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1.发明申请PROCESS FOR PREPARING A TITANIUM-CONTAINING ZEOLITIC MATERIAL HAVING AN MWW FRAMEWORK STRUCTURE 审中-公开制备含有MWW框架结构的含钛的ZEOLITIC材料的方法
公开(公告)号：WO2014122152A1
公开(公告)日：2014-08-14
申请号：PCT/EP2014/052205
申请日：2014-02-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , LÜTZEL, Hans-Jürgen , UHL, Georg , BAYER, Robert , VOGELSANG, Regina , TELES, Joaquim Henrique , RIEDEL, Dominic , URBANCZYK, Daniel , WEGERLE, Ulrike
CPC classification number: B01J37/0045 , B01J29/7038 , B01J29/89 , C01B39/085
Abstract: A process for the preparation of a titanium-containing zeolitic material having an MWW framework structure, the process comprising(i)providing a zeolitic material having an MWW framework structure comprising SiO 2 and B 2 O 3 , (ii)incorporating titanium into the zeolitic material provided in (i) comprising(ii.1) preparing an aqueous synthesis mixture containing the zeolitic material provided in (i), an MWW template compound and a titanium source, (ii.2) hydrothermally synthesizing a titanium-containing zeolitic material having an MWW framework structure from the aqueous synthesis mixture prepared in (ii.1), obtaining a mother liquor comprising the titanium-containing zeolitic material having an MWW framework structure;(iii)spray-drying the mother liquor obtained from (ii.2) comprising the titanium-containing zeolitic material having an MWW framework structure.
Abstract translation: 一种制备具有MWW骨架结构的含钛沸石材料的方法，该方法包括（i）提供具有包含SiO 2和B 2 O 3的MWW骨架结构的沸石材料，（ii）将钛掺入提供于（ i）包括（ii.1）制备含有（i）中提供的沸石材料的水性合成混合物，MWW模板化合物和钛源，（ii.2）水热合成具有MWW骨架结构的含钛沸石材料 从（ii.1）中制备的水性合成混合物得到包含具有MWW骨架结构的含钛沸石材料的母液;（iii）喷雾干燥由（ii.2）得到的母液， 含有MWW骨架结构的沸石材料。
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2.发明申请PROCESS FOR PREPARING A BORON CONTAINING ZEOLITIC MATERIAL HAVING MWW FRAMEWORK STRUCTURE 审中-公开制备含有MWW框架结构的含硼材料的硼砂工艺
公开(公告)号：WO2014122150A1
公开(公告)日：2014-08-14
申请号：PCT/EP2014/052203
申请日：2014-02-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , LÜTZEL, Hans-Jürgen , UHL, Georg , BAYER, Robert , VOGELSANG, Regina , SCHLOSSER, Robert , RUSLIM, Franky , CZAJKA, Pawel
CPC classification number: C01B39/12 , B01J29/86 , B01J37/009 , B01J37/04 , B01J37/06 , B01J37/08 , B01J37/10 , C01B37/007 , C01B39/46 , C01B39/48 , C01P2002/70 , C01P2006/12 , C01P2006/90
Abstract: A process for preparing an aluminum-free boron containing zeolitic material comprising the framework structure MWW (BMWW), comprising (a) hydrothermally synthesizing the BMWW from a synthesis mixture containing water, a silicon source, a boron source, and an MWW template compound obtaining the BMWW in its mother liquor, the mother liquor having a pH above 9; (b) adjusting the pH of the mother liquor, obtained in (a) and containing the BMWW, to a value in the range of from 6 to 9; (c) separating the BMWW from the pH- adjusted mother liquor obtained in (b) by filtration in a filtration device.
Abstract translation: 一种制备包含框架结构MWW（BMWW）的无铝含硼沸石材料的方法，包括（a）从含水的合成混合物，硅源，硼源和MWW模板化合物水热合成BMWW，获得 宝马在母液中，母液pH值高于9; （b）将（a）中获得并含有BMWW的母液的pH调节至6至9的值; （c）通过在过滤装置中过滤将BMWW与（b）中得到的经pH调节的母液分离。
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3.发明申请A TIN-CONTAINING ZEOLITIC MATERIAL HAVING AN MWW-TYPE FRAMEWORK STRUCTURE 审中-公开含有MWW型框架结构的含TIN的新兴材料
公开(公告)号：WO2015067655A1
公开(公告)日：2015-05-14
申请号：PCT/EP2014/073809
申请日：2014-11-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , UHL, Georg , TELES, Joaquim Henrique , VAUTRAVERS, Nicolas , RIEDEL, Dominic
CPC classification number: B01J29/7088 , B01J35/002 , B01J35/1019 , B01J37/08 , B01J37/30 , B01J2229/183 , B01J2229/186 , C01B39/026 , C01B39/06 , C01B39/12 , C01B39/46 , C01B39/48 , C07C45/58 , C07C2601/10 , C07C47/225
Abstract: A process for preparing a tin-containing zeolitic material having an MWW-typeframe- work structure comprising providing a zeolitic material having an MWW-typeframework structure having vacant tetrahedral framework sites, providing a tin-ion source in solid form,and incorporating tin into the zeolitic material via solid-state ion exchange.
