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    1.
    发明专利
    未知

    公开(公告)号：DE50205120D1

    公开(公告)日：2006-01-05

    申请号：DE50205120

    申请日：2002-07-09

    Applicant: DEGUSSA

    Inventor： DESCHLER DR ,  KRAFCZYK DR ,  LUGINSLAND DR ,  KORTH DR ,  KIEFER INGO ,  HORN DR

    IPC: C07B61/00 ,  C07F7/18 ,  C08K5/5419 ,  C08L21/00

    Abstract: Trialkoxysilyl compounds in which one or two of the methoxy or alkoxy groups attached to silicon are replaced by larger groups, e.g. 9-30C alkyl, aryl, 2-30C alkyl(poly)ether or triorganosilyl are new. Organosilicon compounds of formula (I) and/or (II) are new. R = methyl or ethyl; R' = 9-30C alkyl or alkenyl, aryl, aralkyl, 2-30C alkylether, 2-30C alkyl-polyether (all optionally branched) or R'''3Si; R'' = optionally unsaturated 1-30C aliphatic, aromatic or aliphatic/aromatic hydrocarbylene; R''' = 1-30C alkyl or alkenyl, aralkyl or aryl; X = NH3-n with n = 1, 2 or 3 and m = 1, or OCOR' with n = m = 1, or SH with n = m = 1, or S with n = 2 and m = 1-10, or SCOR' with n = m = 1, or H with n = m = 1. Independent claims are also included for: (1) a method for the production of (I) and (II) by reacting trialkoxysilyl compounds of formula ((RO)3Si-R)n-Xm (III) with alcohols R'-OH, with continuous removal of the resulting R-OH by distillation; and (2) rubber mixtures containing rubber, filler etc. and at least one compound (I) and/or (II).

    2.
    发明专利
    未知

    公开(公告)号：DE50104868D1

    公开(公告)日：2005-01-27

    申请号：DE50104868

    申请日：2001-09-06

    Applicant: DEGUSSA

    Inventor： KRAFCZYK DR ,  DESCHLER DR ,  MICHEL RUDOLF ,  BATZ-SOHN DR

    IPC: C07F7/18

    Abstract: Production of yellow bis-(3-(triethoxysilyl)-propyl)polysulfane (average sulfur chain length less than 4 and iodine color number no greater than 10 mg iodine/100 ml) comprises mixing neutral chloropropyltriethoxysilane with chloropropyltrichlorosilane and reaction with sodium sulfide and sulfur, disodium tetrasulfide and Nas2S or disodium trisulfide and Na2S in ethanol. A process for the production of yellow bis-(3-(triethoxysilyl)-propyl)polysulfone having an average sulfur chain length of less than 4 and an iodine color number of no greater than 10 mg iodine/100 ml comprises mixing neutral chloropropyltriethoxysilane with chloropropyltrichlorosilane followed by reaction with sodium sulfide (Na2S) and sulfur, disodium tetrasulfide (N2S4) and Nas2S or disodium trisulfide (Na2S3) and Na2S in ethanol.

    3.
    发明专利
    未知

    公开(公告)号：DE50108425D1

    公开(公告)日：2006-01-26

    申请号：DE50108425

    申请日：2001-05-12

    Applicant: DEGUSSA

    Inventor： KRAFCZYK DR ,  DESCHLER DR ,  MICHEL RUDOLF

    IPC: C07F7/18

    Abstract: Process for the preparation of yellow bis(3-[triethoxysilyl]propyl)tetrasulfane having an iodine colour value of

    4.
    发明专利
    未知

    公开(公告)号：DE50300291D1

    公开(公告)日：2005-03-10

    申请号：DE50300291

    申请日：2003-04-25

    Applicant: DEGUSSA

    Inventor： KRAFCZYK DR ,  DESCHLER DR ,  LUGINSLAND DR ,  REIMUND DR ,  HASSE ANDRE ,  MAYER MELANIE

    IPC: C07B61/00 ,  B60C1/00 ,  C07F7/18 ,  C08K5/00 ,  C08K5/548 ,  C08L21/00

    Abstract: Mercaptosilanes with 9-30C alkoxy as well as methoxy and/or ethoxy substituents are new. Mercaptosilanes with 9-30C alkoxy as well as methoxy and/or ethoxy substituents and of formula RO-Si(R1O)2-R2-SH (I) or R1O-Si(RO)2-R2-SH (II) are new when R1 is a mixture and the content of one component in the mixture is 10-50 mol.%. R = methyl or ethyl; R1 = 9-30C alkyl; and R2 = optionally unsaturated aliphatic and/or aromatic 1-30C hydrocarbylene An Independent claim is also included for preparation of the mercaptosilanes.

