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公开(公告)号：WO2010139054A1
公开(公告)日：2010-12-09
申请号：PCT/CA2010/000816
申请日：2010-05-31
Applicant: INTEGRAN TECHNOLOGIES, INC. , FACCHINI, Diana , GONZALEZ, Francisco , MCCREA, Jonathan , UETZ, Mike , PALUMBO, Gino , TOMANTSCHGER, Klaus , NAGARAJAN, Nandakumar , VICTOR, Jared J. , ERB, Uwe
Inventor： FACCHINI, Diana , GONZALEZ, Francisco , MCCREA, Jonathan , UETZ, Mike , PALUMBO, Gino , TOMANTSCHGER, Klaus , NAGARAJAN, Nandakumar , VICTOR, Jared J. , ERB, Uwe
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness Cr coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial and hydrophobic properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基材的强度，磨损和/或润滑性，而不降低与未涂覆或等效厚度的Cr涂覆的基材相比的疲劳性能。 包含Co的细晶粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其他应力的物品和/或需要抗微生物和疏水性质的应用中。
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2.发明申请PROCESS FOR ELECTROPLATING METALLIC AND METALL MATRIX COMPOSITE FOILS, COATINGS AND MICROCOMPONENTS 审中-公开电镀金属和金属基复合材料，涂料和微生物的方法
公开(公告)号：WO2004001100A1
公开(公告)日：2003-12-31
申请号：PCT/EP2002/007023
申请日：2002-06-25
Applicant: INTEGRAN TECHNOLOGIES, INC. , PALUMBO, Gino , BROOKS, Iain , MCCREA, Jonathan , HIBBARD, Glenn, D. , GONZALEZ, Francisco , TOMANTSCHGER, Klaus , ERB, Uwe
Inventor： PALUMBO, Gino , BROOKS, Iain , MCCREA, Jonathan , HIBBARD, Glenn, D. , GONZALEZ, Francisco , TOMANTSCHGER, Klaus , ERB, Uwe
IPC: C25D1/04
CPC classification number: C25D1/04 , C25D5/02 , C25D5/06 , C25D5/08 , C25D5/18 , C25D5/20 , C25D7/04 , C25D15/00 , C25D15/02
Abstract: The invention relates to a process for forming coatings or free-standing deposits of nano-crystalline metals, metal alloys or metal matrix composites. The process employs drum plating or selective plating processes involving pulse electrode-position and a non-stationary anode or cathode. Novel nano-crystalline metal matrix composites and micro components are disclosed as well. Also described is a process for forming micro-components with grain sizes below 1,000nm.
Abstract translation: 本发明涉及一种用于形成纳米结晶金属，金属合金或金属基质复合材料的涂层或独立沉积物的方法。 该方法采用包括脉冲电极位置和非固定阳极或阴极的鼓电镀或选择性电镀工艺。 还公开了新颖的纳米晶体金属基复合材料和微型组件。 还描述了一种用于形成粒度小于1000nm的微组件的方法。
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公开(公告)号：WO2010139053A1
公开(公告)日：2010-12-09
申请号：PCT/CA2010/000815
申请日：2010-05-31
Applicant: INTEGRAN TECHNOLOGIES, INC. , TOMANTSCHGER, Klaus , MCCREA, Jonathan , NAGARAJAN, Nandakumar , GONZALEZ, Francisco , PALUMBO, Gino , PANAGIOTOPOULOS, Konstantinos , KATUGAHA, Herath , FACCHINI, Diana , VICTOR, Jared J. , ERB, Uwe
Inventor： TOMANTSCHGER, Klaus , MCCREA, Jonathan , NAGARAJAN, Nandakumar , GONZALEZ, Francisco , PALUMBO, Gino , PANAGIOTOPOULOS, Konstantinos , KATUGAHA, Herath , VICTOR, Jared J. , ERB, Uwe
