公开(公告)号：CA3106758A1

公开(公告)日：2020-02-20

申请号：CA3106758

申请日：2019-08-06

Applicant: BASF SE

Inventor： ROHDE WOLFGANG ,  GILBERT DAVID JOHANN ,  SCHULER BERNHARD ,  KUHN OLIVER ,  MENTGES MICHAEL

IPC: B03C1/00 ,  B03C1/01 ,  B03C1/30 ,  B03C3/00

Abstract: The present invention relates to a process for concentrating desired particles comprising a carrier-magnetic-separation comprising the following steps a) providing a feedstock which contains the desired particles and an undesired material;b) adding hydrophobic magnetic particles to the feedstock which results in a loaded feedstock containing agglomerates of the magnetic particles and the desired particles or of the magnetic particles and the undesired material; c) separating the agglomerates from the loaded feedstock by a separation method which results in isolated agglomerates, where the separation method is selected from sorting, electric separation, magnetic separation, screening, classification, gravity concentration,and flotation;d) breaking up the isolated agglomerates to obtain a suspension comprising the magnetic particles in desagglomerated form; and e) separating the magnetic particles from the suspension obtained in step d) by a separation method selected from sorting, electric separation, magnetic separation, screening, classification, gravity concentration, and flotation.

公开(公告)号：ES2422296T3

公开(公告)日：2013-09-10

申请号：ES07822220

申请日：2007-11-05

Applicant: BASF SE ,  BASF AGRO B V ARNHEM NL ZUERICH BRANCH

Inventor： SUKOPP MARTIN ,  KUHN OLIVER ,  GROENING CARSTEN ,  KEIL MICHAEL ,  LONGLET JON J

IPC: C07D231/44 ,  A01N43/00 ,  A01N43/56 ,  A61K31/415 ,  A61P33/00

Abstract: Proceso para la sulfinilación de un derivado pirazol, caracterizado porque 5-amino-1-[2,6-dicloro-4-(trifluorometil)fenil]-1 H-pirazol-3-carbonitrilo (II) se hace reaccionar con un agente de sulfinilación seleccionado de ácidotrifluorometilsulfínico, anhídrido de ácido trifluorometilsulfínico, y un trifluorometilsulfinato alcalino o sal de metalalcalinotérreo y mezclas del ácido y/o las sales, en la presencia de por lo menos un complejo de aminoácido endonde las aminas se seleccionan de aminas terciarias y los ácidos se seleccionan de ácido fluorhídrico, ácidoclorhídrico, ácido bromhídrico, ácido yodhídrico, ácido p-toluenosulfónico, ácido bencenosulfónico, ácido xilenosulfónico, ácido metanosulfónico y ácido trifluorometilsulfónico, y con la adición de un agente de halogenación.

公开(公告)号：UA98475C2

公开(公告)日：2012-05-25

申请号：UAA200905383

申请日：2007-11-05

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KUHN OLIVER ,  GRONING CARSTEN ,  KEIL MICHAEL ,  LONGLET JON J

IPC: C07D231/44 ,  A01N31/08 ,  A01N43/56 ,  A61K31/415 ,  A61P33/00

Abstract: Данноеизобретениекасаетсяновогоспособасульфинированияпроизводнойпиразола, вкотором 5-амино-1-[2,6-дихлор-4-(трифторметил)фенил]-1Н-пиразол-3-карбонитрил (II) подвергаютреакциис сульфинирующимагентом S вприсутствиипокрайнеймереодногоамино/кислотногокомплекса, вкоторомамин(ы) выбран(ы) извторичныхи/илитретичныхаминов, акислота(ы) выбрана(ы) изфтористоводородной, хлористоводородной, бромистоводороднойи йодистоводороднойкислотыи производныхсульфоновойкислоты, придобавлениигалогенирующегоагента, гдеS представляетсобой [CFS(O)]O; илиCFS(O)X, гдеX означаетфтор, хлор, бром, йод, гидроксигруппуилисольщелочногоилищелочноземельногометаллагидроксигруппы; илиихсмеси,гдетемпературареакционнойсмесиникогданепревышает 39 °C.

