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    METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS
    3.
    发明申请
    METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS 审中-公开
    从糖醇制备胺的方法

    公开(公告)号：WO2009027249A3

    公开(公告)日：2009-06-18

    申请号：PCT/EP2008060742

    申请日：2008-08-15

    Applicant: BASF SE ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  MELDER JOHANN-PETER

    Inventor： ERNST MARTIN ,  HOFFER BRAM WILLEM ,  MELDER JOHANN-PETER

    IPC: C07C209/16 ,  C07C211/10 ,  C07C211/11 ,  C07D241/02 ,  C07D295/00

    CPC classification number: C07C209/16 ,  C04B24/122 ,  C04B28/02 ,  C07C213/02 ,  C07D241/04 ,  C07D295/02 ,  C07D295/023 ,  C07C211/09 ,  C07C211/10 ,  C07C211/11 ,  C07C215/08

    Abstract: The invention relates to a method for producing amines by reacting sugar alcohols with hydrogen and an amination agent, selected from the group containing ammonia, primary and secondary amines, in the presence of a catalyst at a temperature of between 100°C and 400°C and at a pressure of between 1 and 40 MPa (10 to 400 bar). The catalyst preferably contains a metal or several metals or one or more oxygen-containing compounds of metals in groups 8 and/or 9 and/or 10 and/or 11 of the periodic table of elements. Preferably, the sugar alcohol is obtained by the hydrogenation of the corresponding sugars. The invention also relates to the use of the reaction product as an additive in cement or concrete production and in other application areas.

    Abstract translation: 本发明涉及一种通过糖醇与氢气和选自氨，伯和仲胺中选择的胺化剂反应制备胺的方法，在催化剂的存在下，在100℃的温度至400℃和压力 1至40MPa（10至400巴）。 催化剂优选含有一种或多种金属或一种或多种元素周期表第8和/或9族和/或10和/或11族金属的含氧化合物。 糖醇优选通过相应糖的氢化获得。 本发明还涉及反应产物作为水泥或混凝土生产和其它应用中的添加剂的用途。

    HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF
    5.
    发明申请
    HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF 审中-公开
    加氢催化剂，生产和使用

    公开(公告)号：WO2010089266A3

    公开(公告)日：2010-12-23

    申请号：PCT/EP2010051143

    申请日：2010-02-01

    Applicant: BASF SE ,  WIGBERS CHRISTOF WILHELM ,  STEINER JOCHEN ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  SCHWAB EKKEHARD ,  MELDER JOHANN-PETER

    Inventor： WIGBERS CHRISTOF WILHELM ,  STEINER JOCHEN ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  SCHWAB EKKEHARD ,  MELDER JOHANN-PETER

    IPC: B01J23/78 ,  B01J23/83 ,  B01J27/18 ,  B01J27/185 ,  B01J35/04 ,  B01J37/02 ,  C07C209/48 ,  C07C211/11 ,  C07C211/12 ,  C07C211/36 ,  C07C253/30 ,  C07C255/24

    CPC classification number: B01J23/78 ,  B01J23/83 ,  B01J27/1853 ,  B01J35/04 ,  B01J37/0201 ,  B01J37/0205 ,  B01J37/0215 ,  B01J37/0234 ,  C07C209/48 ,  C07C253/30 ,  C07C2601/14 ,  C07C211/11 ,  C07C211/12 ,  C07C211/36 ,  C07C255/24

    Abstract: The invention relates to a method for improving the catalytic properties of a catalyst that exists in the form of a structured monolith and comprises one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. The invention further relates to a method for hydrogenating compounds comprising at least one unsaturated carbon-carbon, carbon-nitrogen or carbon-oxygen compound, in the presence of a catalyst comprising one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst exists in the form of a structured monolith, characterized in that the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. In addition, the invention relates to the use of a base compound selected from the group of alkali, earth alkali and rare earth metals for improving the catalytic properties of a catalyst, comprising copper and/or cobalt and/or nickel, wherein the catalyst exists in the form of a structured monolith.