CPC classification number: C23C18/1641 , A63B59/70 , A63B2102/24 , B32B1/08 , B32B3/30 , B32B7/02 , B32B15/08 , B32B15/18 , B32B15/20 , B32B27/08 , B32B27/16 , B32B27/18 , B32B27/20 , B32B27/281 , B32B27/285 , B32B27/288 , B32B27/302 , B32B27/304 , B32B27/308 , B32B27/32 , B32B27/322 , B32B27/34 , B32B27/36 , B32B27/365 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2255/06 , B32B2255/10 , B32B2255/20 , B32B2255/205 , B32B2262/101 , B32B2262/106 , B32B2264/02 , B32B2264/10 , B32B2264/12 , B32B2270/00 , B32B2307/202 , B32B2307/212 , B32B2307/30 , B32B2307/51 , B32B2307/538 , B32B2307/54 , B32B2307/718 , B32B2457/00 , B32B2509/00 , B32B2535/00 , B32B2597/00 , B32B2605/00 , C09J163/00 , C23C14/021 , C23C14/024 , C23C14/028 , C23C16/0227 , C23C16/0254 , C23C16/0272 , C23C18/1851 , C23C18/1855 , C23C18/1893 , C23C18/1896 , C25D5/54 , Y10T428/12111 , Y10T428/12389 , Y10T428/12451 , Y10T428/12472 , Y10T428/12569 , Y10T428/12944 , Y10T428/1355 , Y10T428/24355 , Y10T428/24545 , Y10T428/24612 , Y10T428/26 , Y10T428/269
Abstract: Metal-clad polymer articles containing structural fine-grained and/or amorphous metallic coatings/layers optionally containing solid particulates dispersed therein, are disclosed. The fine-grained and/or amorphous metallic coatings are particularly suited for strong and lightweight articles, precision molds, sporting goods, automotive parts and components exposed to thermal cycling although the coefficient of linear thermal expansion (CLTE) of the metallic layer and the substrate are mismatched. The interface between the metallic layer and the polymer is suitably pretreated to withstand thermal cycling without failure.
Abstract translation: 公开了包含分散在其中的任选地含有固体颗粒的结构细晶粒和/或非晶金属涂层/层的金属包层聚合物制品。 细晶粒和/或非晶金属涂层特别适用于强而轻的制品，精密模具，运动用品，暴露于热循环的汽车部件和部件，尽管金属层和基材的线性热膨胀系数（CLTE） 不匹配。 金属层和聚合物之间的界面适当地经过预处理以承受热循环而不失败。
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4.发明申请
公开(公告)号：WO2006063469A1
公开(公告)日：2006-06-22
申请号：PCT/CA2005/001925
申请日：2005-12-16
Applicant: INTEGRAN TECHNOLOGIES, INC.
Inventor： PALUMBO, Gino , MCCREA, Jonathan , TOMANTSCHGER, Klaus , BROOKS, Iain , JEONG, Daehyun , LIMOGES, Dave , PANAGIOTOPOULOS, Konstantinos , ERB, Uwe
CPC classification number: C25D7/00 , A01K87/00 , A45B9/00 , A63B49/02 , A63B49/10 , A63B49/12 , A63B53/04 , A63B53/0466 , A63B53/047 , A63B53/10 , A63B53/12 , A63B59/00 , A63B59/50 , A63B60/54 , A63B2053/0416 , A63B2209/00 , A63B2209/023 , B82Y30/00 , C23C26/00 , C25D5/00 , C25D15/02 , F42B5/30 , Y10T428/12049 , Y10T428/12201 , Y10T428/12569 , Y10T428/1321 , Y10T428/24612 , Y10T428/249941 , Y10T428/31507 , Y10T428/31511 , Y10T428/31681 , Y10T428/31685 , Y10T428/31692
Abstract: Lightweight articles comprising a polymeric material at least partially coated with a fine-grained metallic material are disclosed. The fine-grained metallic material has an average grain size of 2nm to 5,000nm, a thickness between 25 micron and 5cm, and a hardness between 200VHN and 3,000 VHN. The lightweight articles are strong and ductile and exhibit high coefficients of restitution and a high stiffness and are particularly suitable for a variety of applications including aerospace and automotive parts, sporting goods, and the like.