公开(公告)号：ZA200903973B

公开(公告)日：2012-02-29

申请号：ZA200903973

申请日：2009-06-08

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KEIL MICHAEL ,  KUHN OLIVER ,  GRONING CARSTEN ,  LONGLET JON J

IPC: C07D20060101 ,  A01N20060101 ,  A61K20060101 ,  A61P20060101

Abstract: The present invention relates to a process for the sulfinylation of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile (II) is reacted with a sulfinylating agent S in the presence of at least one amine acid complex wherein the amine(s) are selected from secondary and/or tertiary amines and the acid(s) are selected from hydrofluoric, hydrochloric, hydrobromic and hydroiodic acid and sulfonic acid derivatives, and with the addition of a halogenating agent, wherein S is [CF3S(O)]2O; or CF3S(O)X wherein X means fluoro, chloro, bromo, iodo, a hydroxy group, or an alkaline or alkaline earth metal salt of the hydroxy group; or mixtures thereof, wherein the temperature of the reaction mixture at no time exceeds 39° C.

公开(公告)号：NZ576638A

公开(公告)日：2011-12-22

申请号：NZ57663807

申请日：2007-11-05

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KUHN OLIVER ,  GRONING CARSTEN ,  KEIL MICHAEL ,  LONGLET JON J

IPC: C07D231/44 ,  A01N43/00 ,  A01N43/56 ,  A61K31/415 ,  A61P33/00

Abstract: Disclosed is a process for the sulfinylation of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile is reacted with a sulfinylating agent S in the presence of at least one amine acid complex wherein the amine(s) are selected from secondary and/or tertiary amines and the acid(s) are selected from hydrochloric acid, hydrofluoric acid, ptoluenesulfonic acid, benzenesulfonic acid, 4-ethyl benzenesulfonic acid, 4-chlorobenzenesulfonic acid, xylene sulfonic acid, 2,3-dimethylbenzene sulfonic acid, 2,4-dimethylbenzene sulfonic acid, 2,5-dimethylbenzene sulfonic acid, 2,6-dimethylbenzene sulfonic acid, 1-napthalenesulfonic acid, 2- napthalenesulfonic acid, mixtures of two or more of the isomers of dimethylbenzene sulfonic acid, mesitylene sulfonic acid, methanesulfonic acid, camphor sulfonic acid, and trifluoromethylsulfonic acid, , and with the addition of a halogenating agent, wherein S is [CF3S(O)]2O; or CF3S(O)X wherein X means fluoro, chloro, bromo, iodo, a hydroxy group, or an alkaline or alkaline earth metal salt of the hydroxy group; or mixtures thereof, wherein the temperature of the reaction mixture at no time exceeds 39 degrees Celsius. Also disclosed is a method of treating animals against infestation or infection by parasites or protecting growing plants from infestation from insects, acarids or nematodes by applying or ingesting a 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-(trifluoromethylsulfinyl)-pyrazole-3-carbonitrile prepared by the above process.

公开(公告)号：AU2021380951A1

公开(公告)日：2023-06-22

申请号：AU2021380951

申请日：2021-11-19

Applicant: BASF SE

Inventor： TUERKOGLU GAZI ,  LEED MARINA GRACE DICKENS ,  KELLER WILHELM ,  SOLFRANK MARTINA ,  KELLER ROBERT ANTHONY ,  REICH OLIVER ,  LEINO CALLEJA DAVID ,  HOH LI NOI LILIAN ,  KUHN OLIVER ,  SATHYANARAYANA SHYAM SUNDAR ,  PAHNKE KAI ,  ELTZE TOBIAS ,  BEIL CHRISTIAN

IPC: B29B17/02 ,  B07C5/34 ,  G06Q10/00

Abstract: Computer-implemented method for controlling sorting of plastic compounds, comprising the steps of: providing a computer-based database comprising entries on a plurality of markers each identifying a specific plastic compound (S100); receiving scan data from a sample of a plastic compound (S200); identifying a marker in the sample of the plastic compound based on the received scan data and the plurality of markers of the database (S300); sorting of plastic compounds based on the identified marker of the sample of the plastic compound (S400).

公开(公告)号：BRPI0718774A2

公开(公告)日：2013-12-03

申请号：BRPI0718774

申请日：2007-11-05

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KUHN OLIVER ,  GROENING CARSTEN ,  KEIL MICHAEL ,  LONGLET JON J

IPC: C07D231/44 ,  A01N43/00 ,  A01N43/56 ,  A61K31/415 ,  A61P33/00

Abstract: The present invention relates to a process for the of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile (II) is reacted with a sulfinylating agent selected from trifluoromethylsulfinic acid, trifluoromethylsulfinic acid anhydride, and a trifluoromethylsulfinate alkaline or alkaline earth metal salt and mixtures of the acid and/or the salt(s), in the presence of at least one amine acid complex wherein the amine(s) are selected from tertiary amines and the acid(s) are selected from hydrofluoric, hydrochloric, hydrobromic and hydroiodic acid and sulfonic acid derivatives, and with the addition of a halogenating agent.

