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公开(公告)号:CZ9700984A3
公开(公告)日:1998-05-13
申请号:CZ98497
申请日:1997-04-01
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING , SCHNAITMANN DIETER DR , BOHMER MARTIN
CPC classification number: C09B48/00
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公开(公告)号:DE4433041A1
公开(公告)日:1996-03-21
申请号:DE4433041
申请日:1994-09-16
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING , WILKER GERHARD
Abstract: Prepn. of 4,10-dibromo-anthraquinone pigment (I) comprises (a) wet milling coarsely crystalline crude (I) to the required fineness in aq. medium in a stirred ball mill with a power of over 2.5 kW/l and stirrer peripheral velocity of over 12 m/s, using milling balls with a dia. of less than 1.0 mm; and (b-1) isolating (I) from the suspension or (b-2) finishing the pre-pigment from wet milling by high temp. treatment in an aq. or aq.-organic medium or liquid aromatic cpd. and then isolating (I).
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公开(公告)号:DE3926563A1
公开(公告)日:1991-02-14
申请号:DE3926563
申请日:1989-08-11
Applicant: HOECHST AG
Inventor: DIETZ ERWIN DR , URBAN MANFRED DIPL ING
IPC: C09B5/62
Abstract: New perylene compounds based on perylene-3,4,9,10-tetracarboxylic monoanhydride monoimides substituted on one or both imide nitrogen atoms by alkylene- or arylenesulphonic groups, or on corresponding tetracarboxylic diimides or on a halogenated product thereof can be used not only as dispersing agents for pigments of the same class of compounds or other categories but also directly as pigments and fluorescent as well as polymer-soluble dyes.
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公开(公告)号:DE4413848A1
公开(公告)日:1995-10-26
申请号:DE4413848
申请日:1994-04-21
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING
IPC: C09B67/00 , C09B67/04 , C09B67/10 , C09B67/12 , C09B67/20 , C09D17/00 , C09D11/02 , C08K5/3417 , D01F1/04 , B02C17/14 , B02C17/00 , B02C23/06
Abstract: Fine pulverisation of crude Cu phthalocyanine (CuPc) pigments comprises (a) dry grinding the coarsely crystalline pigment, then (b) wet milling the prepigment in aq. suspension, with addn. of 0.1-5 wt.% inert organic solvent, in a ball mill with stirrer, operating at a power of over 2.5 kW/l and stirring rate of 12 m/s, using milling balls with a dia. of at most 1 mm.
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公开(公告)号:DE4403231A1
公开(公告)日:1995-08-10
申请号:DE4403231
申请日:1994-02-03
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING
IPC: C09B67/04 , C09B48/00 , C09B67/00 , C09B67/10 , C09B67/22 , C09B67/52 , C09K23/32 , C09B67/20 , B01F17/32 , C09D17/00 , C09D11/02 , C07D471/04 , C08K5/3437 , B02C17/00
Abstract: Prodn. of pigments (IA), mixed crystal pigments (IB) or pigment formulations (IC) based on linear, (un)substd. quinacridones comprises (a) wet milling the coarsely crystalline crude pigment to the required deg. of fineness in a liquid aq., aq. organic or organic medium in a ball mill with a power of over 2.5 kW/l, which has a stirrer operating at a peripheral velocity of over 12 ms and used milling balls with a dia. of at most 0.9 mm; (b) opt. subjecting the pre-pigment to solvent treatment at 50-200 deg.C; and then (c) isolating the pigment in the usual way.
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公开(公告)号:DE19510668A1
公开(公告)日:1996-09-26
申请号:DE19510668
申请日:1995-03-23
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING , WILKER GERHARD
Abstract: Prepn. of 4,10-dibromo-anthraquinone pigment (I) comprises (a) wet milling coarsely crystalline crude (I) to the required fineness in aq. medium in a stirred ball mill with a power of over 2.5 kW/l and stirrer peripheral velocity of over 12 m/s, using milling balls with a dia. of less than 1.0 mm; and (b-1) isolating (I) from the suspension or (b-2) finishing the pre-pigment from wet milling by high temp. treatment in an aq. or aq.-organic medium or liquid aromatic cpd. and then isolating (I).
