REACTOR FOR CARRYING OUT A THREE-PHASE REACTION OF A LIQUID PHASE AND A GASEOUS PHASE OVER A FIXED CATALYST BED

    公开(公告)号:CA2691642C

    公开(公告)日:2015-12-22

    申请号:CA2691642

    申请日:2008-06-20

    Applicant: BASF SE

    Abstract: The invention relates to a reactor (R) for performing a three-phase reaction of a fluid phase (1) and a gaseous phase (2) on a packed bed catalyst (F), the packed bed catalyst (F) being disposed horizontally in the reactor (R) and the fluid phase (1) and the gaseous phase (2) being fed through the reactor (R) from the bottom to the top, using a mixing and distributing device (MV) across the packed bed catalyst (F), characterized in that the mixing and distributing device (MV) comprises a trough distributor (TV) for the fluid phase (1) having trough-shaped channels (K) and drain tubes (A) in the trough-shaped channels (K) for the fluid phase (1), and a distributor floor (B) disposed below and at a distance from the trough distributor (TV) in which vertical spouts (T) are disposed, having one or more openings (P1) for the inlet of the gaseous phase (2) and one or more openings (P2) disposed below the openings (P1) for the inlet of the gaseous phase, for the inlet of the fluid phase (1) into the spouts (T), and the number and size of the openings (P2) for the inlet of the fluid phase (1) being designed such that the fluid level on the distribution floor (B) is adjusted to be below the openings (P1) for the inlet of the gaseous phase (2) and above the openings (P2) for the inlet of the fluid phase (1) for a prescribed inlet flow of fluid.

    TRAY FOR A MASS TRANSFER COLUMN
    3.
    发明专利

    公开(公告)号:CA2855714A1

    公开(公告)日:2013-05-23

    申请号:CA2855714

    申请日:2012-11-14

    Applicant: BASF SE

    Abstract: The invention relates to a base for a mass transfer column, comprising gas through-openings which are distributed over the base (1) and at least one baffle plate (11) for directing the flow of liquid flowing on the base, said base (1) being loadable with a liquid via at least one inlet (3). The base has at least one inlet (3), at least one separating weir (5) which separates the inflowing liquid into two flows, and at least two outlets (12) or at least two inlets (3) and at least one outlet (12) for the liquid. Each flow flows along a flow path (7; 9) to an outlet (12). The invention further relates to a mass transfer column which contains the base and to a use of the base and the mass transfer column.

    TRAY FOR A MASS TRANSFER COLUMN
    5.
    发明专利

    公开(公告)号:CA2855714C

    公开(公告)日:2019-05-21

    申请号:CA2855714

    申请日:2012-11-14

    Applicant: BASF SE

    Abstract: The invention relates to a tray for a mass transfer column, having gas passage openings distributed over the tray (1), and having at least one baffle (11) for flow diversion of liquid flowing on the tray, it being possible for the tray (1) to be fed with a liquid via at least one entry (3). The tray has at least one entry (3), at least one separating weir (5), which separates the inflowing liquid into two streams, and at least two exits (12), or has at least two entries (3) and at least one exit (12) for the liquid, each stream flowing along a flow path (7; 9) to an exit (12). The invention further relates to a mass transfer column comprising the tray, and to a use of tray and mass transfer column.

    Dispositivo y procedimiento para obtener productos altamente puros a partir de una extracción de columna

    公开(公告)号:ES2435544T3

    公开(公告)日:2013-12-20

    申请号:ES08874459

    申请日:2008-11-19

    Applicant: BASF SE

    Abstract: Dispositivo colector de líquidos para su uso en una columna que contiene al menos un lecho de empaquetadura,que comprende - un dispositivo colector para recolectar el líquido que sale del lecho de empaquetadura y - al menos una extracción de la columna, caracterizado porque todos los elementos del dispositivo colector están separados con respecto a la pared decolumna o con respecto a la pared de columna y al menos una pared separadora que se encuentra en la columna,de modo que el líquido que baja por la pared no llega al interior de la extracción del dispositivo colector de líquidos,estando los elementos unidos mediante elementos distanciadores con la pared de columna y/o dado el caso con lapared separadora, estando los elementos colocados de forma suelta sobre dispositivos de apoyo, y/o estando loselementos fijados en una rejilla de soporte del lecho de empaquetadura que se encuentra por encima de loselementos.

    Plato para una columna de transferencia de masa

    公开(公告)号:ES2758840T3

    公开(公告)日:2020-05-06

    申请号:ES12784023

    申请日:2012-11-14

    Applicant: BASF SE

    Abstract: Plato para una columna de absorción para la preparación de ácido nítrico con aberturas de paso de gas, que están dispuestas distribuidas por el plato (1), así como al menos una chapa deflectora (11) para la desviación de flujo de líquido que fluye sobre el plato, en donde el plato (1) a través de al menos una entrada (3) puede cargarse con un líquido, caracterizado porque el plato presenta al menos una entrada (3), al menos un dique de separación (5) que separa el líquido entrante en dos corriente, y presenta al menos dos salidas (12) o al menos dos entradas (3) y al menos una salida (12) para el líquido, y en donde cada corriente a lo largo de trayecto (7; 9) de flujo separado fluye desde la entrada (3) hacia una salida (12) y en donde sobre el plato (1) a lo largo de los trayectos (7; 9) de flujo están dispuestos en cada caso elementos (13) de transmisión de calor que están configurados como elementos de enfriamiento de modo que los trayectos (7; 9) de flujo están diseñados de modo que la longitud de cada trayecto (7; 9) de flujo sea esencialmente igual.

    9.
    发明专利
    未知

    公开(公告)号:AT403478T

    公开(公告)日:2008-08-15

    申请号:AT05821914

    申请日:2005-12-31

    Applicant: BASF SE

    Abstract: Process for the preparation of on-spec phthalic anhydride by the distillative purification of crude phthalic anhydride at reduced pressure, where the crude phthalic anhydride is passed to the distillation column above a side take-off, the low-boiling components are removed at the top of the column or in the vicinity of the top of the column and the on-spec phthalic anhydride is removed from the side take-off of the column, in which a distillation column is used whose number of theoretical plates located above the supply of the crude phthalic anhydride into the distillation column is 10 to 20 and the column is operated at a reflux ratio of from 0.1 to 0.5.

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