Abstract translation: 公开了包含至少部分涂覆有细粒金属材料的聚合材料的轻质制品。 细晶金属材料的平均晶粒尺寸为2nm至5,000nm，厚度为25微米至5cm，硬度为200VHN至3,000VHN。 轻型制品是坚固的和延展性的并且表现出高的恢复系数和高刚度，并且特别适用于各种应用，包括航空航天和汽车零件，运动用品等。
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5.发明申请
公开(公告)号：WO2006063468A1
公开(公告)日：2006-06-22
申请号：PCT/CA2005/001923
申请日：2005-12-16
Applicant: INTEGRAN TECHNOLOGIES, INC.
Inventor： PALUMBO, Gino , MCCREA, Jonathan , TOMANTSCHGER, Klaus , BROOKS, Iain , JEONG, Daehyun , LIMOGES, Dave , PANAGIOTOPOULOS, Konstantinos , ERB, Uwe
CPC classification number: C25D7/00 , A01K87/00 , A45B9/00 , A63B49/02 , A63B49/10 , A63B49/12 , A63B53/04 , A63B53/10 , A63B53/12 , A63B59/00 , A63B59/50 , A63B59/70 , A63B60/54 , A63B2053/0416 , A63B2209/00 , A63B2209/02 , A63B2209/023 , B82Y30/00 , C23C24/04 , C23C28/021 , C23C28/027 , C25D5/00 , C25D7/0607 , C25D15/02 , F41H5/0457 , F42B5/30 , F42B6/04 , F42B12/80 , Y10T428/12028 , Y10T428/12063 , Y10T428/12146 , Y10T428/12292 , Y10T428/12493 , Y10T428/12535 , Y10T428/12597 , Y10T428/12674 , Y10T428/12701 , Y10T428/12708 , Y10T428/12736 , Y10T428/12743 , Y10T428/1275 , Y10T428/12757 , Y10T428/12764 , Y10T428/12778 , Y10T428/12937 , Y10T428/12972 , Y10T428/13 , Y10T428/24942 , Y10T428/256 , Y10T428/26 , Y10T428/2918 , Y10T428/2956 , Y10T428/2958 , Y10T428/2964 , Y10T428/30 , Y10T428/31678
Abstract: Fine-grained (average grain size 1nm to 1,000nm) metallic coatings optionally containing solid particulates dispersed therein are disclosed. The fine-grained metallic materials are significantly harder and stronger than conventional coatings of the same chemical composition due to Hall-Petch strengthening and have low linear coefficients of thermal expansion (CTEs). The invention provides means for matching the CTE of the fine-grained metallic coating to the one of the substrate by adjusting the composition of the alloy and/or by varying the chemistry and volume fraction of particulates embedded in the coating. The fine-grained metallic coatings are particularly suited for strong and lightweight articles, precision molds, sporting goods, automotive parts and components exposed to thermal cycling. The low CTEs and the ability to match the CTEs of the fine-grained metallic coatings with the CTEs of the substrate minimize dimensional changes during thermal cycling and prevent premature failure.
Abstract translation: 公开了细颗粒（平均晶粒尺寸1nm至1,000nm）金属涂层，其任选地含有分散在其中的固体颗粒。 由于Hall-Petch强化，细粒金属材料比同一化学成分的常规涂层显着更硬和更强，并且具有低线性热膨胀系数（CTE）。 本发明提供了通过调节合金的组成和/或通过改变嵌入涂层中的微粒的化学和体积分数来匹配细粒金属涂层的CTE与基体之一的方法。 细粒金属涂层特别适用于强而轻的制品，精密模具，运动用品，汽车零件和暴露于热循环的部件。 低CTE和将细粒金属涂层的CTE与衬底的CTE匹配的能力使热循环期间的尺寸变化最小化并防止过早失效。
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Patent Agency Ranking
公开(公告)号：EP0670916B2
公开(公告)日：2003-03-26
申请号：EP94900026.9
申请日：1993-11-26
Applicant: Integran Technologies Inc.
