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    BIS-(SILYL-ETHYL)-OLIGOSULPHIDES AND A PROCESS FOR THEIR PRODUCTION
    2.
    发明专利
    BIS-(SILYL-ETHYL)-OLIGOSULPHIDES AND A PROCESS FOR THEIR PRODUCTION 未知

    公开(公告)号：CA1144936A

    公开(公告)日：1983-04-19

    申请号：CA342418

    申请日：1979-12-20

    Applicant: DEGUSSA

    Inventor： SCHWARZ RUDOLF ,  KLEINSCHMIT PETER ,  LIEDTKE CHRISTA ,  WOLFF SIEGFRIED

    IPC: C08L7/00 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C08G75/02 ,  C08G75/14 ,  C08K5/5425 ,  C08K5/548 ,  C08L21/00 ,  C08L23/00 ,  C08L33/00 ,  C08L33/02 ,  C08L101/00 ,  C08K5/54

    Abstract: Bis-(silyl-ethyl)-oligosulphide obtained by reacting a vinyl silane having the formula (CH2=CH)m-SiR?R4-(m+n) wherein R represents chlorine, iodine, C1-C3-alkoxy, 2-methoxy-ethoxy, 2-ethoxy-ethoxy or hydroxy, R1 represents C1-C3-alkyl, phenyl or C5-C7-cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m + n is 1, 2 or 3, with sulphur and, when required, with hydrogen sulphide in a molar ratio ranging from 1:2.5 to 1:10 and of vinyl silane to hydrogen sulphide from 1:0 to 0:5 at a temperature between approximately 100 and 200.degree.C under a pressure ranging from 1 to 25 bars (total pressure at the reaction temperature) and in the presence of Sulphidation catalysts and when required hydrolysis or partial hydrolysis of the reaction product. The corresponding process of production and the use of a bis-(silyl-ethyl)-oligosulphide as a reinforcing additive (adhesion promoter) in a crosslinkable rubber mixture containing a silicate filler and when required carbon black as well as sulphur and other conventional mixture components are also disclosed.

    3.
    发明专利
    未知

    公开(公告)号：DD147945A5

    公开(公告)日：1981-04-29

    申请号：DD21746279

    申请日：1979-12-07

    Applicant: DEGUSSA

    Inventor： SCHWARZ RUDOLF ,  KLEINSCHMIDT PETER ,  LIEDTKE CHRISTA ,  WOLFF SIEGFRIED

    IPC: C08L7/00 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C08G75/02 ,  C08G75/14 ,  C08K5/5425 ,  C08K5/548 ,  C08L21/00 ,  C08L23/00 ,  C08L33/00 ,  C08L33/02 ,  C08L101/00

    Abstract: Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH2=CH)m-SiRn1R4-(m+n) in which R represents chlorine, bromine, iodine, C1-C3-alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R1 represents C1-C3-alkyl, phenyl or C5-C7-cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100 DEG and 200 DEG C. under pressure of from 1 to 25 bars (total pressure at the reaction) temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.

    BIS-(SILYLETHYL)-OLIGOSULPHIDES AND PREPARATION THEREOF
    4.
    发明专利
    BIS-(SILYLETHYL)-OLIGOSULPHIDES AND PREPARATION THEREOF 未知

    公开(公告)号：MY8500457A

    公开(公告)日：1985-12-31

    申请号：MY8500457

    申请日：1985-12-30

    Applicant: DEGUSSA

    Inventor： SCHWARZ RUDOLF ,  KLEINSCHMIT PETER ,  LIEDTKE CHRISTA ,  WOLFF SIEGFRIED

    IPC: C08L7/00 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C08G75/02 ,  C08G75/14 ,  C08K5/5425 ,  C08K5/548 ,  C08L21/00 ,  C08L23/00 ,  C08L33/00 ,  C08L33/02 ,  C08L101/00 ,  C08K5/54

    Abstract: Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH2=CH)m-SiRn1R4-(m+n) in which R represents chlorine, bromine, iodine, C1-C3-alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R1 represents C1-C3-alkyl, phenyl or C5-C7-cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100 DEG and 200 DEG C. under pressure of from 1 to 25 bars (total pressure at the reaction) temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.

    5.
    发明专利
    未知

    公开(公告)号：DE2856229A1

    公开(公告)日：1980-07-03

    申请号：DE2856229

    申请日：1978-12-27

    Applicant: DEGUSSA

    Inventor： SCHWARZ RUDOLF DR ,  KLEINSCHMIT PETER DR ,  LIEDTKE CHRISTA ,  WOLFF SIEGFRIED DIPL CHEM

    IPC: C08L7/00 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C08G75/02 ,  C08G75/14 ,  C08K5/5425 ,  C08K5/548 ,  C08L21/00 ,  C08L23/00 ,  C08L33/00 ,  C08L33/02 ,  C08L101/00 ,  C08L9/00 ,  C08K5/37 ,  C08K5/54

    Abstract: Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH2=CH)m-SiRn1R4-(m+n) in which R represents chlorine, bromine, iodine, C1-C3-alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R1 represents C1-C3-alkyl, phenyl or C5-C7-cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100 DEG and 200 DEG C. under pressure of from 1 to 25 bars (total pressure at the reaction) temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.

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