    5.
    发明专利
    未知

    公开(公告)号：DE50205449D1

    公开(公告)日：2006-02-02

    申请号：DE50205449

    申请日：2002-07-09

    Applicant: DEGUSSA

    Inventor： DESCHLER DR ,  KRAFCZYK DR ,  LUGINSLAND DR ,  KORTH DR ,  KIEFER INGO ,  HORN DR

    IPC: C07B61/00 ,  C07F7/18 ,  C08K5/5419 ,  C08L21/00

    Abstract: Trialkoxysilyl compounds in which one or two of the methoxy or alkoxy groups attached to silicon are replaced by larger groups, e.g. 9-30C alkyl, aryl, 2-30C alkyl(poly)ether or triorganosilyl are new. Organosilicon compounds of formula (I) and/or (II) are new. R = methyl or ethyl; R' = 9-30C alkyl or alkenyl, aryl, aralkyl, 2-30C alkylether, 2-30C alkyl-polyether (all optionally branched) or R'''3Si; R'' = optionally unsaturated 1-30C aliphatic, aromatic or aliphatic/aromatic hydrocarbylene; R''' = 1-30C alkyl or alkenyl, aralkyl or aryl; X = NH3-n with n = 1, 2 or 3 and m = 1, or OCOR' with n = m = 1, or SH with n = m = 1, or S with n = 2 and m = 1-10, or SCOR' with n = m = 1, or H with n = m = 1. Independent claims are also included for: (1) a method for the production of (I) and (II) by reacting trialkoxysilyl compounds of formula ((RO)3Si-R)n-Xm (III) with alcohols R'-OH, with continuous removal of the resulting R-OH by distillation; and (2) rubber mixtures containing rubber, filler etc. and at least one compound (I) and/or (II).

    7.
    发明专利
    未知

    公开(公告)号：DE50003514D1

    公开(公告)日：2003-10-09

    申请号：DE50003514

    申请日：2000-11-04

    Applicant: DEGUSSA

    Inventor： KRAFCZYK DR ,  MUENZENBERG DR ,  ZEZULKA GERD RAINHARD

    IPC: C07F9/165

    Abstract: A process for the production of sulfur- and phosphorus-containing silane compounds comprises reaction of a halogen containing silane with phosphorus pentasulfide and a metal sulfide. A process for the production of sulfur- and phosphorus-containing compounds of formula (R n(R O)3-n-Si-Alk-S-)3P=S (1) comprises reaction of a halogen-containing silane of formula R n(R O)3-n-Si-Alk-Hal (2) with phosphorus pentasulfide (P4S10) and a metal sulfide. Alk = 1-10C alkylene; R ,R each = 1-5C alkyl, 5-8C cycloalkyl, phenyl, benzyl or 2-methoxyethyl; Hal = halogen; and n = 0-2.

    10.
    发明专利
    未知

    公开(公告)号：DE59907927D1

    公开(公告)日：2004-01-15

    申请号：DE59907927

    申请日：1999-10-26

    Applicant: DEGUSSA

    Inventor： LUGINSLAND DR ,  KRAFCZYK DR ,  LORTZ DR

    IPC: B60C1/00 ,  B29D30/06 ,  B60C11/00 ,  C08G77/28 ,  C08G77/392 ,  C08G77/50 ,  C08L9/00 ,  C08L21/00 ,  C08L83/08 ,  C08L83/14

    Abstract: Sulfur-functional polyorganosiloxanes containing side-chain groups which can bond with silicic acid (preferably alkoxy or haloalkoxy) and side-chain groups which can bond with elastomers, preferably mercapto, thiocyanato, disulfide or polysulfide groups. Sulfur-functional polyorganosiloxanes of formula (I), R -R = H, 1-4C alkyl, alkoxy, haloalkyl or haloalkoxy, phenyl, aryl or aralkyl; W = a group which can bond to silicic acid, preferably 1-4C alkoxy or haloalkoxy; Y = alkyl, haloalkyl, phenyl, aryl or aralkyl; Z = a 0-6C alkylidene group; A = a group which can form bonds with at least one elastomer in a rubber mixture, i.e. mercapto or thiocyanato if q = 1, or disulfide or polysulfide (Sx) if q = 2; x = 2-10; (k+m+n+p) = 3 or more; k = n = 0 (optionally). Independent claims are also included for (a) a process for the production of (I) by reacting compounds of formula (IV) with compounds of formula MSH, MSCN or M2Sx, or with M2S and sulfur, in an alcohol W-H at 20-150 degrees C under normal pressure, optionally with a catalyst, using compounds in which X = halogen; M = a metal ion; (b) rubber mixtures containing (I); (c) a process for the production of rubber mixtures by using (I) and other filler(s) in addition to rubber; (d) molded products obtained from these rubber mixtures.

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