Inventor： ERB, Uwe , EL-SHERIK, Abdelmounam M. , CHEUNG, Cedric K.S. , AUS, Martin J.
CPC classification number: C25D3/562 , C25D3/12 , C25D5/18 , Y10S75/954
Abstract: A process for producing nanocrystalline materials, and in particular nanocrystalline nickel having an average grain size of less than about 11 nanometers and ternary and quaternary nickel-iron alloys, such as NiFeCr and NiFeCrMn alloys, having a grain size less than about 100 nm is described. The nanocrystalline nickel is electrodeposited onto the cathode in an aqueous acidic electrolytic cell by application of a pulsed D.C. current. The ternary and quaternary Nickel-Iron alloys and other binary, ternary and quaternary alloys may be produced by D.C. electroplating or by pulsed d.C. electroplating. The cell electrolyte also contains a stress reliever, such as saccharin, which helps to control the grain size. The novel products of the invention find utility as wear resistant coatings, hydrogen storage materials, magnetic materials and as catalysts for hydrogen evolution.
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7.发明公开
公开(公告)号：EP1737652A1
公开(公告)日：2007-01-03
申请号：EP05821047.7
申请日：2005-12-16
Applicant: Integran Technologies Inc.
Inventor： PALUMBO, Gino , MCCREA, Jonathan , TOMANTSCHGER, Klaus , BROOKS, Iain , JEONG, Daehyun , LIMOGES, Dave , PANAGIOTOPOULOS, Konstantinos , ERB, Uwe , WANG, Andrew
CPC classification number: C25D7/00 , A01K87/00 , A45B9/00 , A63B49/02 , A63B49/10 , A63B49/12 , A63B53/04 , A63B53/0466 , A63B53/047 , A63B53/10 , A63B53/12 , A63B59/00 , A63B59/50 , A63B60/54 , A63B2053/0416 , A63B2209/00 , A63B2209/023 , B82Y30/00 , C23C26/00 , C25D5/00 , C25D15/02 , F42B5/30 , Y10T428/12049 , Y10T428/12201 , Y10T428/12569 , Y10T428/1321 , Y10T428/24612 , Y10T428/249941 , Y10T428/31507 , Y10T428/31511 , Y10T428/31681 , Y10T428/31685 , Y10T428/31692
Abstract: Lightweight articles comprising a polymeric material at least partially coated with a fine-grained metallic material are disclosed. The fine-grained metallic material has an average grain size of 2nm to 5,000nm, a thickness between 25 micron and 5cm, and a hardness between 200VHN and 3,000 VHN. The lightweight articles are strong and ductile and exhibit high coefficients of restitution and a high stiffness and are particularly suitable for a variety of applications including aerospace and automotive parts, sporting goods, and the like.
Abstract translation: 公开了包含至少部分涂覆有细粒金属材料的聚合物材料的轻量制品。 细粒金属材料具有2nm至5,000nm的平均粒径，25微米至5cm的厚度以及200VHN至3,000VHN的硬度。 轻质制品坚固且具有延展性，并且具有高恢复系数和高刚度，并且特别适用于各种应用，包括航空和汽车部件，体育用品等。
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公开(公告)号：EP2438216A1
公开(公告)日：2012-04-11
申请号：EP10782857.6
申请日：2010-05-31
Applicant: Integran Technologies Inc.
Inventor： FACCHINI, Diana , GONZALEZ, Francisco , MCCREA, Jonathan , UETZ, Mike , PALUMBO, Gino , TOMANTSCHGER, Klaus , NAGARAJAN, Nandakumar , VICTOR, Jared J. , ERB, Uwe
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness Cr coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial and hydrophobic properties.
