METHOD FOR CLEANING AQUEOUS GLYOXAL SOLUTIONS
    2.
    发明申请
    METHOD FOR CLEANING AQUEOUS GLYOXAL SOLUTIONS 审中-公开
    清洁水性甘醇溶液的方法

    公开(公告)号:WO2010076252A3

    公开(公告)日:2010-09-16

    申请号:PCT/EP2009067611

    申请日:2009-12-21

    CPC classification number: C07C45/80 C07C47/127

    Abstract: The invention relates to a method for cleaning an aqueous glyoxal solution comprising at least one acid by extractive acid separation, comprising the steps of: I) mixing an aqueous glyoxal solution with an ion exchanger solution, comprising 20 to 60 wt % of a tertiary amine and 80 to 40 wt % of an organic solvent immiscible with water at a dwell time of

    Abstract translation: 一种用于纯化的乙二醛水溶液,其含有至少一种酸,酸包括我步骤:a)用含有20至60重量的叔胺%和80〜40的离子交换溶液混合的乙二醛水溶液的提取分离方法 重量的非在<5分钟的停留时间的任何可与水混溶的有机溶剂和30〜100℃的温度下的%,用于在提取的乙二醛水溶液制备混合物从步骤I)中分离的混合物,II) 和加载的离子交换溶液和分离在30的温度下装载离子交换剂溶液至100℃,和iii)分离在的温度下叔胺和纯化的乙二醛水溶液和叔胺的分离所提取的乙二醛水溶液<30° C.

    METHOD AND DEVICE FOR PRODUCING ISOCYANATES
    3.
    发明申请
    METHOD AND DEVICE FOR PRODUCING ISOCYANATES 审中-公开
    制备异氰酸酯的方法和装置

    公开(公告)号:WO2010106131A3

    公开(公告)日:2010-12-29

    申请号:PCT/EP2010053527

    申请日:2010-03-18

    Abstract: The invention relates to a method for producing isocyanates by converting the corresponding amine with phosgene in the gas phase, in the presence of an inert medium as applicable, wherein phosgene and amine are first vaporized and then overheated to reaction temperature, the overheated phosgene and amine are mixed and added to a reactor wherein the phosgene and the amine are converted to isocyanate, wherein the dwell time of the phosgene at temperatures greater than 300°C equals a maximum of 5 sec and/or the temperature of heat transfer surfaces in contact with the phosgene is 20 K above the phosgene temperature to be set at maximum. The invention further relates to a device for producing isocyanates by converting the corresponding amine with phosgene in the gas phase.

    Abstract translation: 本发明涉及一种通过在气相中,与光气使相应的胺反应,任选地在惰性介质的存在下,其中光气与胺第一蒸发,然后进一步过热到一个反应温度,混合过热光气和胺和反应器中制备的异氰酸酯 被供给,其中光气与胺反应以形成异氰酸酯,其中,在温度高于300℃s的光气的停留时间不超过5和/或其中的温度是在与光气的传热表面接触在调整Phosgentemperatur上述最为20K 是。 本发明还涉及一种用于通过使相应的胺与光气在气相中反应来生产异氰酸酯的设备。

    7.
    发明专利
    未知

    公开(公告)号:AT538078T

    公开(公告)日:2012-01-15

    申请号:AT06763996

    申请日:2006-06-30

    Applicant: BASF SE

    Abstract: Process for recovering cyclododecatriene (CDT) from a solution containing CDT and high boilers such as deactivated catalyst and polymers, which includes feeding the solution into a preheater and heating it, subsequently depressurizing it through a downstream pressure maintenance device and feeding the resulting two-phase mixture into a helical tube evaporator and there reducing the CDT content of the liquid phase by partial evaporation and discharging a gaseous product stream having an increased concentration of CDT.

Patent Agency Ranking