    Abstract translation: 本发明涉及一种用于改善的催化剂，其存在于结构化的整料和或多种元素的选自由钴，镍的含有基团和铜中选择的形式的催化性质，其中与所述催化剂的一种或多种基本 选自碱金属，碱土金属和稀土金属的选择的化合物所接触。 本发明还涉及一种方法，用于包含在催化剂的存在下对含至少一个不饱和碳 - 碳，碳 - 氮或碳 - 氧键的化合物的氢化的组中选择的一种或多种元素自由钴，镍 和铜，其中，所述催化剂是在结构化的单块形式，其特征在于，所述催化剂与选自碱金属，碱土和在接触稀土金属中的一种或多种碱性化合物接触。 此外，本发明是使用选自碱金属，碱土金属和稀土金属中选出的碱性化合物，以提高催化剂的催化性能而言，包含铜和/或钴和/或镍，其特征在于，以结构化的形式的催化剂 整料是存在的。

    3-AMINOMETHYL-1-CYCLOHEXYLAMINE, AND METHOD FOR THE PRODUCTION THEREOF
    7.
    发明申请
    3-AMINOMETHYL-1-CYCLOHEXYLAMINE, AND METHOD FOR THE PRODUCTION THEREOF 审中-公开
    3-氨基甲基环己基胺1 AND METHOD FOR MAKING

    公开(公告)号：WO2010009994A3

    公开(公告)日：2010-03-25

    申请号：PCT/EP2009058887

    申请日：2009-07-13

    Applicant: BASF SE ,  ERNST MARTIN ,  DAHMEN KIRSTEN ,  OFTRING ALFRED

    Inventor： ERNST MARTIN ,  DAHMEN KIRSTEN ,  OFTRING ALFRED

    IPC: C07C211/36

    CPC classification number: C07C211/36 ,  C07B2200/09 ,  C07C2601/14

    Abstract: The invention relates to 3-aminomethyl-1-cyclohexylamine and a method for the production thereof by a) reacting cyclohexenone with hydrogen cyanide in the presence of a basic catalyst, b) reacting the cyclohexanone nitrile obtained in step a) with ammonia in the presence of an imine-forming catalyst, and c) reacting the reaction mixture that is obtained in step b) and contains 3-cyanocyclohexylimine with hydrogen and ammonia on hydrogenation catalysts. The invention further relates to the use of 3-aminomethyl-1-cyclohexylamine as a curing agent for epoxy resins, as an intermediate product when producing diisocyanates, as an initiator entity when producing polyetherols, and/or as a monomer for producing polyamides.

    Abstract translation: 本发明涉及3-氨基甲基-1-环己基胺和用于通过其制备方法）在碱性催化剂的存在下反应与氰化氢环己烯酮，b）通过在步骤a）Cyclohexanonnitrils与氨在亚胺形成催化剂的存在下得到的产物反应，和 c））的步骤b中获得的产物进行反应与氢气和氨的加氢催化剂的反应混合物含有3- Cyanocyclohexylimin-。 本发明进一步涉及使用3-氨基甲基-1-环己基胺的作为固化剂的环氧树脂，如二异氰酸酯的制造中的中间体，如在聚醚多元醇和/或作为用于聚酰胺的制造的单体的制造中的起动器。

    5-ISOPROPYL-3-AMINOMETHYL-2-METHYL-1-AMINO-CYCLOHEXANE (CARVONE DIAMINE), AND METHOD FOR THE PRODUCTION THEREOF
    8.
    发明申请
    5-ISOPROPYL-3-AMINOMETHYL-2-METHYL-1-AMINO-CYCLOHEXANE (CARVONE DIAMINE), AND METHOD FOR THE PRODUCTION THEREOF 审中-公开
    5-异丙基-3-氨基甲基-2-甲基-1-氨基 - 环己烷（CARVONDIAMIN）和用于制备方法

    公开(公告)号：WO2010009995A2

    公开(公告)日：2010-01-28

    申请号：PCT/EP2009058888

    申请日：2009-07-13

    Applicant: BASF SE ,  ERNST MARTIN ,  OFTRING ALFRED ,  WISSEL-STOLL KATHRIN ,  UENSAL OEMER ,  FREYER STEPHAN ,  ALTENHOFF ANSGAR GEREON ,  STAFFEL WOLFGANG

    Inventor： ERNST MARTIN ,  OFTRING ALFRED ,  WISSEL-STOLL KATHRIN ,  UENSAL OEMER ,  FREYER STEPHAN ,  ALTENHOFF ANSGAR GEREON ,  STAFFEL WOLFGANG

