METHOD FOR PRODUCING N-PHOSPHONOMETHYLGLYCINE
    2.
    发明申请
    METHOD FOR PRODUCING N-PHOSPHONOMETHYLGLYCINE 审中-公开
    获得N-磷酸乙二醇甘氨酸的方法

    公开(公告)号:WO03000704A3

    公开(公告)日:2003-05-01

    申请号:PCT/EP0206903

    申请日:2002-06-21

    CPC classification number: C07F9/3813

    Abstract: The invention relates to a method for producing N-phosphonomethylglycine from an aqueous mixture containing N-phosphonomethylglycine, ammonium halogenides and alkali halides or earth alkali halides and optionally, organic impurities in a dissolved form. According to the invention, (a) the pH-value of the mixture is regulated to a value of 2 - 8, (b) the mixture is separated by means of a selective nano-filtration membrane, to obtain a retentate rich in N-phosphonomethylglycine and poor in halogenides and a permeate rich in halogenides and poor in N-phosphonomethylglycine and (c) the N-phosphonmethylglycine is prepared from the retentate. The inventive method enables the production of N-phosphonomethylglycine by simultaneously separating the halogenide salts thereof.

    Abstract translation: 本发明涉及一种方法,用于N-膦酰甲基甘氨酸的从含有N-膦酰,卤化铵和碱金属或碱土金属的卤化物以及任选的溶解的有机杂质的含水混合物,其包含(a)所述混合物的pH至一个值的恢复 在2至8的范围内设定,(b)将该混合物在选择性纳米过滤膜的分离使得得到的N-膦酰甲基甘氨酸渗透物中卤化物在N-膦酰甲基甘氨酸更丰富和更差的以卤化物渗余物和更丰富和更差的 和(c)从渗余物中回收N-膦酰基甲基甘氨酸。 本发明的方法允许回收N-膦酰基甲基甘氨酸并同时除去卤化物盐。

    7.
    发明专利
    未知

    公开(公告)号:MX234328B

    公开(公告)日:2006-02-13

    申请号:MXPA03011309

    申请日:2002-06-21

    Applicant: BASF AG

    Abstract: The invention relates to a process for preparing N-phosphono-methylglycine by reacting a hexahydrotriazine compound with a triacyl phosphite in an organic solvent, hydrolyzing the resulting phosphono compound after prior extraction into an aqueous phase and separation from the organic phase. The process avoids decomposition of the organic solvent during hydrolysis.

    PROCEDIMIENTO PARA LA OBTENCION DE N-FOSFONOMETILGLICINA.

    公开(公告)号:ES2233846T3

    公开(公告)日:2005-06-16

    申请号:ES02754734

    申请日:2002-06-21

    Applicant: BASF AG

    Abstract: Procedimiento para la obtención de N- fosfonometilglicina a partir de una mezcla acuosa que contiene N-fosfonometilglicina, halogenuros de amonio, así como halogenuros de metales alcalinos o alcalinotérreos y, dado el caso, impurezas orgánicas, en el que: (a) se ajusta el pH de la mezcla a un valor comprendido en el intervalo de 2 a 8, (b) se efectúa una separación de la mezcla en una membrana de nanofiltración selectiva, obteniéndose un retentato enriquecido en N-fosfonometilglicina y empobrecido en halogenuros y un permeato enriquecido en halogenuros y empobrecido en N- fosfonometilglicina y (c) se obtiene la N-fosfonometilglicina a partir del retentato.

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