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公开(公告)号:DE3926564A1
公开(公告)日:1991-02-14
申请号:DE3926564
申请日:1989-08-11
Applicant: HOECHST AG
Inventor: DIETZ ERWIN DR , URBAN MANFRED DIPL ING
IPC: C09B5/62 , C08K13/06 , C09B67/20 , C09B67/22 , C09D7/12 , C09D11/02 , C09D11/10 , C09D161/20 , C09D161/28
Abstract: PCT No. PCT/EP90/01311 Sec. 371 Date Mar. 6, 1992 Sec. 102(e) Date Mar. 6, 1992 PCT Filed Aug. 9, 1990 PCT Pub. No. WO91/02034 PCT Pub. Date Feb. 21, 1991.Pigment preparations consisting essentially of (a) at least one pigment based on perylene-3,4,9,10-tetracarboxylic dianhydride or on corresponding monoimides or diimides of tetracarboxylic acid monoanhydride, or a halogenation product thereof, (b) at least one pigment dispergent based on perylene-3,4,9,10-monoimide substituted on one or both imide nitrogen atoms by alkylene or arylene sulphonic or carboxylic acid groups or on corresponding diimides of tetracarboxylic acid monoanhydride, or a halogenation product thereof. The dispergents used appreciably enhance the key properties of perylene pigments, such as dispersibility, coloring power, stability to flocculation, transparency, rheological behavior and surface properties of the application medium. These new preparations are suitable for the pigmentation of high-quality lacquers and synthetic resins.
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公开(公告)号:DE3931052A1
公开(公告)日:1990-03-22
申请号:DE3931052
申请日:1989-09-16
Applicant: HOECHST AG
Inventor: DIETZ ERWIN DR , SCHIESSLER SIEGFRIED DR , URBAN MANFRED DIPL ING
Abstract: Pigment prepn. contains organic pigments (I) and basic additives, which are 1,3,6-trioxo- 1,3,6-trihydro- benzimidazo(2,1-b)benzo (1mn)(3,8)phenanthrolin-2-yl cpds. of formula (Q-A)xY (II), where Q = a gp. of formula (III), R1 = halogen, 1-4C alkyl, 1-4C alkoxy or CN; R2 = halogen; m and n = 0, 1, 2, 3 or 4; A = a chemical bond or a divalent -(CH2)p-, -CR3R4-, arylene, -S-, -O-or -NR5- gp. or a combination of these; p = 1-12; R3 and R5 = H or 1-6C alkyl; R4 = 1-6C alkyl; Y = a tert. N atom, -NR6R7, =NR8 or a satd. or unsatd. heterocyclic gp. and contains at least one tert. N atom; R6-8 = 1-20C alk(en)yl (opt. with hetero-atoms in the chain and/or terminal OH, prim. amino or acylamino gps.), a 5-6C cycloaliphatic or araliphatic gp. or an alkylene-heteroaryl gp.; x = 1-6. USE/ADVANTAGE - The prepn. is claimed for pigmenting high mol. organic materials and lacquer systems. It has much better dispersibility, flocculation stability, rheology, gloss and strength of colour than usual and is useful in plastic compsns., melts, spinning solns., lacquers, paints and printing inks.
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公开(公告)号:CZ98497A3
公开(公告)日:1998-05-13
申请号:CZ98497
申请日:1997-04-01
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING , SCHNAITMANN DIETER DR , BOHMER MARTIN
Abstract: Preparation of pigments, mixed crystal pigments or pigment preparations based on linear, optionally substituted quinacridones of formula (I) is by hydrolysing a cyclisation reaction mixture of a dianilinoterephthalic acid of formula (IA) and a polyphosphoric acid (or ester) with water or an aqueous mineral acid solution at 110 degrees C or above and then, depending on the nature of the product (A) directly isolating the pigment; (B) subjecting the pre-pigment to a finishing treatment, optionally after adding an organic solvent, and then isolating it; (C) finely dividing the coarse crystalline crude pigment and then isolating it; or (D) subjecting the finely-divided pre-pigment to a finishing treatment, optionally after adding a solvent, and then isolating it. In the formulae, R , R = H, Cl, Br or F or 1-4C alkyl, 1-4C alkoxy, carbonamido (optionally substituted by 1-6C alkyl) or a phenoxy- or aryl-ring optionally substituted by further aromatic, aliphatic or heterocyclic rings.
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公开(公告)号:DE4413849A1
公开(公告)日:1995-10-26
申请号:DE4413849
申请日:1994-04-21
Applicant: HOECHST AG
Inventor: URBAN MANFRED DIPL ING
IPC: C09B67/00 , C09B67/04 , C09B67/20 , C09D17/00 , C09D11/02 , C08J3/20 , C08K5/3437 , D01F1/04 , B02C17/14 , B02C17/00 , B02C23/06
Abstract: Fine pulverisation of crude polycyclic organic pigments comprises (a) dry grinding the coarsely crystalline pigment, then (b) wet milling the prepigment in aq. suspension in a ball mill with stirrer, operating at a power of over 2.5 kW/l and stirring rate of 12 m/s, using milling balls with a dia. of at most 1 mm.
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