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9.发明授权PROCESS FOR ELECTROPLATING METALLIC AND METALL MATRIX COMPOSITE FOILS, COATINGS AND MICROCOMPONENTS 有权电镀法金属和金属基复合薄膜，涂层和微型元件
公开(公告)号：EP1516076B1
公开(公告)日：2008-02-27
申请号：EP02754753.8
申请日：2002-06-25
Applicant: Integran Technologies Inc.
Inventor： PALUMBO, Gino , BROOKS, Iain , MCCREA, Jonathan , HIBBARD, Glenn, D. , GONZALEZ, Francisco , TOMANTSCHGER, Klaus , ERB, Uwe
CPC classification number: C25D1/04 , C25D5/02 , C25D5/06 , C25D5/08 , C25D5/18 , C25D5/20 , C25D7/04 , C25D15/00 , C25D15/02
Abstract: The invention relates to a process for forming coatings or free-standing deposits of nanocrystalline metals, metal alloys or metal matrix composites. The process employs drum plating or selective plating processes involving pulse electrodeposition and a non-stationary anode or cathode. Novel nanocrystalline metal matrix composites and micro components are disclosed as well. Also described is a process for forming micro components with grain sizes below 1,000nm.
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公开(公告)号：EP2437935A1
公开(公告)日：2012-04-11
申请号：EP10782856.8
申请日：2010-05-31
Applicant: Integran Technologies Inc.
Inventor： TOMANTSCHGER, Klaus , MCCREA, Jonathan , NAGARAJAN, Nandakumar , GONZALEZ, Francisco , PALUMBO, Gino , PANAGIOTOPOULOS, Konstantinos , KATUGAHA, Herath , VICTOR, Jared J. , ERB, Uwe , FACCHINI, Diana
CPC classification number: C23C18/1641 , A63B59/70 , A63B2102/24 , B32B1/08 , B32B3/30 , B32B7/02 , B32B15/08 , B32B15/18 , B32B15/20 , B32B27/08 , B32B27/16 , B32B27/18 , B32B27/20 , B32B27/281 , B32B27/285 , B32B27/288 , B32B27/302 , B32B27/304 , B32B27/308 , B32B27/32 , B32B27/322 , B32B27/34 , B32B27/36 , B32B27/365 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2255/06 , B32B2255/10 , B32B2255/20 , B32B2255/205 , B32B2262/101 , B32B2262/106 , B32B2264/02 , B32B2264/10 , B32B2264/12 , B32B2270/00 , B32B2307/202 , B32B2307/212 , B32B2307/30 , B32B2307/51 , B32B2307/538 , B32B2307/54 , B32B2307/718 , B32B2457/00 , B32B2509/00 , B32B2535/00 , B32B2597/00 , B32B2605/00 , C09J163/00 , C23C14/021 , C23C14/024 , C23C14/028 , C23C16/0227 , C23C16/0254 , C23C16/0272 , C23C18/1851 , C23C18/1855 , C23C18/1893 , C23C18/1896 , C25D5/54 , Y10T428/12111 , Y10T428/12389 , Y10T428/12451 , Y10T428/12472 , Y10T428/12569 , Y10T428/12944 , Y10T428/1355 , Y10T428/24355 , Y10T428/24545 , Y10T428/24612 , Y10T428/26 , Y10T428/269
Abstract: Metal-clad polymer articles containing structural fine-grained and/or amorphous metallic coatings/layers optionally containing solid particulates dispersed therein, are disclosed. The fine-grained and/or amorphous metallic coatings are particularly suited for strong and lightweight articles, precision molds, sporting goods, automotive parts and components exposed to thermal cycling although the coefficient of linear thermal expansion (CLTE) of the metallic layer and the substrate are mismatched. The interface between the metallic layer and the polymer is suitably pretreated to withstand thermal cycling without failure.
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