公开(公告)号：UA98628C2

公开(公告)日：2012-06-11

申请号：UAA200905234

申请日：2007-11-05

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KUHN OLIVER ,  GRONING CARSTEN ,  KEIL MICHAEL ,  LONGLET JON J

IPC: C07D231/44 ,  A01N43/56 ,  A61K31/415 ,  A61P33/00

Abstract: Данноеизобретениекасаетсяспособасульфинилированияпроизводнойпиразола, вкотором 5-амино-1-[2,6- дихлор-4-(трифторметил)фенил]-1Н-пиразол-3-карбонитрил (II) подвергаютреакциис сульфинилирующимагентом S вприсутствиипокрайнеймереодногоамино/кислотногокомплекса, гдеамин(ы) выбран(ы) изциклическихвторичныхаминов, акислота(ы) выбрана(ы) изпроизводныхсульфоновойкислоты, придобавлениигалогенизирующегоагента, где S представляетсобой [CFS(O)]O; илиCFS(O)X, гдеX означаетфтор, хлор, бром, йод, группугидрокси, илисольщелочногоилищелочноземельногометаллагидроксигруппы; илиихсмеси.

公开(公告)号：ZA200903969B

公开(公告)日：2012-02-29

申请号：ZA200903969

申请日：2009-06-08

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KEIL MICHAEL ,  KUHN OLIVER ,  GRONING CARSTEN ,  LONGLET JON J

IPC: C07D20060101 ,  A01N20060101 ,  A61K20060101 ,  A61P20060101

Abstract: The present invention relates to a process for the sulfinylation of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile (II) is reacted with a sulfinylating agent S in the presence of at least one amine acid complex wherein the amine(s) are selected from cyclic secondary amines and the acid(s) are selected from sulfonic acid derivatives, and with the addition of a halogenating agent, wherein S is [CF3S(O)]2O; or CF3S(O)X wherein X means fluoro, chloro, bromo, iodo, a hydroxy group, or an alkaline or alkaline earth metal salt of the hydroxy group; or mixtures thereof.

公开(公告)号：NZ576593A

公开(公告)日：2011-12-22

申请号：NZ57659307

申请日：2007-11-05

Applicant: BASF SE

Inventor： SUKOPP MARTIN ,  KUHN OLIVER ,  GRONING CARSTEN ,  KEIL MICHAEL ,  LONGLET JON J

IPC: C07D231/44 ,  A01N43/00 ,  A01N43/56 ,  A61K31/415 ,  A61P33/00

Abstract: Disclosed is a process for the sulfinylation of a pyrazole derivative, characterized in that 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1 H-pyrazole-3-carbonitrile is reacted with a sulfinylating agent S in the presence of at least one amine acid complex wherein the amine(s) are selected from cyclic secondary amines selected from piperidine, 2-methylpiperidine, 4-methylpiperidine, pyrrolidine, 2-methylpyrrolidine, 3-methylpyrrolidine, imidazolidine, pyrrole, piperazine, and morpholine, and the acid(s) are selected from p-toluenesulfonic acid, benzenesulfonic acid, 4-ethyl benzenesulfonic acid, 4-chlorobenzenesulfonic acid, xylenesulfonic acid, 2,3-dimethylbenzene sulfonic acid, 2,4:"dimethylbenzene sulfonic acid, 2,5-dimethylbenzene sulfonic acid, 2,6-dimethylbenzene sulfonic acid, 1-napthalenesulfonic acid, 2-napthalenesulfonic acid, mixtures of two or more of the isomers of dimethylbenzene sulfonic acid, mesitylene sulfonic acid, methane-sulfonic acid, camphor sulfonic acid, and trifluoromethylsulfonic acid, and with the addition of a halogenating agent, wherein S is [CF3S(O)]2O; or CF3S(O)X wherein X means fluoro, chloro, bromo, iodo, a hydroxy group, or an alkaline or alkaline earth metal salt of the hydroxy group; or mixtures thereof. Also disclosed is a method of treating animals against infestation or infection by parasites or protecting growing plants from infestation from insects, acarids or nematodes by applying or ingesting a 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-(trifluoromethylsulfinyl)-pyrazole-3-carbonitrile prepared by the above process.