Abstract translation: 一种制备具有MWW型框架结构的含锡沸石材料的方法，包括提供具有具有空白四面体框架位点的MWW型框架结构的沸石材料，提供固体形式的锡离子源，并将锡掺入 沸石材料通过固态离子交换。
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4.发明申请
公开(公告)号：WO2018115117A1
公开(公告)日：2018-06-28
申请号：PCT/EP2017/083806
申请日：2017-12-20
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , LÜTZEL, Hans-Jürgen , UHL, Georg , TELES, Joaquim Henrique , RIEDEL, Dominic , URBANCZYK, Daniel , WEGERLE, Ulrike , WEBER, Markus , WÖRZ, Nicolai Tonio , MÜLLER, Christian
Abstract: A process for preparing an extrudable composition comprising a titanium-containing zeo- litic material having framework type MWW, the process comprising providing a titanium- containing zeolitic material having framework type MWW, having a water absorption ca- pacity of at least 11 weight-%, subjecting the titanium-containing zeolitic material having framework type MWW an acid treatment, optionally incorporating zinc in the acid-treated titanium-containing zeolitic material having framework type MWW; preparing a composi- tion comprising the titanium-containing zeolitic material having framework type MWW obtained from (ii) or (iii), a precursor of a silica binder, water, and a kneading agent, wherein the composition does not comprise a polyethylene oxide.
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5.发明申请A PROCESS FOR THE PREPARATION OF AN MWW ZEOLITIC MATERIAL COMPRISING BORON AND TITANIUM 审中-公开制备包含硼和钛的MWW ZEOLITIC MATERIAL的制备方法
公开(公告)号：WO2016038030A1
公开(公告)日：2016-03-17
申请号：PCT/EP2015/070488
申请日：2015-09-08
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , UHL, Georg , TELES, Joaquim Henrique , RIEDEL, Dominic
CPC classification number: B01J29/89 , B01J37/0009 , B01J37/0018 , B01J37/009 , B01J37/04 , B01J37/06 , B01J37/086 , B01J37/10 , C01B39/00 , C01B39/085 , C01B39/12 , C01B39/48 , C01P2002/72 , C01P2002/82 , C01P2002/86
Abstract: A process for the preparation of a zeolitic material having an MWW framework structure and comprising boron and titanium, the process comprising (i) providing an aqueous synthesis mixture comprising a silica source, a boron source, a titanium source, and an MWW templating agent; (ii) heating the aqueous synthesis mixture to a temperature in the range of from 160 to 190 °C; (iii) subjecting the synthesis mixture (ii) to hydrothermal synthesis conditions, obtaining, in its mother liquor, a precursor of the zeolitic material; (iv) separating the precursor from its mother liquor; (v) calcining the separated precursor, obtaining the zeolitic material having an MWW framework structure and comprising boron and titanium.
Abstract translation: 一种制备具有MWW骨架结构并包含硼和钛的沸石材料的方法，该方法包括（i）提供包含二氧化硅源，硼源，钛源和MWW模板剂的含水合成混合物; （ii）将所述水性合成混合物加热至160至190℃的温度; （iii）使合成混合物（ii）经受水热合成条件，在其母液中获得沸石材料的前体; （iv）从其母液中分离前体; （v）煅烧分离的前体，获得具有MWW骨架结构并包含硼和钛的沸石材料。
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Patent Agency Ranking
公开(公告)号：WO2018115118A1
公开(公告)日：2018-06-28
申请号：PCT/EP2017/083810
申请日：2017-12-20
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , LÜTZEL, Hans-Jürgen , UHL, Georg , TELES, Joaquim Henrique , RIEDEL, Dominic , URBANCZYK, Daniel , WEGERLE, Ulrike , WEBER, Markus , WÖRZ, Nicolai Tonio , MÜLLER, Christian , SCHMITT, Rüdiger , ROMANI FERNANDEZ, Xiana , WÜRZ, Harald
Abstract: Use of an acid-treated titanium-containing zeolitic material having framework type MWW for preparing a composition having a relative plasticity of less than 1.
