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    PROCESS FOR PREPARATION OF ALUMINUM SALT OF PHOSPHONIC ACID ESTER
    2.
    发明申请
    PROCESS FOR PREPARATION OF ALUMINUM SALT OF PHOSPHONIC ACID ESTER 审中-公开
    磷酸铝的制备方法

    公开(公告)号：WO2013077989A1

    公开(公告)日：2013-05-30

    申请号：PCT/US2012/063310

    申请日：2012-11-02

    Applicant: ICL-IP AMERICA INC.

    Inventor： ZILBERMAN, Joseph ,  LEE, Julia ,  LEVCHIK, Sergei, V. ,  YANG, Yankai

    IPC: C07F9/40 ,  C08K5/5333 ,  C09K21/12

    CPC classification number: C09K21/12 ,  C07F9/4006 ,  C07F9/4021 ,  C07F9/5407 ,  C07F9/5442 ,  C08K5/5317 ,  C08K5/5333

    Abstract: There is provided herein a process for the preparation of aluminum salts of phosphonic acid esters by reacting phosphonic acid diesters with aluminum hydroxide in the presence of a catalyst. The catalyst is selected from the group consisting of a phase transfer catalyst, a thermally stable tertiary amine having a boiling point higher than about 140°C, a thermally stable tertiary phosphine having a boiling point higher than 140°C and combinations thereof. The aluminum phosphonates prepared can be used for making flame retarded thermoplastic polymers.

    Abstract translation: 本文提供了在催化剂存在下使膦酸二酯与氢氧化铝反应制备膦酸酯的铝盐的方法。 催化剂选自相转移催化剂，沸点高于约140℃的热稳定叔胺，沸点高于140℃的热稳定叔膦及其组合。 所制备的膦酸铝可用于制备阻燃热塑性聚合物。

    POLYOLEFIN FLAME RETARDANT COMPOSITION AND SYNERGISTS THEREOF
    3.
    发明申请
    POLYOLEFIN FLAME RETARDANT COMPOSITION AND SYNERGISTS THEREOF 审中-公开
    聚烯烃阻燃剂组合物及其合成

    公开(公告)号：WO2013116283A1

    公开(公告)日：2013-08-08

    申请号：PCT/US2013/023768

    申请日：2013-01-30

    Applicant: ICL-IP AMERICA INC.

    Inventor： LEVCHICK, Sergei, V. ,  ZILBERMAN, Joseph ,  DESIKAN, Anantha, Narayan ,  ALESSIO, Gerald, R.

    IPC: C08K5/5333 ,  C08K3/22 ,  H01B3/44 ,  H01B7/295

    CPC classification number: C08K5/5333 ,  C08K3/016 ,  C08K3/22 ,  C08K5/5313 ,  C08K5/5317 ,  C08K2003/2227 ,  H01B3/28 ,  H01B3/441 ,  H01B7/295 ,  Y10T428/139 ,  C08L23/02

    Abstract: There is provided herein a flame-retarded polyolefin composition comprising a thermoplastic polyolefin, an inorganic flame retardant filler and a metal phosphonate or metal phosphinate synergist of the general formula (A): where Me is a metal, R 1 and R 2 are the same or different linear or branched or cyclic alkyls having up to 6 carbon atoms, or benzyl, n is a metal valency and can be, 1, 2, 3 or 4, x is 1 for metal phosphonates and x is 0 for metal phosphinates. There is also provided a method for making a flame-retarded polyolefin composition comprising contacting at least one thermoplastic polyolefin polymer with at least one inorganic flame retardant filler and at least one metal phosphonate or metal phosphinate synergist and heating the mixture to above the melting temperature of the thermoplastic polyolefin.f

    Abstract translation: 本文提供了阻燃聚烯烃组合物，其包含热塑性聚烯烃，无机阻燃填料和通式（A）的金属膦酸盐或金属次膦酸盐增效剂：其中Me是金属，R 1和R 2相同或不同 具有至多6个碳原子的直链或支链或环状烷基或苄基，n是金属价态，并且对于金属膦酸盐可以是1,2,3或4，对于金属膦酸盐，x是0。 还提供了一种制备阻燃聚烯烃组合物的方法，其包括使至少一种热塑性聚烯烃聚合物与至少一种无机阻燃填料和至少一种金属膦酸盐或金属次膦酸盐增效剂接触，并将混合物加热至高于 热塑性聚烯烃

    WATER MISCIBLE SOLVENT BASED PROCESS FOR PURIFYING A BISPHOSPHATE
    4.
    发明申请
    WATER MISCIBLE SOLVENT BASED PROCESS FOR PURIFYING A BISPHOSPHATE 审中-公开
    用于净化双磷酸盐的基于水的混合溶剂的方法

    公开(公告)号：WO2010075276A1

    公开(公告)日：2010-07-01

    申请号：PCT/US2009/068975

    申请日：2009-12-21

    Applicant: ICL-IP AMERICA INC. ,  ZILBERMAN, Joseph ,  CANFI, Dorit ,  GREGOR, Andrew ,  PIOTROWSKI, Andrew

    Inventor： ZILBERMAN, Joseph ,  CANFI, Dorit ,  GREGOR, Andrew ,  PIOTROWSKI, Andrew

    IPC: C07F9/12 ,  C08K5/523 ,  C09K21/12

    CPC classification number: C07F9/12 ,  C08K5/523 ,  C09K21/12

    Abstract: There is provided herein a process for purifying bisphosphate comprising solvating a molten bisphosphate in a mixture of water and water miscible solvent; cooling the solution over a period and to a temperature that provides for crystallization of solid product; increasing the pH of the solution prior to, and/or during, and/or after the initiation of crystallization, and/or after crystallization, by the addition of a base; and after crystallization is complete, separating solid product from the solution; washing the separated solid product in the same and/or different mixture of water and water miscible solvent; and, washing the solid product which has been washed in the mixture with water.

    Abstract translation: 本文提供了一种纯化二磷酸盐的方法，其包括在水和水混溶性溶剂的混合物中溶解熔融的二磷酸盐; 在一段时间内将溶液冷却至提供固体产物结晶的温度; 在结晶开始之前和/或期间和/或之后，和/或在结晶后，通过加入碱来增加溶液的pH值; 结晶完成后，将固体产物与溶液分离; 在与水和水混溶的溶剂的相同和/或不同混合物中洗涤分离的固体产物; 并且用水洗涤已经在混合物中洗涤的固体产物。

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