine and poor in halogenides and a permeate rich in halogenides and poor in N-phosphonomethylglycine and (c) the N-phosphonmethylglycine is prepared from the retentate. The inventive method enables the production of N-phosphonomethylglycine by simultaneously separating the halogenide salts thereof.
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公开(公告)号：SI1401846T1
公开(公告)日：2005-06-30
申请号：SI200230059
申请日：2002-06-21
Applicant: BASF AG
Inventor： VANDENMERSCH HUGUES , VOSS HARTWIG , ORSTEN STEFAN , WULFF CHRISTIAN
Abstract: The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
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