    IPC: C07C211/36

    CPC classification number: C07C211/36

    Abstract: The invention relates to 5-isopropyl-3-aminomethyl-2-methyl-1-amino-cyclohexane (carvone diamine) and a method for the production thereof by a) reacting carvone with hydrogen cyanide, b) then reacting the carvone nitrile obtained in step a) with ammonia in the presence of an imine-forming catalyst, and c) subsequently reacting the reaction mixture that is obtained in step b) and contains carvone nitrilimine with hydrogen and ammonia on hydrogenation catalysts. The invention further relates to the use of carvone diamine as a curing agent for epoxy resins, as an intermediate product when producing diisocyanates, as an initiator entity when producing polyetherols, and/or as a monomer for producing polyamides.

    Abstract translation: 本发明涉及5-异丙基-3-氨基甲基-2-甲基-1-氨基 - 环己烷（Carvondiamin）和由a）用氰化氢香芹酮的反应及其制备方法，B）在步骤中得到的Carvonnitrils的后续反应一） 在用于形成亚胺的催化剂存在下的含Carvonnitrilimin与氢气和氨在氢化催化剂的反应混合物的氨和c）在步骤b中获得的产物的后续反应）。 本发明进一步涉及使用固化剂的环氧树脂Carvondiamin如，如在二异氰酸酯的制造中的中间体，如在聚醚多元醇和/或作为用于生产聚酰胺的单体的制造中的起动器。

    METHOD FOR PRODUCING N,N-SUBSTITUTED-3-AMINOPROPAN-1-OLS
    10.
    发明申请
    METHOD FOR PRODUCING N,N-SUBSTITUTED-3-AMINOPROPAN-1-OLS 审中-公开
    用于生产N，N-二取代-3-氨基-1- OLAND

    公开(公告)号：WO2010052181A3

    公开(公告)日：2010-09-30

    申请号：PCT/EP2009064438

    申请日：2009-11-02

    Applicant: BASF SE ,  WIGBERS CHRISTOF WILHELM ,  MELDER JOHANN-PETER ,  ERNST MARTIN

    Inventor： WIGBERS CHRISTOF WILHELM ,  MELDER JOHANN-PETER ,  ERNST MARTIN

    IPC: C07C213/00 ,  C07C215/08

    CPC classification number: C07C213/02 ,  C07C227/08 ,  Y02P20/582 ,  C07C215/08 ,  C07C229/12

    Abstract: The present invention relates to a method for producing N,N-substituted-3-aminopropan-1-ols by a) converting secondary amine with acrolein at a temperature of (-50) to 100°C and a pressure of 0.01 to 300 bar, and b) converting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a pressure of 1 to 400 bar, characterized in that in step a) the molar ratio of secondary amine to acrolein is 1:1 or more and the temperature in step b) is in the range of (-50) to 70°C. In a preferred embodiment, an acrolein that was obtained from glycerine based on renewable raw materials is used. The invention further relates to the use of an N,N-dimethyl-3-aminopropan-1-ol (DMAPOL) based on renewable raw materials as a catalyst for producing polyurethane, as a scrubbing liquid in gas scrubbing, in the field of electronics chemicals and electroplating, as a feed material in organic synthesis, and as an intermediate product in the production of pharmaceuticals and plant protection agents.

    Abstract translation: 本发明涉及一种方法，用于制备的N，N-取代的3-氨基丙-1-醇通过a）在（-50的温度下与丙烯醛仲胺的反应）至100℃和0.01的压力 至300巴，和b））在1至400巴的压力下在步骤a）与氢气和氨在氢化催化剂的存在下反应混合物中得到的产物，其特征在于，在阶段的仲胺为丙烯醛1的摩尔比反应： 1以上且在步骤b的范围为（-50）至70℃的温度） 在一个优选的实施方案中，丙烯醛被用于已经从甘油基于可再生资源获得的。 此外，本发明涉及使用一个N，基于可再生原料的N-二甲基-3-氨基丙烷-1-醇（DMAPOL）的，作为用于聚氨酯生产的催化剂，如在气体洗涤器中的洗涤液，在电子化学品和电镀领域中，如在起始原料 有机合成并作为医药和农药的制造中间体。

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