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7.发明申请
公开(公告)号：WO2015067654A1
公开(公告)日：2015-05-14
申请号：PCT/EP2014/073803
申请日：2014-11-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , TELES, Joaquim Henrique , VAUTRAVERS, Nicolas , UHL, Georg , HERMANS, Ive , WOLF, Patrick , HAMMOND, Ceri
IPC: C01B39/06 , C07D313/04 , C01B39/12
CPC classification number: B01J29/7057 , B01J29/06 , B01J29/40 , B01J29/7007 , B01J29/7015 , B01J29/7038 , B01J29/7065 , B01J29/7088 , B01J29/89 , B01J35/002 , B01J35/1019 , B01J37/10 , B01J37/30 , B01J2229/183 , B01J2229/186 , C01B39/026 , C01B39/06 , C01B39/38 , C01B39/46 , C01P2002/82 , C07D313/04
Abstract: A process for preparing a tin-containing zeolitic material having a BEA framework structure comprising providing a zeolitic material having a BEA framework structure having vacant tetrahedral framework sites, providing a tin-ion source in solid form, incorporating tin into the zeolitic material via solid-state ion exchange, calcining the zeolitic material, and treating the calcined zeolitic material with an aqueous solution having a pH of at most 5.
Abstract translation: 一种制备具有BEA骨架结构的含锡沸石材料的方法，包括提供具有空白四面体骨架位点的BEA骨架结构的沸石材料，提供固体形式的锡离子源，通过固相合成将锡掺入沸石材料中， 状态离子交换，煅烧沸石材料，以及用pH至多为5的水溶液处理煅烧沸石材料。
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公开(公告)号：WO2013117537A1
公开(公告)日：2013-08-15
申请号：PCT/EP2013/052224
申请日：2013-02-05
Applicant: BASF SE
Inventor： MÜLLER, Ulrich , PARVULESCU, Andrei-Nicolae , YANG, Jeff , LÜTZEL, Hans-Jürgen , UHL, Georg , DUMSER, Stefan
CPC classification number: C01B39/026 , B01J29/86 , B01J29/89 , B01J37/0045 , B01J2229/22 , B01J2229/30 , C01B39/12
Abstract: The present invention relates to a process for process for the preparation of a zeolitic material which process comprises (i) providing a boron-containing zeolitic material and (ii) deboronating the boron-containing zeolitic material by treating the boron-containing zeolitic material with a liquid solvent system thereby obtaining a deboronated zeolitic material, which liquid solvent system does not contain an inorganic or organic acid, or a salt thereof.
Abstract translation: 本发明涉及一种制备沸石材料的方法，该方法包括（i）提供含硼沸石材料和（ii）通过用含硼沸石材料处理含硼沸石材料来使硼含量沸石材料脱硼 液体溶剂系统，从而获得脱硼沸石材料，该液体溶剂体系不含无机或有机酸或其盐。
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公开(公告)号：EP3066051A1
公开(公告)日：2016-09-14
申请号：EP14795813.6
申请日：2014-11-05
Applicant: BASF SE
Inventor： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , TELES, Joaquim Henrique , VAUTRAVERS, Nicolas , UHL, Georg , HERMANS, Ive , WOLF, Patrick , HAMMOND, Ceri
IPC: C01B39/06 , C07D313/04 , C01B39/12
CPC classification number: B01J29/7057 , B01J29/06 , B01J29/40 , B01J29/7007 , B01J29/7015 , B01J29/7038 , B01J29/7065 , B01J29/7088 , B01J29/89 , B01J35/002 , B01J35/1019 , B01J37/10 , B01J37/30 , B01J2229/183 , B01J2229/186 , C01B39/026 , C01B39/06 , C01B39/38 , C01B39/46 , C01P2002/82 , C07D313/04
Abstract: A process for preparing a tin-containing zeolitic material having a BEA framework structure comprising providing a zeolitic material having a BEA framework structure having vacant tetrahedral framework sites, providing a tin-ion source in solid form, incorporating tin into the zeolitic material via solid-state ion exchange, calcining the zeolitic material, and treating the calcined zeolitic material with an aqueous solution having a pH of at most 5.
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公开(公告)号：EP2812282B1
公开(公告)日：2018-05-09
申请号：EP13702241.4
申请日：2013-02-05
Applicant: BASF SE
Inventor： MÜLLER, Ulrich , PARVULESCU, Andrei-Nicolae , YANG, Jeff , LÜTZEL, Hans-Jürgen , UHL, Georg , DUMSER, Stefan
CPC classification number: C01B39/026 , B01J29/86 , B01J29/89 , B01J37/0045 , B01J2229/22 , B01J2229/30 , C01B39/12
Abstract: The present invention relates to a process for process for the preparation of a zeolitic material which process comprises (i) providing a boron-containing zeolitic material and (ii) deboronating the boron-containing zeolitic material by treating the boron-containing zeolitic material with a liquid solvent system thereby obtaining a deboronated zeolitic material, which liquid solvent system does not contain an inorganic or organic acid, or a salt thereof.
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